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Information card for entry 4023967
Preview
| Coordinates | 4023967.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | Fraenkel 1469 |
|---|---|
| Formula | C32 H58 Li2 N2 |
| Calculated formula | C32 H58 Li2 N2 |
| Title of publication | Structural Distortions and Dynamic Behavior of the Elusive "L"-Shaped cis-Bicyclo[3.3.0]octenyllithium: X-ray Crystallographic and NMR Studies |
| Authors of publication | Gideon Fraenkel; Xiao Chen; Judith Gallucci; Yan Lu |
| Journal of publication | Journal of Organic Chemistry |
| Year of publication | 2007 |
| Journal volume | 72 |
| Pages of publication | 4961 - 4965 |
| a | 11.3719 ± 0.001 Å |
| b | 17.364 ± 0.002 Å |
| c | 16.532 ± 0.003 Å |
| α | 90° |
| β | 99.11 ± 0.005° |
| γ | 90° |
| Cell volume | 3223.4 ± 0.7 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 9 |
| Hermann-Mauguin space group symbol | C 1 c 1 |
| Hall space group symbol | C -2yc |
| Residual factor for all reflections | 0.0635 |
| Residual factor for significantly intense reflections | 0.0544 |
| Weighted residual factors for significantly intense reflections | 0.1396 |
| Weighted residual factors for all reflections included in the refinement | 0.1471 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.051 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178418 (current) | 2016-03-21 | cif/4/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/02/39. |
4023967.cif |
| 120074 | 2014-07-11 | Adding DOIs to range 4/02 structures. | 4023967.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4023967.cif |
| 966 | 2010-01-30 | cif/ Adding _cod_database_code tags to all COD entries. Adding tag description to the cif_cod.dic dictionary so that COD entries can be validated. |
4023967.cif |
| 823 | 2009-09-25 | cif/ Depositing information from the Chem-Comm-2003_01-17 and J-Org-Chem-2007_13-20 publications. |
4023967.cif |
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Users of the data should acknowledge the original authors of the
structural data.