#------------------------------------------------------------------------------ #$Date: 2020-05-08 11:07:35 +0300 (Fri, 08 May 2020) $ #$Revision: 251905 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/3/50/01/3500104.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500104 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.0723 _cell_length_b 13.3794 _cell_length_c 4.8987 _exptl_crystal_F_000 360.00 _reflns_d_resolution_high 0.7699 _cod_data_source_file 35phcl.fcf _cod_data_source_block 35phcl _shelx_title ' diop372_a.res in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 77.84 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1684.82 1544.24 35.72 o 6 0 0 41.32 28.68 0.66 o 8 0 0 4401.63 4665.47 186.21 o 10 0 0 248.02 269.70 6.84 o 12 0 0 769.13 795.91 18.57 o 14 0 0 444.10 483.26 15.30 o 2 1 0 11.01 12.10 0.59 o 4 1 0 2679.90 2482.67 99.11 o 6 1 0 500.46 482.06 6.46 o 8 1 0 884.09 912.10 12.93 o 10 1 0 185.85 169.29 2.55 o 12 1 0 249.36 257.35 4.07 o 14 1 0 11.82 12.35 0.84 o 2 2 0 150.29 137.80 3.28 o 4 2 0 76.25 79.97 1.28 o 6 2 0 573.94 514.68 6.92 o 8 2 0 683.97 717.24 9.12 o 10 2 0 10.33 13.19 0.53 o 12 2 0 28.62 30.02 0.81 o 14 2 0 337.98 378.69 11.70 o 4 3 0 1039.13 946.86 13.38 o 6 3 0 224.54 202.86 3.46 o 8 3 0 180.97 181.29 2.52 o 10 3 0 2212.22 2320.45 35.06 o 12 3 0 10.96 9.36 0.82 o 14 3 0 150.42 171.31 5.06 o 0 4 0 1119.41 1146.30 45.74 o 2 4 0 2826.46 3000.98 119.73 o 4 4 0 1640.28 1731.47 30.85 o 6 4 0 571.63 520.52 7.91 o 8 4 0 530.73 527.26 7.54 o 10 4 0 179.73 178.75 2.91 o 12 4 0 1052.16 1114.35 20.07 o 14 4 0 24.43 26.74 1.02 o 2 5 0 246.90 259.22 5.23 o 4 5 0 1657.55 1674.78 25.30 o 6 5 0 326.35 327.94 5.04 o 8 5 0 326.69 323.25 5.00 o 10 5 0 275.94 283.37 4.45 o 12 5 0 0.65 3.58 0.63 o 14 5 0 251.99 247.64 4.66 o 0 6 0 6058.83 5960.85 168.56 o 2 6 0 1754.97 1894.53 33.82 o 4 6 0 3485.10 3971.32 121.00 o 6 6 0 5.41 3.09 0.29 o 8 6 0 737.24 753.61 11.49 o 10 6 0 344.88 353.67 5.15 o 12 6 0 2357.06 2517.22 45.01 o 14 6 0 1.77 2.17 0.56 o 2 7 0 1508.10 1458.80 45.54 o 4 7 0 575.99 538.52 8.86 o 6 7 0 237.95 239.78 4.05 o 8 7 0 315.58 317.53 4.94 o 10 7 0 1081.59 1106.41 15.74 o 12 7 0 5.77 5.95 0.66 o 14 7 0 1.90 2.15 0.63 o 0 8 0 4.81 2.21 0.32 o 2 8 0 531.06 578.73 11.71 o 4 8 0 0.29 0.27 0.23 o 6 8 0 467.83 460.83 9.36 o 8 8 0 122.22 128.97 2.55 o 10 8 0 39.36 41.26 0.90 o 12 8 0 60.89 62.10 4.77 o 2 9 0 1727.42 1861.47 43.97 o 4 9 0 358.24 360.29 7.36 o 6 9 0 144.86 127.37 2.52 o 8 9 0 136.70 132.67 2.63 o 10 9 0 688.11 695.75 10.66 o 12 9 0 59.71 60.17 1.77 o 0 10 0 5972.87 6315.62 216.39 o 2 10 0 132.34 131.29 2.54 o 4 10 0 130.33 121.27 2.39 o 6 10 0 180.54 200.70 4.27 o 8 10 0 1044.45 1041.51 18.23 o 10 10 0 89.24 89.33 1.76 o 12 10 0 212.36 206.66 6.18 o 2 11 0 94.44 98.79 2.01 o 4 11 0 858.93 871.97 15.73 o 6 11 0 88.29 92.48 1.97 o 8 11 0 348.11 331.80 6.90 o 10 11 0 3.37 1.43 0.55 o 12 11 0 138.24 130.89 4.12 o 0 12 0 3753.02 4098.09 115.71 o 2 12 0 127.48 123.80 3.48 o 4 12 0 26.19 24.97 0.90 o 6 12 0 20.97 27.72 0.95 o 8 12 0 746.50 725.36 12.01 o 10 12 0 23.75 16.46 0.94 o 2 13 0 842.08 891.63 20.83 o 4 13 0 288.47 298.76 5.59 o 6 13 0 50.92 48.57 1.34 o 8 13 0 162.19 163.22 2.93 o 10 13 0 457.87 450.08 8.21 o 0 14 0 49.12 50.45 2.64 o 2 14 0 106.75 113.49 2.63 o 4 14 0 2.69 2.44 0.66 o 6 14 0 132.76 130.29 2.67 o 8 14 0 69.44 66.73 1.54 o 2 15 0 120.69 123.57 3.29 o 4 15 0 110.67 116.54 2.70 o 6 15 0 39.94 42.76 1.39 o 0 16 0 493.01 511.29 12.04 o 2 16 0 245.54 258.45 4.89 o 4 16 0 463.94 492.77 14.23 o 6 16 0 18.64 12.22 0.89 o 2 17 0 4.32 4.19 0.80 o 1 0 1 244.61 265.99 16.51 o 4 0 1 2097.85 2281.91 32.18 o 5 0 1 433.59 433.57 5.82 o 6 0 1 1104.10 1197.44 17.19 o 7 0 1 380.17 397.87 5.79 o 8 0 1 11.12 13.77 0.46 o 9 0 1 249.84 251.50 3.94 o 10 0 1 1527.68 1572.48 23.81 o 11 0 1 771.34 777.97 11.89 o 12 0 1 28.95 28.50 0.87 o 13 0 1 145.02 149.42 2.73 o 14 0 1 75.05 74.95 2.13 o 15 0 1 57.65 60.27 2.02 o 0 1 1 140.53 149.80 3.81 o 1 1 1 1.94 1.18 0.12 o 2 1 1 2794.16 3016.20 53.84 o 3 1 1 1102.18 1113.13 12.83 o 4 1 1 11.30 9.22 0.18 o 5 1 1 972.84 1030.80 10.30 o 6 1 1 2176.67 2266.67 21.31 o 7 1 1 98.48 79.15 0.87 o 8 1 1 76.84 65.96 0.82 o 9 1 1 125.69 125.49 1.46 o 10 1 1 0.39 1.31 0.21 o 11 1 1 28.59 29.71 0.58 o 12 1 1 135.85 136.97 1.76 o 13 1 1 40.87 43.46 0.80 o 14 1 1 74.93 87.50 2.14 o 15 1 1 136.67 133.12 1.91 o 1 2 1 848.95 892.66 18.12 o 2 2 1 1300.92 1290.28 19.47 o 3 2 1 536.40 565.18 6.04 o 4 2 1 701.05 660.46 6.42 o 5 2 1 82.77 71.95 0.80 o 6 2 1 211.50 211.71 2.24 o 7 2 1 29.20 29.89 0.39 o 8 2 1 376.86 374.33 3.59 o 9 2 1 0.95 1.10 0.18 o 10 2 1 243.23 249.24 2.79 o 11 2 1 219.28 229.80 2.69 o 12 2 1 65.87 65.80 0.95 o 13 2 1 18.01 19.45 0.61 o 14 2 1 0.65 0.36 0.39 o 15 2 1 14.67 16.24 0.95 o 1 3 1 3268.61 3157.25 125.92 o 2 3 1 10.13 8.57 0.17 o 3 3 1 114.16 113.86 1.43 o 4 3 1 309.07 282.01 3.16 o 5 3 1 1079.90 1077.40 10.43 o 6 3 1 6.90 4.94 0.18 o 7 3 1 1155.23 1150.03 11.17 o 8 3 1 1085.77 1068.52 10.10 o 9 3 1 0.78 0.40 0.17 o 10 3 1 0.60 0.39 0.22 o 11 3 1 127.63 127.74 1.63 o 12 3 1 413.33 409.99 4.86 o 13 3 1 284.13 293.12 3.68 o 14 3 1 44.43 44.89 0.88 o 15 3 1 46.78 44.53 1.12 o 1 4 1 1337.42 1391.70 18.51 o 2 4 1 1151.74 1198.77 13.81 o 3 4 1 246.59 215.95 2.44 o 4 4 1 1048.69 1006.74 10.42 o 5 4 1 704.96 716.84 7.18 o 6 4 1 19.42 18.24 0.31 o 7 4 1 62.77 72.81 0.76 o 8 4 1 1.88 1.72 0.16 o 9 4 1 348.74 342.52 3.51 o 10 4 1 586.69 597.06 7.68 o 11 4 1 33.79 32.09 0.62 o 12 4 1 113.38 116.30 1.60 o 13 4 1 106.17 105.31 1.50 o 14 4 1 101.03 103.46 1.54 o 15 4 1 201.08 190.63 3.65 o 0 5 1 149.39 127.53 2.62 o 1 5 1 3.74 4.45 0.18 o 2 5 1 336.61 303.99 3.17 o 3 5 1 208.18 209.63 2.29 o 4 5 1 213.95 238.17 2.89 o 5 5 1 1.81 2.40 0.13 o 6 5 1 1668.61 1724.51 17.22 o 7 5 1 413.04 391.03 3.98 o 8 5 1 336.71 332.09 3.40 o 9 5 1 32.79 32.17 0.54 o 10 5 1 298.04 309.40 3.56 o 11 5 1 168.82 170.14 2.12 o 12 5 1 26.60 25.02 0.68 o 13 5 1 150.54 153.76 2.13 o 14 5 1 186.80 186.58 2.54 o 1 6 1 1956.38 2172.94 28.89 o 2 6 1 2701.88 2867.39 43.23 o 3 6 1 393.03 319.46 3.59 o 4 6 1 78.89 68.57 0.88 o 5 6 1 738.36 779.11 8.68 o 6 6 1 23.35 30.76 0.49 o 7 6 1 92.43 100.74 1.11 o 8 6 1 268.95 276.64 2.95 o 9 6 1 584.00 590.29 6.40 o 10 6 1 1187.65 1213.77 12.58 o 11 6 1 17.55 17.48 0.54 o 12 6 1 127.07 127.94 1.83 o 13 6 1 74.26 72.77 1.33 o 14 6 1 306.84 291.30 4.05 o 0 7 1 1720.14 1841.82 24.49 o 1 7 1 346.15 301.33 3.16 o 2 7 1 12.78 6.90 0.25 o 3 7 1 68.80 70.27 0.85 o 4 7 1 13.51 9.61 0.34 o 5 7 1 388.97 373.21 4.07 o 6 7 1 314.39 323.41 3.54 o 7 7 1 692.32 689.24 7.43 o 8 7 1 623.54 613.85 6.89 o 9 7 1 15.43 16.69 0.45 o 10 7 1 100.85 102.32 1.28 o 11 7 1 0.61 0.77 0.28 o 12 7 1 38.13 41.08 0.85 o 13 7 1 222.65 221.77 3.15 o 14 7 1 70.05 71.12 2.17 o 1 8 1 0.86 0.29 0.14 o 2 8 1 29.23 23.10 0.46 o 3 8 1 41.97 35.09 0.57 o 4 8 1 1022.94 1021.88 11.83 o 5 8 1 146.37 146.85 1.74 o 6 8 1 6.60 6.21 0.26 o 7 8 1 2.78 3.34 0.25 o 8 8 1 153.52 146.93 1.78 o 9 8 1 3.96 3.37 0.26 o 10 8 1 101.51 109.95 1.36 o 11 8 1 37.19 38.13 0.75 o 12 8 1 76.46 74.91 1.47 o 13 8 1 92.24 88.25 1.52 o 0 9 1 922.81 944.32 18.56 o 1 9 1 396.29 401.57 5.17 o 2 9 1 98.83 96.63 1.30 o 3 9 1 100.01 84.74 1.16 o 4 9 1 101.67 113.68 1.78 o 5 9 1 399.52 392.38 5.35 o 6 9 1 87.37 82.47 1.24 o 7 9 1 248.92 255.53 3.56 o 8 9 1 304.21 301.29 3.62 o 9 9 1 33.32 30.84 0.62 o 10 9 1 6.30 6.49 0.35 o 11 9 1 57.33 54.83 0.99 o 12 9 1 230.71 231.66 3.69 o 13 9 1 88.85 81.95 1.79 o 1 10 1 12.43 13.05 0.44 o 2 10 1 1464.05 1519.55 17.56 o 3 10 1 1187.65 1240.26 14.35 o 4 10 1 19.55 14.48 0.53 o 5 10 1 64.80 53.36 0.97 o 6 10 1 179.83 173.07 2.65 o 7 10 1 86.68 83.01 1.36 o 8 10 1 26.59 27.20 0.67 o 9 10 1 95.67 94.42 1.31 o 10 10 1 418.69 415.52 5.40 o 11 10 1 272.04 272.13 3.85 o 12 10 1 16.78 17.35 0.98 o 0 11 1 188.75 187.71 3.58 o 1 11 1 0.75 0.85 0.29 o 2 11 1 720.87 748.44 9.56 o 3 11 1 171.85 172.71 2.36 o 4 11 1 8.15 5.61 0.37 o 5 11 1 118.73 105.98 1.75 o 6 11 1 966.36 941.04 12.66 o 7 11 1 1.45 2.95 0.38 o 8 11 1 0.64 1.16 0.36 o 9 11 1 50.25 50.93 0.94 o 10 11 1 0.04 1.07 0.39 o 11 11 1 1.50 2.45 0.45 o 1 12 1 55.20 52.38 0.96 o 2 12 1 956.75 987.09 13.26 o 3 12 1 587.99 620.36 9.53 o 4 12 1 30.20 23.83 0.64 o 5 12 1 40.88 35.57 0.92 o 6 12 1 159.62 147.88 2.08 o 7 12 1 19.42 16.53 0.73 o 8 12 1 11.24 10.87 0.47 o 9 12 1 6.81 8.20 0.42 o 10 12 1 285.00 278.38 3.89 o 11 12 1 222.19 211.81 3.67 o 0 13 1 368.84 382.87 6.45 o 1 13 1 244.38 254.18 3.57 o 2 13 1 57.98 59.86 1.39 o 3 13 1 31.08 29.83 0.93 o 4 13 1 59.04 61.91 1.12 o 5 13 1 344.98 338.72 4.70 o 6 13 1 78.16 75.97 1.24 o 7 13 1 205.79 215.43 2.79 o 8 13 1 137.87 145.84 1.87 o 9 13 1 8.72 6.08 0.43 o 10 13 1 3.44 2.66 0.55 o 1 14 1 0.18 0.08 0.36 o 2 14 1 33.32 36.54 0.95 o 3 14 1 28.86 27.35 0.84 o 4 14 1 224.85 226.80 3.23 o 5 14 1 48.65 53.02 1.01 o 6 14 1 11.93 10.13 0.55 o 7 14 1 9.06 6.73 0.43 o 8 14 1 62.30 55.75 1.20 o 0 15 1 230.13 248.79 5.20 o 1 15 1 30.27 29.13 0.79 o 2 15 1 11.49 9.57 0.47 o 3 15 1 14.71 15.31 0.62 o 4 15 1 0.97 0.79 0.40 o 5 15 1 11.29 11.18 0.64 o 6 15 1 77.01 77.32 1.75 o 7 15 1 108.63 117.83 2.66 o 1 16 1 276.43 286.32 4.22 o 2 16 1 294.90 304.12 4.46 o 3 16 1 67.95 63.61 1.30 o 4 16 1 25.12 23.97 1.53 o 5 16 1 137.17 137.88 3.04 o 0 17 1 33.41 33.57 2.51 o 1 17 1 15.95 11.39 0.91 o 2 17 1 20.32 17.14 0.99 o 0 0 2 205.99 217.01 4.41 o 1 0 2 1734.00 1690.96 33.76 o 2 0 2 551.41 573.41 8.95 o 3 0 2 624.87 707.97 10.74 o 4 0 2 416.18 408.25 5.59 o 5 0 2 1964.67 1965.65 24.80 o 6 0 2 2224.05 2439.12 36.74 o 7 0 2 301.61 277.68 4.30 o 8 0 2 157.92 160.70 2.58 o 9 0 2 338.32 352.31 5.92 o 10 0 2 234.04 239.30 4.50 o 11 0 2 95.30 89.38 1.76 o 12 0 2 69.93 64.97 1.42 o 13 0 2 643.43 653.60 11.88 o 14 0 2 36.56 31.89 1.25 o 1 1 2 61.45 53.08 0.71 o 2 1 2 790.48 889.09 10.72 o 3 1 2 1228.58 1285.18 13.72 o 4 1 2 3220.53 3456.47 40.38 o 5 1 2 1208.68 1194.54 10.41 o 6 1 2 375.96 393.00 3.98 o 7 1 2 164.02 173.81 1.89 o 8 1 2 7.15 7.20 0.36 o 9 1 2 556.98 544.16 6.38 o 10 1 2 31.75 26.26 0.61 o 11 1 2 89.72 103.53 1.39 o 12 1 2 0.77 0.64 0.32 o 13 1 2 124.80 115.74 1.65 o 14 1 2 0.46 0.44 0.42 o 0 2 2 73.96 68.38 1.23 o 1 2 2 831.11 824.45 9.52 o 2 2 2 624.38 654.79 7.48 o 3 2 2 394.47 388.98 4.22 o 4 2 2 42.72 39.73 0.41 o 5 2 2 1502.09 1594.18 14.52 o 6 2 2 472.36 457.04 4.48 o 7 2 2 413.56 399.37 4.34 o 8 2 2 19.17 18.96 0.45 o 9 2 2 71.13 70.61 1.00 o 10 2 2 15.36 15.77 0.52 o 11 2 2 4.82 6.56 0.34 o 12 2 2 22.54 21.40 0.62 o 13 2 2 421.56 456.37 6.83 o 14 2 2 23.87 23.97 0.79 o 1 3 2 152.52 129.64 1.74 o 2 3 2 110.19 104.67 1.36 o 3 3 2 1559.78 1536.20 18.16 o 4 3 2 768.16 741.21 7.03 o 5 3 2 1039.50 1029.76 9.45 o 6 3 2 50.16 40.28 0.51 o 7 3 2 53.76 47.65 0.61 o 8 3 2 138.82 141.00 1.63 o 9 3 2 539.59 531.99 6.01 o 10 3 2 6.44 5.53 0.30 o 11 3 2 302.25 307.01 3.69 o 12 3 2 7.32 7.40 0.50 o 13 3 2 16.89 20.13 0.89 o 14 3 2 10.52 10.24 0.61 o 0 4 2 124.47 119.28 2.24 o 1 4 2 1334.54 1299.77 17.84 o 2 4 2 8.18 9.27 0.27 o 3 4 2 1.17 0.54 0.10 o 4 4 2 14.32 17.08 0.26 o 5 4 2 427.04 417.83 3.99 o 6 4 2 16.37 15.68 0.36 o 7 4 2 1041.27 1056.26 10.28 o 8 4 2 0.06 0.41 0.22 o 9 4 2 19.29 19.49 0.51 o 10 4 2 22.18 24.89 0.59 o 11 4 2 20.56 20.99 0.63 o 12 4 2 4.94 4.42 0.39 o 13 4 2 288.72 297.89 4.23 o 14 4 2 45.70 42.70 1.26 o 1 5 2 180.84 230.38 2.98 o 2 5 2 11.73 10.66 0.25 o 3 5 2 1307.20 1360.32 16.21 o 4 5 2 394.02 402.24 3.95 o 5 5 2 980.71 931.30 9.06 o 6 5 2 472.10 473.88 4.80 o 7 5 2 388.48 371.25 4.06 o 8 5 2 1770.60 1806.37 18.67 o 9 5 2 72.82 74.91 1.12 o 10 5 2 128.06 126.02 1.71 o 11 5 2 265.43 272.63 3.63 o 12 5 2 2.24 1.61 0.39 o 13 5 2 48.45 50.43 1.11 o 14 5 2 28.83 28.01 1.18 o 0 6 2 716.61 799.58 10.70 o 1 6 2 1426.96 1476.43 14.32 o 2 6 2 371.67 384.37 3.67 o 3 6 2 12.32 15.57 0.28 o 4 6 2 20.56 18.03 0.36 o 5 6 2 119.03 109.32 1.23 o 6 6 2 272.80 269.48 3.37 o 7 6 2 1085.55 1125.18 12.08 o 8 6 2 5.15 4.78 0.28 o 9 6 2 35.49 33.58 0.63 o 10 6 2 200.43 197.46 2.67 o 11 6 2 52.63 51.88 0.99 o 12 6 2 26.64 25.67 0.94 o 13 6 2 259.12 252.80 3.77 o 1 7 2 1.66 4.91 0.17 o 2 7 2 8.46 9.66 0.27 o 3 7 2 1160.27 1236.00 12.79 o 4 7 2 65.57 63.87 0.89 o 5 7 2 678.00 671.61 7.53 o 6 7 2 293.06 289.21 3.46 o 7 7 2 231.54 228.14 2.68 o 8 7 2 125.74 127.39 1.58 o 9 7 2 180.67 181.26 2.17 o 10 7 2 33.27 36.23 0.80 o 11 7 2 258.97 266.06 3.96 o 12 7 2 5.62 5.53 0.46 o 13 7 2 19.36 17.52 0.85 o 0 8 2 0.31 0.44 0.20 o 1 8 2 400.34 376.90 3.43 o 2 8 2 262.88 253.78 2.80 o 3 8 2 88.88 93.39 1.17 o 4 8 2 0.85 1.12 0.24 o 5 8 2 398.42 383.76 4.36 o 6 8 2 595.07 591.21 6.58 o 7 8 2 397.90 397.07 4.93 o 8 8 2 1.77 1.60 0.27 o 9 8 2 11.34 11.95 0.47 o 10 8 2 18.27 19.27 0.64 o 11 8 2 0.62 0.45 0.48 o 12 8 2 7.16 6.49 0.56 o 13 8 2 205.72 195.89 5.90 o 1 9 2 80.29 89.26 0.99 o 2 9 2 1.22 2.30 0.22 o 3 9 2 553.71 521.42 6.71 o 4 9 2 1.38 1.51 0.26 o 5 9 2 473.78 491.79 6.05 o 6 9 2 26.60 26.47 0.62 o 7 9 2 32.48 33.47 0.70 o 8 9 2 70.02 70.04 1.08 o 9 9 2 316.54 338.73 5.37 o 10 9 2 30.58 32.14 0.76 o 11 9 2 109.96 103.48 2.34 o 12 9 2 0.18 1.12 0.81 o 0 10 2 26.06 24.17 0.67 o 1 10 2 430.11 439.66 4.65 o 2 10 2 5.03 3.87 0.27 o 3 10 2 70.50 65.68 1.07 o 4 10 2 26.71 29.88 0.71 o 5 10 2 656.62 677.26 8.69 o 6 10 2 240.99 236.07 3.01 o 7 10 2 174.43 171.44 2.50 o 8 10 2 47.83 45.97 0.95 o 9 10 2 104.13 104.45 1.65 o 10 10 2 50.14 49.42 1.02 o 11 10 2 32.11 29.07 1.83 o 1 11 2 17.14 17.59 0.56 o 2 11 2 229.25 202.89 2.54 o 3 11 2 265.19 231.36 2.95 o 4 11 2 1564.69 1564.00 20.91 o 5 11 2 376.61 414.35 6.05 o 6 11 2 180.10 174.99 2.41 o 7 11 2 47.96 49.91 1.01 o 8 11 2 56.17 55.30 1.14 o 9 11 2 198.31 206.30 3.14 o 10 11 2 16.01 19.20 0.91 o 11 11 2 13.13 10.76 1.46 o 0 12 2 91.65 87.54 1.74 o 1 12 2 232.37 236.84 3.02 o 2 12 2 0.10 0.04 0.34 o 3 12 2 104.71 95.16 1.79 o 4 12 2 85.77 89.04 1.45 o 5 12 2 451.60 457.12 5.94 o 6 12 2 69.26 66.93 1.34 o 7 12 2 76.11 80.63 1.47 o 8 12 2 31.90 29.95 0.79 o 9 12 2 85.01 86.60 1.38 o 10 12 2 8.20 7.88 0.80 o 1 13 2 55.14 58.05 1.05 o 2 13 2 30.38 27.41 0.78 o 3 13 2 317.95 310.82 4.60 o 4 13 2 0.02 -0.15 0.40 o 5 13 2 223.00 234.65 3.35 o 6 13 2 8.97 7.16 0.50 o 7 13 2 23.26 23.09 0.82 o 8 13 2 97.86 92.50 1.66 o 9 13 2 213.86 223.55 6.53 o 0 14 2 1.28 2.37 0.78 o 1 14 2 129.17 128.69 2.24 o 2 14 2 51.11 48.64 1.17 o 3 14 2 43.07 43.73 1.01 o 4 14 2 0.26 0.66 0.44 o 5 14 2 174.05 166.91 2.61 o 6 14 2 158.67 147.97 2.34 o 7 14 2 122.82 134.36 5.91 o 1 15 2 0.45 0.13 0.58 o 2 15 2 33.78 34.40 1.14 o 3 15 2 217.54 219.81 4.80 o 4 15 2 0.02 0.39 0.68 o 5 15 2 156.18 169.59 6.59 o 6 15 2 42.54 51.14 1.53 o 0 16 2 60.05 62.57 3.78 o 1 16 2 218.07 239.93 7.63 o 2 16 2 70.48 72.74 3.17 o 3 16 2 9.32 8.13 0.73 o 1 0 3 255.94 252.31 3.92 o 2 0 3 0.54 1.20 0.19 o 3 0 3 89.59 76.14 1.15 o 4 0 3 1311.04 1374.92 17.40 o 5 0 3 98.05 90.70 1.29 o 6 0 3 66.85 74.37 1.10 o 7 0 3 3.62 4.58 0.55 o 8 0 3 577.64 564.61 11.05 o 9 0 3 8.79 9.88 0.66 o 10 0 3 33.04 29.71 1.27 o 11 0 3 331.90 318.75 6.66 o 12 0 3 7.20 7.69 0.84 o 13 0 3 32.08 34.85 2.06 o 0 1 3 2301.55 2522.89 38.08 o 1 1 3 915.87 928.29 9.31 o 2 1 3 159.31 182.75 1.84 o 3 1 3 0.21 0.26 0.14 o 4 1 3 107.40 106.66 1.07 o 5 1 3 47.27 42.05 0.54 o 6 1 3 23.30 28.48 0.42 o 7 1 3 2056.07 2041.32 23.46 o 8 1 3 402.41 433.11 5.62 o 9 1 3 83.23 67.37 1.15 o 10 1 3 0.06 0.61 0.42 o 11 1 3 3.39 4.99 0.50 o 12 1 3 129.05 131.68 3.54 o 13 1 3 130.69 124.07 2.27 o 1 2 3 210.97 199.47 2.29 o 2 2 3 555.18 545.36 5.33 o 3 2 3 1458.96 1477.61 14.77 o 4 2 3 0.66 0.79 0.14 o 5 2 3 626.42 630.71 5.55 o 6 2 3 27.28 27.87 0.48 o 7 2 3 183.03 165.92 2.08 o 8 2 3 1.25 2.53 0.32 o 9 2 3 253.69 259.08 3.47 o 10 2 3 231.22 238.15 3.06 o 11 2 3 335.65 337.67 4.70 o 12 2 3 2.37 1.23 0.60 o 13 2 3 8.46 6.52 0.57 o 0 3 3 121.91 124.75 1.89 o 1 3 3 159.77 155.62 1.69 o 2 3 3 372.71 343.11 4.23 o 3 3 3 61.80 55.68 0.70 o 4 3 3 1.37 0.71 0.14 o 5 3 3 106.73 96.85 1.08 o 6 3 3 496.99 482.61 5.25 o 7 3 3 193.50 180.08 2.85 o 8 3 3 96.24 99.09 1.57 o 9 3 3 99.06 98.38 1.58 o 10 3 3 14.49 13.22 0.59 o 11 3 3 6.91 6.43 0.57 o 12 3 3 76.40 75.11 1.56 o 13 3 3 49.42 50.87 1.31 o 1 4 3 94.35 89.34 1.16 o 2 4 3 285.16 281.12 3.35 o 3 4 3 685.58 658.96 7.37 o 4 4 3 87.17 82.26 0.90 o 5 4 3 131.91 130.12 1.50 o 6 4 3 30.46 32.30 0.59 o 7 4 3 1.17 1.84 0.29 o 8 4 3 61.49 60.87 1.10 o 9 4 3 240.99 232.94 3.51 o 10 4 3 200.96 207.40 3.17 o 11 4 3 221.99 232.31 4.46 o 12 4 3 1.00 1.75 0.53 o 13 4 3 6.51 4.41 0.82 o 0 5 3 872.51 853.16 15.33 o 1 5 3 341.91 334.53 4.33 o 2 5 3 0.94 2.39 0.21 o 3 5 3 1108.73 1163.53 13.51 o 4 5 3 314.34 294.87 3.14 o 5 5 3 2626.43 2791.94 29.80 o 6 5 3 132.69 125.21 1.66 o 7 5 3 135.69 134.91 1.89 o 8 5 3 181.28 177.42 2.57 o 9 5 3 100.56 102.00 1.85 o 10 5 3 99.59 101.35 1.88 o 11 5 3 123.34 127.60 3.57 o 12 5 3 355.15 358.70 5.63 o 13 5 3 241.19 254.52 6.19 o 1 6 3 176.10 180.38 2.20 o 2 6 3 20.34 19.15 0.40 o 3 6 3 347.62 342.56 3.75 o 4 6 3 523.81 519.74 5.45 o 5 6 3 7.69 8.23 0.32 o 6 6 3 73.49 71.25 1.09 o 7 6 3 98.11 95.77 1.51 o 8 6 3 308.04 310.81 4.32 o 9 6 3 182.20 180.75 2.80 o 10 6 3 82.91 81.96 1.62 o 11 6 3 159.58 156.32 4.42 o 12 6 3 6.47 5.68 0.57 o 0 7 3 285.58 299.20 4.67 o 1 7 3 81.37 74.08 0.88 o 2 7 3 62.00 57.90 0.78 o 3 7 3 432.47 443.54 5.02 o 4 7 3 117.95 116.39 1.45 o 5 7 3 639.74 649.89 7.62 o 6 7 3 44.34 43.41 0.95 o 7 7 3 51.45 48.47 1.02 o 8 7 3 103.93 103.81 1.64 o 9 7 3 137.86 134.49 2.50 o 10 7 3 8.94 7.98 0.63 o 11 7 3 17.61 14.23 1.63 o 12 7 3 177.44 170.65 4.34 o 1 8 3 116.71 107.26 1.25 o 2 8 3 407.41 385.40 4.23 o 3 8 3 912.88 932.99 10.86 o 4 8 3 25.82 24.42 0.59 o 5 8 3 299.86 302.15 4.46 o 6 8 3 24.90 25.42 0.82 o 7 8 3 95.88 97.14 1.56 o 8 8 3 8.03 8.40 0.55 o 9 8 3 272.96 269.70 4.31 o 10 8 3 210.95 202.72 4.40 o 11 8 3 170.20 171.38 3.85 o 0 9 3 207.13 198.28 3.43 o 1 9 3 212.19 212.97 2.49 o 2 9 3 41.54 41.89 0.71 o 3 9 3 0.50 0.85 0.30 o 4 9 3 2.46 2.79 0.43 o 5 9 3 19.24 18.47 0.75 o 6 9 3 123.31 117.97 2.07 o 7 9 3 438.90 462.93 7.52 o 8 9 3 93.08 92.55 1.72 o 9 9 3 0.31 0.25 0.72 o 10 9 3 8.62 6.47 0.86 o 11 9 3 1.56 4.25 3.03 o 1 10 3 70.21 67.79 1.05 o 2 10 3 34.59 37.67 0.91 o 3 10 3 96.13 99.62 1.81 o 4 10 3 252.02 249.84 4.32 o 5 10 3 106.87 99.97 1.82 o 6 10 3 9.41 8.80 0.59 o 7 10 3 0.05 0.88 0.44 o 8 10 3 129.58 121.07 3.23 o 9 10 3 12.66 11.15 0.78 o 10 10 3 44.23 47.03 1.90 o 0 11 3 984.00 920.80 18.62 o 1 11 3 431.51 421.41 6.14 o 2 11 3 100.46 90.09 1.67 o 3 11 3 0.05 0.01 0.43 o 4 11 3 52.56 51.39 1.28 o 5 11 3 44.63 44.37 1.17 o 6 11 3 87.71 82.06 1.64 o 7 11 3 1159.24 1227.34 17.45 o 8 11 3 191.19 174.26 2.88 o 9 11 3 101.00 98.20 2.43 o 1 12 3 76.34 75.73 1.68 o 2 12 3 11.22 11.16 0.62 o 3 12 3 190.63 197.40 3.02 o 4 12 3 133.03 124.97 2.21 o 5 12 3 90.00 92.54 2.11 o 6 12 3 17.91 17.06 0.83 o 7 12 3 23.16 23.91 0.96 o 8 12 3 75.90 71.78 2.43 o 0 13 3 186.71 185.17 6.98 o 1 13 3 54.51 55.34 2.26 o 2 13 3 8.82 10.84 0.61 o 3 13 3 0.04 -0.22 0.59 o 4 13 3 6.17 6.24 0.67 o 5 13 3 7.24 4.72 0.80 o 6 13 3 78.97 78.24 2.43 o 7 13 3 206.03 219.41 6.26 o 1 14 3 21.06 20.68 1.34 o 2 14 3 141.14 139.37 3.79 o 3 14 3 317.15 321.95 7.76 o 4 14 3 5.85 7.11 1.37 o 5 14 3 107.88 109.67 3.62 o 0 15 3 57.82 57.92 2.42 o 1 15 3 66.82 61.78 1.84 o 2 15 3 11.19 7.99 0.94 o 0 0 4 41.74 45.43 1.27 o 1 0 4 32.22 30.35 0.76 o 2 0 4 574.07 577.67 8.53 o 3 0 4 50.74 49.95 0.99 o 4 0 4 3.95 3.29 0.32 o 5 0 4 0.66 1.77 0.32 o 6 0 4 333.41 350.55 5.11 o 7 0 4 23.41 16.87 0.92 o 8 0 4 128.89 111.92 2.95 o 9 0 4 170.87 143.85 5.17 o 10 0 4 0.42 3.39 1.83 o 11 0 4 0.40 -0.37 0.82 o 12 0 4 49.85 57.68 3.39 o 1 1 4 186.81 190.61 2.16 o 2 1 4 994.43 1001.05 10.76 o 3 1 4 1.01 0.98 0.20 o 4 1 4 374.99 360.38 4.28 o 5 1 4 186.42 176.52 1.92 o 6 1 4 0.30 0.23 0.25 o 7 1 4 0.00 -0.12 0.37 o 8 1 4 1.45 -0.21 0.39 o 9 1 4 215.54 200.38 3.86 o 10 1 4 971.15 931.03 17.06 o 11 1 4 31.30 24.94 1.07 o 12 1 4 9.95 10.43 2.25 o 0 2 4 1572.33 1586.70 25.95 o 1 2 4 121.45 119.35 1.54 o 2 2 4 235.94 236.47 2.67 o 3 2 4 6.82 6.48 0.26 o 4 2 4 308.86 286.91 2.98 o 5 2 4 101.62 88.32 1.08 o 6 2 4 273.54 283.82 3.76 o 7 2 4 20.09 20.19 0.76 o 8 2 4 494.90 495.87 6.78 o 9 2 4 37.08 38.55 1.44 o 10 2 4 1.87 2.79 1.24 o 11 2 4 0.68 0.03 0.64 o 12 2 4 441.14 433.85 12.60 o 1 3 4 5.15 4.45 0.30 o 2 3 4 80.41 83.03 1.20 o 3 3 4 2.83 2.07 0.24 o 4 3 4 289.66 282.75 2.94 o 5 3 4 3.33 2.99 0.26 o 6 3 4 99.26 95.04 1.35 o 7 3 4 19.83 19.04 0.79 o 8 3 4 91.40 94.55 1.91 o 9 3 4 21.77 22.60 1.22 o 10 3 4 118.85 118.00 4.73 o 11 3 4 8.66 8.85 1.07 o 0 4 4 1108.51 1070.23 33.74 o 1 4 4 139.50 135.85 2.44 o 2 4 4 19.18 17.96 0.51 o 3 4 4 48.81 50.19 0.78 o 4 4 4 9.78 8.03 0.35 o 5 4 4 5.43 5.73 0.30 o 6 4 4 303.12 294.99 3.71 o 7 4 4 36.79 35.58 0.85 o 8 4 4 350.01 362.45 5.71 o 9 4 4 49.80 52.03 2.22 o 10 4 4 14.12 17.83 1.33 o 11 4 4 14.83 16.17 1.33 o 1 5 4 208.43 215.87 3.27 o 2 5 4 1946.92 2065.17 29.21 o 3 5 4 415.63 426.63 5.04 o 4 5 4 23.07 23.86 0.54 o 5 5 4 123.98 126.03 1.64 o 6 5 4 182.48 189.20 2.77 o 7 5 4 114.38 111.83 1.87 o 8 5 4 182.19 172.40 3.14 o 9 5 4 0.26 0.67 0.64 o 10 5 4 485.36 508.38 10.46 o 11 5 4 92.48 91.25 3.25 o 0 6 4 359.88 381.98 7.85 o 1 6 4 102.27 107.70 1.54 o 2 6 4 23.97 23.95 0.58 o 3 6 4 244.17 243.14 2.95 o 4 6 4 46.40 44.93 0.79 o 5 6 4 118.46 124.78 2.22 o 6 6 4 453.44 462.90 6.72 o 7 6 4 19.55 19.02 0.98 o 8 6 4 174.50 173.47 2.98 o 9 6 4 98.16 92.84 1.95 o 10 6 4 42.24 43.25 1.47 o 1 7 4 53.72 57.99 0.96 o 2 7 4 424.65 434.90 5.63 o 3 7 4 98.93 98.53 1.51 o 4 7 4 46.74 44.29 0.92 o 5 7 4 22.10 20.66 0.70 o 6 7 4 147.98 152.61 3.60 o 7 7 4 4.77 2.94 0.57 o 8 7 4 79.99 74.67 3.48 o 9 7 4 0.10 0.11 0.71 o 10 7 4 166.39 160.00 7.42 o 0 8 4 1551.93 1586.28 31.82 o 1 8 4 105.09 105.29 1.63 o 2 8 4 49.53 51.88 1.22 o 3 8 4 0.12 -0.20 0.33 o 4 8 4 178.67 170.97 2.26 o 5 8 4 39.26 42.09 1.11 o 6 8 4 168.72 171.02 3.30 o 7 8 4 48.30 48.55 2.08 o 8 8 4 379.15 363.31 6.16 o 9 8 4 18.39 10.87 1.00 o 1 9 4 38.40 38.65 0.81 o 2 9 4 116.76 122.22 1.86 o 3 9 4 0.15 -0.29 0.46 o 4 9 4 253.92 250.19 3.79 o 5 9 4 19.39 19.15 0.98 o 6 9 4 8.04 6.93 0.65 o 7 9 4 7.05 4.99 0.57 o 8 9 4 20.26 20.60 1.10 o 9 9 4 51.20 56.23 3.84 o 0 10 4 14.65 18.87 1.78 o 1 10 4 23.65 24.10 0.97 o 2 10 4 193.42 190.47 3.38 o 3 10 4 2.56 2.85 0.57 o 4 10 4 18.56 18.87 0.93 o 5 10 4 2.77 3.80 0.76 o 6 10 4 104.38 91.44 1.91 o 7 10 4 7.19 6.55 1.14 o 8 10 4 106.03 101.45 2.86 o 1 11 4 73.61 69.62 2.02 o 2 11 4 667.56 670.04 13.59 o 3 11 4 1.43 3.19 0.61 o 4 11 4 155.54 158.71 3.19 o 5 11 4 136.83 143.17 4.57 o 6 11 4 5.70 3.82 0.87 o 7 11 4 5.29 5.38 1.45 o 0 12 4 52.87 66.75 3.59 o 1 12 4 26.35 27.53 1.38 o 2 12 4 174.07 171.75 4.19 o 3 12 4 1.54 1.43 0.79 o 4 12 4 35.95 35.45 2.41 o 5 12 4 14.62 17.71 1.84 o 1 13 4 42.73 34.72 2.74 o 2 13 4 25.50 26.22 1.83 o 3 13 4 8.39 5.29 1.24 o 1 0 5 6.53 8.36 0.71 o 2 0 5 13.42 12.62 0.64 o 3 0 5 69.84 64.08 1.38 o 4 0 5 352.42 370.95 6.23 o 5 0 5 278.19 257.73 4.41 o 6 0 5 43.68 38.85 1.81 o 7 0 5 44.55 35.23 2.55 o 8 0 5 99.10 90.42 4.56 o 9 0 5 33.89 38.62 3.07 o 0 1 5 461.71 495.22 9.71 o 1 1 5 92.48 92.20 1.34 o 2 1 5 232.55 230.69 2.61 o 3 1 5 0.01 -0.27 0.27 o 4 1 5 159.14 149.96 1.91 o 5 1 5 87.60 85.74 1.30 o 6 1 5 144.61 151.94 2.77 o 7 1 5 33.93 31.42 1.95 o 8 1 5 172.20 171.98 3.90 o 9 1 5 0.10 -0.32 1.12 o 1 2 5 74.02 73.00 1.23 o 2 2 5 525.73 529.69 6.50 o 3 2 5 59.01 59.12 0.90 o 4 2 5 237.25 242.89 2.96 o 5 2 5 144.74 142.45 2.11 o 6 2 5 33.84 35.40 0.97 o 7 2 5 47.12 41.65 1.16 o 8 2 5 47.00 43.59 1.69 o 9 2 5 159.92 155.09 7.11 o 0 3 5 97.56 99.88 2.34 o 1 3 5 0.24 0.52 0.33 o 2 3 5 92.50 94.86 1.42 o 3 3 5 40.14 37.10 0.79 o 4 3 5 0.12 0.33 0.34 o 5 3 5 30.97 32.46 0.79 o 6 3 5 241.20 243.31 4.20 o 7 3 5 0.38 0.20 0.51 o 8 3 5 95.99 90.38 2.85 o 9 3 5 0.07 1.24 1.50 o 1 4 5 167.59 174.93 2.51 o 2 4 5 243.11 249.68 3.49 o 3 4 5 199.97 205.57 2.78 o 4 4 5 234.81 234.71 3.29 o 5 4 5 55.68 57.67 1.42 o 6 4 5 37.40 42.88 1.14 o 7 4 5 84.12 82.18 2.58 o 8 4 5 64.35 73.45 3.02 o 9 4 5 0.31 -1.57 1.57 o 0 5 5 1419.38 1472.94 24.11 o 1 5 5 196.04 201.51 2.94 o 2 5 5 6.92 6.72 0.36 o 3 5 5 28.29 28.32 0.68 o 4 5 5 60.94 59.57 1.07 o 5 5 5 65.56 63.40 1.60 o 6 5 5 127.67 125.85 2.58 o 7 5 5 28.94 30.56 1.60 o 8 5 5 319.40 348.09 35.27 o 1 6 5 536.33 544.70 6.68 o 2 6 5 22.41 23.56 0.70 o 3 6 5 196.88 199.18 2.87 o 4 6 5 282.75 287.99 4.89 o 5 6 5 64.29 65.78 1.43 o 6 6 5 38.56 42.04 1.67 o 7 6 5 137.27 134.62 3.57 o 8 6 5 118.10 126.77 5.94 o 0 7 5 443.56 452.46 7.55 o 1 7 5 18.52 19.24 0.59 o 2 7 5 17.36 17.39 0.59 o 3 7 5 0.26 -0.35 0.38 o 4 7 5 4.28 4.27 0.59 o 5 7 5 17.78 16.58 1.24 o 6 7 5 120.22 111.08 3.92 o 7 7 5 3.25 3.39 1.09 o 1 8 5 0.98 0.94 0.54 o 2 8 5 430.80 444.28 7.45 o 3 8 5 148.65 144.86 2.65 o 4 8 5 140.71 145.32 3.13 o 5 8 5 59.86 60.35 2.07 o 6 8 5 23.26 23.76 1.46 o 0 9 5 75.18 81.54 2.38 o 1 9 5 8.11 7.62 0.66 o 2 9 5 94.41 95.73 2.09 o 3 9 5 9.35 8.85 1.14 o 4 9 5 9.92 8.77 0.83 o 5 9 5 29.86 33.34 1.59 o 1 10 5 10.63 8.25 0.89 o 2 10 5 46.15 49.58 1.54 o 3 10 5 18.76 21.66 1.21 o 0 0 6 237.70 250.80 10.38 o 1 0 6 33.76 38.83 1.61 o 2 0 6 0.30 -0.19 0.88 o 3 0 6 47.74 51.44 2.38 o 4 0 6 19.15 19.25 2.15 o 5 0 6 25.84 23.10 1.76 o 1 1 6 71.35 71.89 1.57 o 2 1 6 16.53 16.13 0.91 o 3 1 6 262.68 273.96 8.05 o 4 1 6 38.68 39.15 3.54 o 5 1 6 78.05 78.58 2.56 o 0 2 6 88.75 94.64 2.56 o 1 2 6 199.12 213.81 4.08 o 2 2 6 1.04 -0.04 0.66 o 3 2 6 11.89 11.08 0.84 o 4 2 6 2.27 0.85 0.51 o 1 3 6 1.42 0.68 0.46 o 2 3 6 13.42 12.13 0.82 o 3 3 6 126.84 129.45 3.88 o 4 3 6 213.50 220.34 5.29 o 0 4 6 1.24 1.15 0.66 o 1 4 6 62.32 63.62 1.66 o 2 4 6 123.83 117.35 4.59 o 3 4 6 127.06 131.38 2.76 o 1 5 6 140.48 148.63 2.47 o 2 5 6 15.42 16.09 1.07 o