#------------------------------------------------------------------------------ #$Date: 2020-05-08 11:51:14 +0300 (Fri, 08 May 2020) $ #$Revision: 251911 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/3/50/01/3500109.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500109 _cell_angle_alpha 90.000 _cell_angle_beta 102.193 _cell_angle_gamma 90.000 _cell_length_a 8.8700 _cell_length_b 14.0927 _cell_length_c 14.8515 _exptl_crystal_F_000 626.79 _reflns_d_resolution_high 0.8294 _cod_data_source_file c4ncl.fcf _cod_data_source_block c4ncl _shelx_title ' C4NCl in P21/n #14' _shelx_refln_list_code 4 _shelx_f_calc_maximum 137.80 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5686.92 6211.32 154.66 o 4 0 0 2987.58 3537.07 96.70 o 6 0 0 8.82 9.04 0.60 o 8 0 0 311.30 308.22 10.62 o 10 0 0 94.12 85.18 4.93 o 1 1 0 944.55 936.51 19.32 o 2 1 0 169.39 180.49 3.01 o 3 1 0 710.15 782.61 12.82 o 4 1 0 866.89 842.37 15.70 o 5 1 0 1415.88 1404.66 24.37 o 6 1 0 408.70 387.45 5.94 o 7 1 0 68.78 67.69 1.52 o 8 1 0 21.41 17.42 1.26 o 9 1 0 8.47 10.18 0.71 o 10 1 0 7.28 7.96 0.72 o 1 2 0 8209.00 7424.67 185.34 o 2 2 0 2330.96 2532.27 44.15 o 3 2 0 125.35 142.65 2.65 o 4 2 0 289.90 350.22 6.99 o 5 2 0 5.65 5.16 0.38 o 6 2 0 11.48 16.13 0.61 o 7 2 0 36.46 36.44 1.17 o 8 2 0 33.34 31.14 1.20 o 9 2 0 76.39 79.12 1.91 o 10 2 0 31.59 33.20 2.13 o 1 3 0 608.95 543.29 16.92 o 2 3 0 2144.80 2270.83 43.51 o 3 3 0 507.72 522.86 9.69 o 4 3 0 145.39 145.16 2.87 o 5 3 0 1201.27 1082.29 18.64 o 6 3 0 13.58 13.91 0.56 o 7 3 0 944.12 871.38 13.47 o 8 3 0 141.58 142.47 3.07 o 9 3 0 0.17 0.15 0.45 o 10 3 0 33.55 32.25 1.87 o 1 4 0 44.29 59.79 2.98 o 2 4 0 6949.60 7066.04 141.67 o 3 4 0 4.74 2.59 0.30 o 4 4 0 167.60 144.51 2.61 o 5 4 0 1428.83 1398.33 19.00 o 6 4 0 106.27 102.31 1.69 o 7 4 0 34.76 36.84 1.08 o 8 4 0 37.74 41.27 1.39 o 9 4 0 192.48 211.69 4.44 o 10 4 0 35.80 33.22 1.74 o 1 5 0 390.01 419.37 18.80 o 2 5 0 1828.56 1904.18 40.66 o 3 5 0 272.27 320.97 6.30 o 4 5 0 572.07 527.74 9.15 o 5 5 0 0.55 1.36 0.30 o 6 5 0 2.50 3.60 0.39 o 7 5 0 95.79 95.01 3.26 o 8 5 0 137.40 139.34 3.16 o 9 5 0 43.18 45.76 1.35 o 0 6 0 772.64 706.01 43.71 o 1 6 0 974.31 1036.71 45.86 o 2 6 0 3702.33 4059.50 86.21 o 3 6 0 383.61 423.86 7.57 o 4 6 0 657.64 605.47 6.90 o 5 6 0 103.56 83.29 1.34 o 6 6 0 1570.36 1460.78 20.23 o 7 6 0 57.33 49.28 1.58 o 8 6 0 87.89 94.38 2.49 o 9 6 0 0.09 0.89 0.52 o 1 7 0 151.94 163.52 6.36 o 2 7 0 4536.07 4531.59 53.60 o 3 7 0 119.68 112.83 1.33 o 4 7 0 702.64 688.80 7.70 o 5 7 0 1146.28 1071.97 13.41 o 6 7 0 8.33 11.72 0.60 o 7 7 0 171.93 171.52 3.75 o 8 7 0 84.22 88.90 2.54 o 9 7 0 4.80 5.75 0.72 o 0 8 0 42.54 65.08 1.01 o 1 8 0 28.44 18.13 0.33 o 2 8 0 0.89 1.15 0.18 o 3 8 0 566.83 509.90 5.14 o 4 8 0 23.60 17.61 0.51 o 5 8 0 115.23 106.01 1.65 o 6 8 0 87.45 92.93 2.07 o 7 8 0 9.37 8.43 0.72 o 8 8 0 19.62 20.96 1.12 o 9 8 0 155.19 151.61 4.18 o 1 9 0 188.33 201.77 1.83 o 2 9 0 207.00 213.83 2.06 o 3 9 0 353.81 369.40 3.81 o 4 9 0 4.57 3.42 0.33 o 5 9 0 410.61 400.97 5.18 o 6 9 0 11.16 8.29 0.64 o 7 9 0 71.91 83.09 2.21 o 8 9 0 96.34 100.01 2.68 o 0 10 0 1377.20 1468.04 16.67 o 1 10 0 245.98 273.44 2.52 o 2 10 0 628.80 675.49 6.10 o 3 10 0 484.94 516.04 5.43 o 4 10 0 2.41 6.21 0.42 o 5 10 0 6.86 6.34 0.52 o 6 10 0 147.98 137.12 2.81 o 7 10 0 49.43 51.32 1.72 o 8 10 0 88.71 99.76 2.86 o 1 11 0 2.03 3.43 0.28 o 2 11 0 1256.43 1322.92 12.26 o 3 11 0 3.72 7.61 0.43 o 4 11 0 395.94 457.70 6.55 o 5 11 0 128.60 131.02 2.41 o 6 11 0 293.42 287.62 5.30 o 7 11 0 3.97 2.49 0.52 o 0 12 0 2015.33 2278.61 31.20 o 1 12 0 3.46 2.55 0.31 o 2 12 0 166.83 170.54 1.99 o 3 12 0 70.89 75.15 1.38 o 4 12 0 21.83 24.82 0.85 o 5 12 0 22.82 22.10 0.85 o 6 12 0 17.63 18.68 0.83 o 7 12 0 60.62 56.85 2.14 o 1 13 0 90.85 101.13 1.38 o 2 13 0 9.94 13.99 0.49 o 3 13 0 47.15 46.29 1.13 o 4 13 0 314.35 332.41 5.35 o 5 13 0 11.00 9.21 0.64 o 6 13 0 13.20 12.47 0.68 o 0 14 0 6.45 8.94 0.95 o 1 14 0 8.89 11.15 0.55 o 2 14 0 3.98 4.78 0.53 o 3 14 0 167.99 169.90 3.04 o 4 14 0 1.66 3.62 0.47 o 5 14 0 60.46 64.67 1.81 o 1 15 0 77.01 83.29 1.87 o 2 15 0 11.98 18.08 1.01 o 3 15 0 19.17 20.30 1.10 o 4 15 0 42.15 42.53 2.08 o 0 16 0 512.42 491.10 18.82 o 1 16 0 155.17 162.50 4.81 o 2 16 0 300.07 283.67 7.10 o 3 16 0 5.24 5.35 1.26 o -9 0 1 43.06 33.65 1.60 o -7 0 1 147.65 137.35 3.56 o -5 0 1 110.60 112.98 4.44 o -3 0 1 576.29 618.12 17.11 o -1 0 1 11750.65 11357.97 283.76 o 1 0 1 823.49 883.37 22.28 o 3 0 1 1710.77 1867.68 43.24 o 5 0 1 17.85 14.97 0.84 o 7 0 1 1462.13 1416.93 29.01 o 9 0 1 191.30 197.67 5.61 o -10 1 1 1.56 4.93 0.52 o -9 1 1 109.97 120.25 2.63 o -8 1 1 261.25 266.53 6.60 o -7 1 1 184.05 163.77 2.65 o -6 1 1 0.78 0.40 0.31 o -5 1 1 552.61 556.94 10.46 o -4 1 1 1.30 0.33 0.26 o -3 1 1 380.95 478.98 9.43 o -2 1 1 1620.84 1662.70 29.43 o -1 1 1 1.32 -0.13 0.13 o 0 1 1 1227.96 1232.02 27.14 o 1 1 1 1093.40 1010.03 18.62 o 2 1 1 18988.81 19789.85 309.50 o 3 1 1 272.31 255.88 4.68 o 4 1 1 1027.73 1045.33 18.56 o 5 1 1 547.37 525.48 8.50 o 6 1 1 0.21 0.36 0.32 o 7 1 1 18.49 17.85 0.70 o 8 1 1 2.67 1.63 0.63 o 9 1 1 37.70 38.92 1.21 o 10 1 1 3.16 2.20 0.40 o -10 2 1 29.68 26.28 0.94 o -9 2 1 30.44 24.75 1.00 o -8 2 1 147.33 152.11 3.26 o -7 2 1 119.15 106.37 1.93 o -6 2 1 51.28 47.80 1.11 o -5 2 1 204.07 241.27 4.60 o -4 2 1 2113.31 2253.82 41.66 o -3 2 1 872.99 950.45 16.05 o -2 2 1 9204.74 9545.65 173.78 o -1 2 1 1826.96 1858.98 39.58 o 0 2 1 2440.43 2188.56 58.29 o 1 2 1 2204.63 2162.12 46.72 o 2 2 1 2436.05 2586.51 50.10 o 3 2 1 851.33 920.19 15.01 o 4 2 1 537.70 631.88 10.76 o 5 2 1 41.82 52.49 1.19 o 6 2 1 1138.65 1093.15 18.10 o 7 2 1 1.17 0.69 0.37 o 8 2 1 184.56 197.45 4.03 o 9 2 1 22.50 23.87 1.03 o 10 2 1 11.41 11.89 0.88 o -10 3 1 2.62 1.86 0.46 o -9 3 1 0.16 0.78 0.46 o -8 3 1 454.26 472.41 8.91 o -7 3 1 5.49 4.09 0.46 o -6 3 1 453.93 414.43 6.33 o -5 3 1 223.94 222.77 5.17 o -4 3 1 5.84 2.34 0.36 o -3 3 1 67.41 68.75 1.52 o -2 3 1 0.21 -0.22 0.22 o -1 3 1 9322.58 9026.61 220.70 o 0 3 1 4996.71 5355.95 327.15 o 1 3 1 889.72 882.34 24.19 o 2 3 1 5873.57 6296.70 136.02 o 3 3 1 132.33 136.30 2.82 o 4 3 1 1950.05 1983.46 34.67 o 5 3 1 127.35 129.87 2.24 o 6 3 1 59.34 60.78 1.32 o 7 3 1 38.06 30.67 0.85 o 8 3 1 7.49 11.13 0.71 o 9 3 1 2.77 5.53 0.62 o 10 3 1 22.95 23.46 1.21 o -10 4 1 202.94 209.98 4.90 o -9 4 1 188.25 196.63 4.16 o -8 4 1 39.17 47.54 1.45 o -7 4 1 390.13 354.17 6.94 o -6 4 1 526.16 511.02 7.29 o -5 4 1 146.53 125.52 1.88 o -4 4 1 1449.84 1537.03 29.54 o -3 4 1 1145.35 1122.27 22.68 o -2 4 1 1190.08 1144.59 24.45 o -1 4 1 291.34 293.44 7.98 o 0 4 1 6025.49 6197.62 378.21 o 1 4 1 2.97 5.18 0.53 o 2 4 1 2457.20 2728.94 74.64 o 3 4 1 62.48 63.18 1.53 o 4 4 1 1547.12 1506.73 25.59 o 5 4 1 406.52 418.43 5.68 o 6 4 1 39.30 35.17 0.95 o 7 4 1 213.98 193.77 3.08 o 8 4 1 154.72 162.51 4.16 o 9 4 1 86.91 86.06 2.29 o 10 4 1 43.17 37.06 1.48 o -10 5 1 144.57 150.43 9.37 o -9 5 1 310.20 328.43 6.25 o -8 5 1 77.84 71.64 1.93 o -7 5 1 233.79 220.40 6.08 o -6 5 1 62.01 59.74 1.21 o -5 5 1 170.12 172.27 2.50 o -4 5 1 525.19 485.38 7.34 o -3 5 1 115.52 122.89 2.88 o -2 5 1 849.59 903.51 20.69 o -1 5 1 152.80 147.96 4.18 o 0 5 1 65.02 64.33 3.13 o 1 5 1 1855.01 1983.55 71.21 o 2 5 1 1931.93 2222.09 60.87 o 3 5 1 293.50 259.62 5.17 o 4 5 1 4.57 1.67 0.24 o 5 5 1 13.02 22.00 0.61 o 6 5 1 825.62 737.57 10.34 o 7 5 1 72.91 71.25 1.90 o 8 5 1 100.63 94.20 2.14 o 9 5 1 8.22 10.49 0.76 o -9 6 1 1.25 1.08 0.46 o -8 6 1 60.64 65.61 2.08 o -7 6 1 94.17 97.64 3.87 o -6 6 1 74.57 66.26 1.67 o -5 6 1 159.41 145.40 2.23 o -4 6 1 374.60 332.22 3.89 o -3 6 1 1823.33 1747.27 30.94 o -2 6 1 225.80 267.70 6.83 o -1 6 1 32.58 19.53 0.96 o 0 6 1 69.60 69.33 2.46 o 1 6 1 1203.54 1172.46 36.94 o 2 6 1 242.45 268.36 7.75 o 3 6 1 361.75 336.94 5.59 o 4 6 1 68.65 67.34 1.05 o 5 6 1 93.20 87.04 1.43 o 6 6 1 214.20 203.04 3.30 o 7 6 1 130.83 125.14 2.87 o 8 6 1 35.18 40.77 1.52 o 9 6 1 15.21 20.20 0.92 o -9 7 1 2.93 2.71 0.49 o -8 7 1 2.43 2.65 0.60 o -7 7 1 292.26 312.47 6.85 o -6 7 1 1340.79 1242.94 21.61 o -5 7 1 355.95 342.49 4.46 o -4 7 1 46.16 52.35 0.84 o -3 7 1 233.22 211.26 2.27 o -2 7 1 648.42 690.82 9.05 o -1 7 1 678.39 743.05 22.65 o 0 7 1 125.96 125.39 4.95 o 1 7 1 3131.49 3292.72 118.19 o 2 7 1 1830.34 1775.88 18.65 o 3 7 1 929.59 917.79 9.47 o 4 7 1 349.29 362.20 4.34 o 5 7 1 39.25 37.10 1.08 o 6 7 1 116.60 108.80 2.38 o 7 7 1 56.96 57.08 1.68 o 8 7 1 65.00 61.92 2.20 o 9 7 1 88.58 90.24 2.90 o -9 8 1 2.82 4.87 0.57 o -8 8 1 21.81 25.21 1.26 o -7 8 1 21.56 20.09 1.09 o -6 8 1 1093.78 1100.09 18.92 o -5 8 1 169.06 157.37 2.35 o -4 8 1 205.13 187.30 2.30 o -3 8 1 158.90 159.89 1.75 o -2 8 1 531.08 453.01 4.13 o -1 8 1 14.86 10.03 0.25 o 0 8 1 1977.85 2004.30 16.35 o 1 8 1 422.90 417.88 3.71 o 2 8 1 55.04 57.67 0.70 o 3 8 1 3.65 4.20 0.27 o 4 8 1 1565.86 1525.49 17.14 o 5 8 1 1.47 0.40 0.34 o 6 8 1 47.19 49.66 1.45 o 7 8 1 3.47 2.51 0.58 o 8 8 1 112.17 110.28 3.23 o 9 8 1 47.94 52.95 2.53 o -8 9 1 76.03 74.33 2.19 o -7 9 1 14.90 17.54 1.03 o -6 9 1 83.64 94.33 2.12 o -5 9 1 59.78 64.29 1.22 o -4 9 1 278.24 270.83 3.29 o -3 9 1 41.37 47.83 0.77 o -2 9 1 1.55 1.32 0.21 o -1 9 1 45.76 44.08 0.60 o 0 9 1 34.56 24.56 0.41 o 1 9 1 370.53 431.57 3.86 o 2 9 1 104.21 86.53 0.97 o 3 9 1 1.47 4.07 0.30 o 4 9 1 1067.18 997.65 11.27 o 5 9 1 45.96 39.71 0.91 o 6 9 1 54.59 60.23 1.58 o 7 9 1 1.09 -0.40 0.51 o 8 9 1 0.31 -0.57 0.57 o -8 10 1 7.37 7.64 0.74 o -7 10 1 27.53 26.49 1.17 o -6 10 1 0.16 0.42 0.46 o -5 10 1 47.33 38.77 1.04 o -4 10 1 275.61 279.00 3.46 o -3 10 1 12.79 15.58 0.47 o -2 10 1 252.13 273.72 2.59 o -1 10 1 862.50 921.29 7.82 o 0 10 1 508.65 520.20 4.35 o 1 10 1 443.50 452.01 3.96 o 2 10 1 150.07 162.74 1.71 o 3 10 1 84.06 82.25 1.18 o 4 10 1 247.36 242.96 3.05 o 5 10 1 16.11 11.82 0.64 o 6 10 1 395.67 412.87 7.45 o 7 10 1 34.57 37.29 1.69 o 8 10 1 62.94 59.29 1.95 o -8 11 1 12.41 10.65 0.95 o -7 11 1 73.31 72.02 2.13 o -6 11 1 44.36 41.80 1.35 o -5 11 1 504.39 559.89 8.43 o -4 11 1 140.26 142.74 2.35 o -3 11 1 25.56 30.31 0.71 o -2 11 1 1.85 4.03 0.31 o -1 11 1 107.39 135.71 1.47 o 0 11 1 106.45 120.89 1.23 o 1 11 1 515.91 586.54 5.47 o 2 11 1 139.56 149.41 1.65 o 3 11 1 445.07 484.63 5.73 o 4 11 1 28.71 36.60 0.99 o 5 11 1 516.53 547.37 8.92 o 6 11 1 18.48 15.83 0.86 o 7 11 1 13.99 14.57 0.87 o -7 12 1 1.73 2.73 0.51 o -6 12 1 32.07 28.90 1.04 o -5 12 1 91.27 92.10 1.96 o -4 12 1 130.82 121.32 2.20 o -3 12 1 198.53 203.41 2.90 o -2 12 1 4.65 10.55 0.45 o -1 12 1 531.74 606.03 5.74 o 0 12 1 1.39 1.02 0.29 o 1 12 1 119.30 137.96 1.66 o 2 12 1 7.03 9.27 0.42 o 3 12 1 57.16 71.13 1.36 o 4 12 1 55.09 69.36 1.43 o 5 12 1 9.16 11.60 0.65 o 6 12 1 160.30 165.62 3.88 o 7 12 1 61.82 59.26 2.16 o -6 13 1 3.38 3.01 0.49 o -5 13 1 105.25 106.53 2.24 o -4 13 1 162.46 158.16 2.76 o -3 13 1 161.62 149.42 2.36 o -2 13 1 6.30 8.61 0.46 o -1 13 1 322.03 358.16 4.25 o 0 13 1 606.50 641.73 7.36 o 1 13 1 142.78 151.84 1.85 o 2 13 1 263.13 256.27 3.15 o 3 13 1 190.22 224.92 3.54 o 4 13 1 46.80 50.38 1.32 o 5 13 1 41.39 40.59 1.21 o 6 13 1 27.65 26.67 1.39 o -6 14 1 71.87 70.52 2.83 o -5 14 1 7.16 6.73 0.60 o -4 14 1 339.14 328.39 5.64 o -3 14 1 88.25 84.17 1.70 o -2 14 1 618.03 705.12 9.78 o -1 14 1 12.30 9.33 0.52 o 0 14 1 9.88 9.48 0.53 o 1 14 1 149.40 149.74 2.21 o 2 14 1 76.36 84.58 1.69 o 3 14 1 0.22 1.82 0.55 o 4 14 1 4.85 5.37 0.53 o 5 14 1 9.74 13.36 0.78 o -4 15 1 0.76 1.01 0.75 o -3 15 1 19.26 20.99 1.36 o -2 15 1 0.70 1.25 0.54 o -1 15 1 13.00 16.88 0.81 o 0 15 1 188.31 197.61 3.30 o 1 15 1 7.02 4.47 0.61 o 2 15 1 318.13 312.96 7.23 o 3 15 1 1.11 0.44 1.12 o 4 15 1 23.30 23.27 2.22 o -3 16 1 249.30 229.72 6.84 o -2 16 1 137.34 123.72 3.37 o -1 16 1 72.53 76.96 3.04 o 0 16 1 165.08 159.14 5.50 o 1 16 1 11.58 12.20 0.87 o 2 16 1 28.84 26.78 1.35 o 3 16 1 3.94 3.62 0.75 o -10 0 2 98.84 96.98 3.62 o -8 0 2 95.21 89.42 3.27 o -6 0 2 929.89 983.35 19.32 o -4 0 2 2641.55 2812.71 65.32 o -2 0 2 3851.16 3837.93 83.74 o 0 0 2 3104.13 2981.56 70.17 o 2 0 2 3225.49 3394.27 84.96 o 4 0 2 11081.73 12118.01 279.06 o 6 0 2 454.36 428.55 9.41 o 8 0 2 222.65 192.56 7.48 o 10 0 2 10.00 11.31 0.95 o -10 1 2 4.70 3.72 0.50 o -9 1 2 604.75 650.31 11.38 o -8 1 2 138.22 129.27 2.69 o -7 1 2 93.34 92.65 2.30 o -6 1 2 74.77 62.87 1.40 o -5 1 2 79.15 82.36 1.62 o -4 1 2 233.28 259.16 4.59 o -3 1 2 47.53 45.99 0.96 o -2 1 2 1929.61 2053.31 36.65 o -1 1 2 2612.37 2725.94 53.73 o 0 1 2 476.11 387.41 7.70 o 1 1 2 1037.69 1124.91 20.04 o 2 1 2 1160.34 1249.11 23.14 o 3 1 2 599.23 734.43 13.13 o 4 1 2 4297.07 4776.48 84.34 o 5 1 2 209.42 230.74 3.88 o 6 1 2 77.45 92.73 1.69 o 7 1 2 0.89 1.11 0.43 o 8 1 2 198.01 218.86 6.98 o 9 1 2 61.81 62.45 1.94 o 10 1 2 99.05 98.64 2.44 o -10 2 2 16.69 18.58 0.81 o -9 2 2 32.41 34.68 1.27 o -8 2 2 1.15 2.24 0.46 o -7 2 2 302.61 302.49 4.67 o -6 2 2 4.69 4.81 0.41 o -5 2 2 276.52 259.13 4.55 o -4 2 2 522.53 538.55 9.78 o -3 2 2 491.37 496.95 9.41 o -2 2 2 3836.95 4084.79 76.13 o -1 2 2 100.50 109.15 2.35 o 0 2 2 2212.40 2306.23 50.83 o 1 2 2 2489.98 2499.03 53.92 o 2 2 2 160.43 140.49 2.72 o 3 2 2 1993.67 2283.22 38.38 o 4 2 2 213.24 180.53 3.54 o 5 2 2 359.34 310.11 5.56 o 6 2 2 607.09 605.74 10.09 o 7 2 2 53.96 59.46 1.26 o 8 2 2 5.40 6.02 0.53 o 9 2 2 22.22 26.83 1.24 o 10 2 2 3.79 3.36 0.42 o -10 3 2 1.79 1.65 0.48 o -9 3 2 231.18 224.42 5.87 o -8 3 2 396.46 387.44 9.44 o -7 3 2 968.98 926.20 14.71 o -6 3 2 246.41 238.43 3.76 o -5 3 2 216.38 204.66 3.81 o -4 3 2 91.13 112.16 2.35 o -3 3 2 839.91 851.03 15.97 o -2 3 2 1.39 1.89 0.22 o -1 3 2 10343.73 10576.25 214.29 o 0 3 2 1294.64 1328.17 41.32 o 1 3 2 5648.22 5924.13 136.96 o 2 3 2 685.97 765.48 15.71 o 3 3 2 36.22 24.56 0.72 o 4 3 2 79.94 70.29 1.37 o 5 3 2 175.51 186.66 2.99 o 6 3 2 1309.24 1238.51 19.96 o 7 3 2 136.14 122.49 2.34 o 8 3 2 25.88 19.34 0.86 o 9 3 2 12.90 12.69 0.86 o -10 4 2 52.72 51.19 1.57 o -9 4 2 5.74 7.46 0.68 o -8 4 2 94.50 90.95 2.17 o -7 4 2 11.80 11.35 0.62 o -6 4 2 1218.20 1160.19 16.66 o -5 4 2 1110.47 996.02 13.80 o -4 4 2 304.13 289.65 6.23 o -3 4 2 1398.70 1420.38 28.88 o -2 4 2 69.57 90.83 2.12 o -1 4 2 521.73 523.55 12.14 o 0 4 2 1.43 1.61 0.27 o 1 4 2 3.59 7.79 0.45 o 2 4 2 257.00 291.56 6.49 o 3 4 2 2743.03 2989.87 64.71 o 4 4 2 2031.82 2015.93 28.27 o 5 4 2 2.29 2.88 0.30 o 6 4 2 979.85 932.55 14.38 o 7 4 2 2.04 1.92 0.47 o 8 4 2 18.35 16.65 0.85 o 9 4 2 40.54 45.60 1.75 o -10 5 2 27.56 28.95 1.11 o -9 5 2 0.45 -0.07 0.53 o -8 5 2 71.90 70.67 2.04 o -7 5 2 43.07 43.78 1.21 o -6 5 2 270.00 250.14 3.75 o -5 5 2 50.56 49.74 0.98 o -4 5 2 97.35 79.14 2.00 o -3 5 2 865.38 874.24 17.91 o -2 5 2 4.53 3.83 0.45 o 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