Crystallography Open Database

Information card for entry 4024471

Preview

Coordinates	4024471.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H41 N O4 Si
Calculated formula	C22 H41 N O4 Si
Title of publication	Diastereoselectivity Control of the Radical Carboazidation of Substituted Methylenecyclohexanes
Authors of publication	Sylvaine Cren; Pascal Schär; Philippe Renaud; Kurt Schenk
Journal of publication	Journal of Organic Chemistry
Year of publication	2009
Journal volume	74
Pages of publication	2942 - 2946
a	26.787 ± 0.003 Å
b	6.7761 ± 0.0004 Å
c	29.664 ± 0.003 Å
α	90°
β	108.47 ± 0.008°
γ	90°
Cell volume	5107 ± 0.9 Å³
Cell temperature	292 ± 2 K
Ambient diffraction temperature	292 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0839
Residual factor for significantly intense reflections	0.0602
Weighted residual factors for significantly intense reflections	0.1598
Weighted residual factors for all reflections included in the refinement	0.1753
Goodness-of-fit parameter for all reflections included in the refinement	1.065
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178423 (current)	2016-03-21	cif/4/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/02/44.	4024471.cif
120074	2014-07-11	Adding DOIs to range 4/02 structures.	4024471.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4024471.cif
966	2010-01-30	cif/ Adding _cod_database_code tags to all COD entries. Adding tag description to the cif_cod.dic dictionary so that COD entries can be validated.	4024471.cif
948	2010-01-19	cif/ Adding CIFs for the Acta-Cryst-B-2009_06/ Acta-Cryst-C-2009_12/ Acta-Cryst-E-2009_12/ J-Appl-Cryst-2009_06/ J-Org-Chem-2009/ deposition.	4024471.cif