#------------------------------------------------------------------------------ #$Date: 2015-06-05 08:39:45 +0300 (Fri, 05 Jun 2015) $ #$Revision: 138287 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/03/03/4030304.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4030304 loop_ _publ_author_name 'Han, Seo-Jung' 'Vogt, Florian' 'May, Jeremy A.' 'Krishnan, Shyam' 'Gatti, Michele' 'Virgil, Scott C.' 'Stoltz, Brian M.' _publ_section_title ; Evolution of a Unified, Stereodivergent Approach to the Synthesis of Communesin F and Perophoramidine. ; _journal_issue 1 _journal_name_full 'The Journal of organic chemistry' _journal_page_first 528 _journal_paper_doi 10.1021/jo502534g _journal_volume 80 _journal_year 2014 _chemical_formula_moiety '2(C23 H23 Br N3 O4), 0.81(C H2 Cl2), 0.19(H2 O)' _chemical_formula_sum 'C46.4 H47.2 Br2 Cl0.8 N6 O8.2' _chemical_formula_weight 1008.40 _chemical_name_systematic ; ? ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2012-10-29 _audit_creation_method ; Olex2 1.2 (compiled Oct 26 2012 17:09:49, GUI svn.r4371) SHELXL-2012, and manual edit ; _cell_angle_alpha 90 _cell_angle_beta 96.873(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 17.6618(8) _cell_length_b 17.4368(7) _cell_length_c 13.5068(5) _cell_measurement_reflns_used 9880 _cell_measurement_temperature 100 _cell_measurement_theta_max 33.69 _cell_measurement_theta_min 2.32 _cell_volume 4129.7(3) _computing_cell_refinement 'SAINT V8.27B (Bruker-AXS, 2007)' _computing_data_collection 'APEX2 2012.4-3 (Bruker-AXS, 2007)' _computing_data_reduction 'SAINT V8.27B (Bruker-AXS, 2007)' _computing_molecular_graphics 'DIAMOND 3 (Crystal Impact, 1999)' _computing_publication_material ; O. V. Dolomanov, L. J. Bourhis, R. J. Gildea, J. A. K. Howard and H. Puschmann, OLEX2: a complete structure solution, refinement and analysis program. J. Appl. Cryst. (2009). 42, 339-341. and SHELXTL (Bruker-AXS, 2007) ; _computing_structure_refinement 'SHELXL-2012/6 (Sheldrick, 2012)' _computing_structure_solution 'SHELXT (Sheldrick, 2012)' _diffrn_ambient_temperature 100 _diffrn_detector_area_resol_mean 8.33 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.963 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0668 _diffrn_reflns_av_unetI/netI 0.0422 _diffrn_reflns_laue_measured_fraction_full 0.999 _diffrn_reflns_laue_measured_fraction_max 0.963 _diffrn_reflns_limit_h_max 30 _diffrn_reflns_limit_h_min -29 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_k_min -29 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 213592 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.963 _diffrn_reflns_theta_full 25.000 _diffrn_reflns_theta_max 37.587 _diffrn_reflns_theta_min 2.144 _diffrn_source_current 30.0 _diffrn_source_power 1.5 _diffrn_source_target Mo _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 2.082 _exptl_absorpt_correction_T_max 1.0000 _exptl_absorpt_correction_T_min 0.8480 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2012/1 (Bruker,2012) was used for absorption correction. wR2(int) was 0.0662 before and 0.0506 after correction. The Ratio of minimum to maximum transmission is 0.8480. The \l/2 correction factor is 0.0015. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.622 _exptl_crystal_description plate _exptl_crystal_F_000 2067 _exptl_crystal_size_max 0.46 _exptl_crystal_size_mid 0.20 _exptl_crystal_size_min 0.05 _refine_diff_density_max 3.944 _refine_diff_density_min -2.054 _refine_diff_density_rms 0.127 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 3.308 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 592 _refine_ls_number_reflns 21060 _refine_ls_number_restraints 3 _refine_ls_restrained_S_all 3.309 _refine_ls_R_factor_all 0.0953 _refine_ls_R_factor_gt 0.0585 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details ; w=1/[\s^2^(Fo^2^)] ; _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0955 _refine_ls_wR_factor_ref 0.0967 _reflns_Friedel_coverage 0.000 _reflns_number_gt 14742 _reflns_number_total 21060 _reflns_threshold_expression 'I > 2\s(I)' _[local]_cod_data_source_file jo502534g_si_013.cif _[local]_cod_data_source_block sjh01 _[local]_cod_chemical_formula_sum_orig 'C46.40 H47.20 Br2 Cl0.80 N6 O8.20' _cod_depositor_comments ; The following automatic conversions were performed: '_diffrn_source_target' value 'MO' changed to 'Mo' according to /home/saulius/struct/COD-crude-data--automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26. Automatic conversion script Id: cif_fix_values 2935 2014-11-11 08:27:57Z andrius Adding full bibliography for 4030304--4030313.cif. ; _cod_database_code 4030304 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: H4A of C4A, H3A of C3A, H2A of C2A, {H3AA,H3AB} of N3A, {H10A,H10B} of C10A, {H11A,H11B} of C11A, {H14A,H14B} of C14A, {H15A,H15B} of C15A, H18A of C18A, H19A of C19A, H20A of C20A, H21A of C21A, {H3BA,H3BB} of N3B, H2B of C2B, H3B of C3B, H4B of C4B, {H10C,H10D} of C10B, {H11C,H11D} of C11B, {H14C,H14D} of C14B, {H15C,H15D} of C15B, H18B of C18B, H19B of C19B, H20B of C20B, H21B of C21B, {H1A,H1B} of C1 At 1.5 times of: {H9AA,H9AB,H9AC} of C9A, {H23A,H23B,H23C} of C23A, {H9BA,H9BB,H9BC} of C9B, {H23D,H23E,H23F} of C23B, {H1C,H1D} of O1 2. Restrained distances O1-H1C 0.84 with sigma of 0.01 O1-H1D 0.84 with sigma of 0.01 H1C-H1D 1.34 with sigma of 0.02 3. Others Sof(Cl1)=Sof(C1)=Sof(H1A)=Sof(H1B)=1-Sof(C1)=1-Sof(C1)=1-Sof(C1) 4.a Secondary CH2 refined with riding coordinates: N3A(H3AA,H3AB), C10A(H10A,H10B), C11A(H11A,H11B), C14A(H14A,H14B), C15A(H15A, H15B), N3B(H3BA,H3BB), C10B(H10C,H10D), C11B(H11C,H11D), C14B(H14C,H14D), C15B(H15C,H15D), C1(H1A,H1B) 4.b Aromatic/amide H refined with riding coordinates: C2A(H2A), C3A(H3A), C4A(H4A), C18A(H18A), C19A(H19A), C20A(H20A), C21A(H21A), C2B(H2B), C3B(H3B), C4B(H4B), C18B(H18B), C19B(H19B), C20B(H20B), C21B(H21B) 4.c Idealised Me refined as rotating group: C9A(H9AA,H9AB,H9AC), C23A(H23A,H23B,H23C), C9B(H9BA,H9BB,H9BC), C23B(H23D, H23E,H23F) ; _shelx_estimated_absorpt_t_max 0.903 _shelx_estimated_absorpt_t_min 0.448 _shelx_hkl_checksum 84687 _shelx_hkl_file ; 2 0 0 25.02 0.92 2 0 0 25.39 0.99 -2 0 0 26.78 0.99 -2 0 0 23.41 1.01 -3 0 0 34.01 1.19 3 0 0 33.64 1.22 3 0 0 33.07 1.31 -3 0 0 36.83 1.31 -3 0 0 30.70 1.34 3 0 0 33.36 1.20 -3 0 0 33.49 1.18 4 0 0 266.30 9.99 4 0 0 262.58 9.30 -4 0 0 252.20 9.03 4 0 0 263.23 9.20 -4 0 0 238.14 10.20 -4 0 0 286.37 10.00 -4 0 0 256.45 9.06 5 0 0 46.15 1.77 -5 0 0 40.95 1.80 5 0 0 46.50 1.64 5 0 0 43.95 1.62 -5 0 0 44.82 1.60 -5 0 0 43.24 1.59 -5 0 0 49.49 1.77 6 0 0 16.02 0.69 -6 0 0 16.48 0.62 -6 0 0 15.03 0.70 6 0 0 15.54 0.63 6 0 0 16.08 0.62 -6 0 0 19.07 0.70 -6 0 0 15.98 0.61 -7 0 0 0.29 0.14 7 0 0 0.39 0.13 -7 0 0 0.34 0.13 7 0 0 0.40 0.11 -7 0 0 0.19 0.09 7 0 0 0.12 0.11 8 0 0 43.79 1.61 -8 0 0 39.21 1.77 8 0 0 42.77 1.59 -8 0 0 43.21 1.56 8 0 0 44.57 1.74 -8 0 0 47.46 1.74 -9 0 0 20.12 0.94 9 0 0 21.66 0.85 -9 0 0 23.15 0.93 9 0 0 23.02 0.93 9 0 0 21.13 0.84 -10 0 0 13.09 0.59 -10 0 0 10.93 0.59 10 0 0 11.74 0.51 10 0 0 12.43 0.58 10 0 0 11.55 0.52 11 0 0 22.88 0.91 -11 0 0 22.89 0.99 11 0 0 22.54 0.89 -11 0 0 21.11 1.01 11 0 0 24.81 1.00 -12 0 0 10.62 0.61 12 0 0 12.44 0.61 12 0 0 11.15 0.54 -12 0 0 11.79 0.61 12 0 0 11.99 0.53 13 0 0 5.83 0.41 13 0 0 4.87 0.36 -13 0 0 4.94 0.39 -13 0 0 4.95 0.41 13 0 0 5.22 0.35 14 0 0 10.85 0.53 -14 0 0 10.44 0.61 14 0 0 10.38 0.54 14 0 0 10.82 0.60 -14 0 0 10.25 0.62 15 0 0 40.85 1.63 -15 0 0 37.63 1.65 15 0 0 38.03 1.47 15 0 0 37.59 1.49 -15 0 0 36.78 1.62 16 0 0 7.76 0.48 -16 0 0 8.28 0.58 16 0 0 7.73 0.50 16 0 0 8.12 0.57 -16 0 0 8.62 0.60 17 0 0 4.38 0.44 -17 0 0 4.55 0.47 -17 0 0 4.24 0.45 17 0 0 3.76 0.36 17 0 0 3.66 0.34 18 0 0 4.02 0.39 -18 0 0 3.46 0.45 -18 0 0 3.24 0.46 18 0 0 4.11 0.37 18 0 0 4.06 0.45 19 0 0 14.61 0.79 -19 0 0 15.01 0.88 19 0 0 15.76 0.88 19 0 0 16.20 0.77 -19 0 0 16.61 0.92 20 0 0 5.89 0.49 20 0 0 7.03 0.49 -20 0 0 7.15 0.64 20 0 0 6.22 0.57 -20 0 0 5.65 0.56 -21 0 0 5.02 0.60 21 0 0 4.40 0.46 -21 0 0 4.61 0.54 21 0 0 5.05 0.49 21 0 0 5.19 0.54 -22 0 0 0.36 0.48 22 0 0 0.25 0.45 22 0 0 0.36 0.36 -22 0 0 0.90 0.48 22 0 0 0.71 0.35 -23 0 0 24.37 1.30 23 0 0 24.22 1.10 23 0 0 22.70 1.25 23 0 0 24.46 1.14 -23 0 0 24.24 1.26 -24 0 0 5.70 0.67 24 0 0 6.19 0.57 24 0 0 5.57 0.54 -24 0 0 4.48 0.62 24 0 0 5.90 0.64 25 0 0 0.14 0.44 25 0 0 0.54 0.49 25 0 0 -0.09 0.40 -25 0 0 -0.67 0.57 -25 0 0 -0.23 0.50 26 0 0 1.78 0.59 26 0 0 2.00 0.49 -26 0 0 1.81 0.62 -26 0 0 2.64 0.67 26 0 0 1.62 0.50 -27 0 0 0.35 0.59 -27 0 0 0.20 0.56 27 0 0 -0.33 0.52 27 0 0 -0.18 0.50 28 0 0 1.85 0.59 -28 0 0 1.89 0.72 28 0 0 1.23 0.60 -28 0 0 1.52 0.60 29 0 0 -0.52 0.53 -1 -1 0 0.00 0.02 1 -1 0 0.02 0.02 -1 -1 0 0.01 0.02 -1 1 0 0.03 0.02 -1 1 0 0.00 0.01 -2 -1 0 217.75 7.64 2 -1 0 229.73 8.46 -2 -1 0 242.84 8.46 -2 -1 0 215.96 7.65 2 -1 0 212.79 7.76 -2 -1 0 212.36 7.61 -2 -1 0 208.60 8.63 2 1 0 223.22 8.46 2 1 0 217.53 7.88 2 1 0 219.68 7.68 2 1 0 213.59 7.78 -2 1 0 209.25 8.46 -2 1 0 238.56 8.65 -2 1 0 217.59 7.77 -3 -1 0 0.72 0.06 -3 -1 0 0.66 0.06 -3 -1 0 0.58 0.08 -3 -1 0 0.73 0.07 -3 -1 0 0.89 0.09 3 -1 0 0.27 0.06 3 -1 0 0.36 0.08 -3 1 0 0.98 0.08 3 1 0 0.52 0.07 3 1 0 0.53 0.07 -3 1 0 0.97 0.09 3 1 0 0.57 0.08 -3 1 0 0.77 0.09 4 -1 0 0.29 0.07 -4 -1 0 0.03 0.10 4 -1 0 0.07 0.08 -4 -1 0 0.05 0.06 -4 -1 0 0.02 0.07 -4 -1 0 0.13 0.09 -4 -1 0 0.10 0.08 4 1 0 0.09 0.08 -4 1 0 0.26 0.09 4 1 0 0.07 0.08 4 1 0 0.16 0.06 -4 1 0 -0.13 0.08 -5 -1 0 3.60 0.23 5 -1 0 3.55 0.19 -5 -1 0 3.19 0.22 -5 -1 0 3.60 0.20 -5 -1 0 3.79 0.19 5 1 0 4.05 0.20 -5 1 0 3.69 0.22 5 1 0 3.67 0.20 -5 1 0 3.82 0.23 5 1 0 3.58 0.22 -6 -1 0 22.96 0.84 6 -1 0 21.95 0.86 -6 -1 0 22.28 0.96 -6 -1 0 23.65 0.95 6 -1 0 24.92 0.95 6 -1 0 23.05 0.88 -6 -1 0 23.15 0.86 6 1 0 24.06 0.87 -6 1 0 24.37 0.95 6 1 0 23.69 0.87 -6 1 0 22.46 0.97 6 1 0 21.65 0.94 -7 -1 0 2.79 0.19 7 -1 0 2.39 0.18 7 -1 0 2.84 0.21 -7 -1 0 2.30 0.21 7 -1 0 2.28 0.18 -7 -1 0 2.82 0.21 -7 -1 0 2.51 0.17 7 1 0 2.58 0.21 -7 1 0 2.75 0.22 -7 1 0 2.50 0.20 7 1 0 2.40 0.18 7 1 0 2.29 0.18 8 -1 0 0.37 0.13 -8 -1 0 0.07 0.15 8 -1 0 0.39 0.14 -8 -1 0 0.27 0.15 -8 -1 0 0.23 0.14 -8 -1 0 0.31 0.10 8 -1 0 0.35 0.12 8 1 0 0.30 0.12 -8 1 0 0.42 0.15 8 1 0 0.50 0.11 -8 1 0 0.60 0.18 8 1 0 0.45 0.15 -9 -1 0 4.75 0.29 9 -1 0 4.26 0.27 9 -1 0 4.55 0.31 -9 -1 0 3.96 0.24 9 -1 0 4.62 0.26 -9 -1 0 4.91 0.33 -9 -1 0 4.00 0.31 9 1 0 4.38 0.27 9 1 0 3.88 0.26 -9 1 0 4.69 0.32 -9 1 0 4.99 0.33 9 1 0 4.17 0.31 10 -1 0 5.95 0.37 10 -1 0 6.19 0.34 10 -1 0 5.65 0.32 -10 -1 0 5.87 0.34 -10 -1 0 6.59 0.38 -10 -1 0 5.81 0.39 -10 -1 0 5.75 0.30 10 1 0 6.02 0.33 -10 1 0 6.18 0.38 10 1 0 5.70 0.33 -10 1 0 7.23 0.40 10 1 0 5.46 0.37 11 -1 0 3.98 0.28 11 -1 0 4.42 0.34 11 -1 0 4.21 0.30 -11 -1 0 3.84 0.33 -11 -1 0 4.31 0.26 -11 -1 0 4.12 0.29 -11 -1 0 3.55 0.31 11 1 0 4.38 0.29 11 1 0 3.85 0.26 -11 1 0 4.40 0.32 -11 1 0 3.80 0.34 11 1 0 3.92 0.31 12 -1 0 15.30 0.66 12 -1 0 15.58 0.75 -12 -1 0 16.94 0.76 -12 -1 0 14.97 0.78 12 -1 0 15.74 0.68 12 1 0 16.04 0.69 12 1 0 17.36 0.76 -12 1 0 16.33 0.77 12 1 0 16.04 0.67 -12 1 0 14.02 0.74 13 -1 0 0.16 0.18 -13 -1 0 0.02 0.22 -13 -1 0 0.17 0.24 13 -1 0 -0.02 0.18 13 -1 0 0.28 0.22 13 1 0 -0.28 0.21 -13 1 0 -0.42 0.23 13 1 0 0.16 0.19 -13 1 0 -0.14 0.21 13 1 0 0.14 0.19 14 -1 0 0.66 0.25 -14 -1 0 0.62 0.27 14 -1 0 0.30 0.20 14 -1 0 0.68 0.22 -14 -1 0 0.80 0.30 14 1 0 0.62 0.26 14 1 0 0.83 0.22 -14 1 0 0.76 0.27 14 1 0 0.70 0.22 -14 1 0 0.76 0.30 -15 -1 0 18.56 0.92 15 -1 0 20.09 0.90 15 -1 0 18.47 0.79 -15 -1 0 17.85 0.91 15 -1 0 18.24 0.82 15 1 0 17.98 0.82 15 1 0 17.98 0.90 15 1 0 18.29 0.80 -15 1 0 18.42 0.92 -15 1 0 18.76 0.90 16 -1 0 0.25 0.24 -16 -1 0 0.13 0.33 16 -1 0 -0.29 0.27 16 -1 0 -0.20 0.21 -16 -1 0 0.16 0.31 16 1 0 -0.02 0.30 16 1 0 0.16 0.23 -16 1 0 0.14 0.30 16 1 0 0.38 0.25 -16 1 0 0.30 0.33 -17 -1 0 0.40 0.37 17 -1 0 -0.12 0.23 17 -1 0 0.17 0.29 17 -1 0 0.41 0.25 -17 -1 0 0.11 0.31 17 1 0 -0.07 0.30 -17 1 0 0.18 0.34 17 1 0 -0.34 0.25 -17 1 0 0.49 0.31 17 1 0 0.31 0.25 18 -1 0 15.41 0.84 -18 -1 0 14.48 0.87 18 -1 0 15.99 0.76 18 -1 0 14.33 0.72 -18 -1 0 14.51 0.84 -18 1 0 14.31 0.84 18 1 0 14.78 0.76 -18 1 0 13.81 0.85 18 1 0 16.04 0.77 18 1 0 16.17 0.85 19 -1 0 0.23 0.29 19 -1 0 0.65 0.34 -19 -1 0 -0.19 0.38 -19 -1 0 0.23 0.37 19 -1 0 0.25 0.32 19 1 0 0.01 0.28 19 1 0 0.55 0.24 19 1 0 0.24 0.35 -19 1 0 0.27 0.41 -19 1 0 0.15 0.36 19 1 0 0.11 0.30 -20 -1 0 2.27 0.48 -20 -1 0 2.86 0.46 20 -1 0 2.71 0.36 20 -1 0 2.63 0.42 20 -1 0 2.16 0.43 20 1 0 2.30 0.36 20 1 0 2.90 0.45 -20 1 0 2.57 0.47 20 1 0 2.78 0.38 20 1 0 2.17 0.30 -20 1 0 2.00 0.44 21 -1 0 3.98 0.41 -21 -1 0 4.17 0.56 21 -1 0 3.39 0.44 21 -1 0 3.52 0.50 -21 -1 0 4.23 0.53 21 1 0 4.72 0.45 -21 1 0 2.34 0.49 -21 1 0 4.76 0.58 21 1 0 4.12 0.51 21 1 0 4.41 0.44 -22 -1 0 8.75 0.70 22 -1 0 9.73 0.69 -22 -1 0 8.03 0.73 22 -1 0 9.09 0.67 22 -1 0 9.14 0.73 22 1 0 9.59 0.64 -22 1 0 8.79 0.73 22 1 0 9.24 0.66 22 1 0 10.01 0.76 -22 1 0 8.84 0.76 23 -1 0 0.55 0.38 23 -1 0 1.07 0.37 -23 -1 0 0.52 0.47 23 -1 0 0.90 0.46 -23 -1 0 0.75 0.51 -23 1 0 1.07 0.50 23 1 0 0.57 0.45 23 1 0 1.52 0.39 -23 1 0 1.16 0.51 23 1 0 0.84 0.39 -24 -1 0 1.13 0.55 -24 -1 0 2.19 0.53 24 -1 0 1.88 0.45 24 -1 0 2.60 0.53 24 -1 0 1.65 0.42 -24 1 0 1.13 0.51 24 1 0 1.93 0.47 24 1 0 1.75 0.44 24 1 0 2.16 0.52 -24 1 0 1.65 0.60 -25 -1 0 -0.71 0.50 25 -1 0 0.20 0.44 -25 -1 0 0.88 0.56 25 -1 0 0.29 0.52 25 -1 0 -0.89 0.39 -25 1 0 0.47 0.54 -25 1 0 -0.16 0.48 25 1 0 -0.15 0.44 25 1 0 0.11 0.48 25 1 0 0.56 0.50 26 -1 0 0.50 0.53 -26 -1 0 -0.13 0.54 26 -1 0 0.13 0.43 -26 -1 0 0.01 0.60 26 1 0 0.03 0.44 -26 1 0 0.05 0.61 26 1 0 -0.28 0.46 26 1 0 0.30 0.52 -26 1 0 -0.60 0.52 -27 -1 0 -0.85 0.63 27 -1 0 0.55 0.57 27 -1 0 -0.14 0.45 -27 -1 0 -0.37 0.53 -27 1 0 0.93 0.64 27 1 0 -0.09 0.52 27 1 0 0.31 0.55 -27 1 0 1.14 0.61 -28 -1 0 1.45 0.69 28 -1 0 0.82 0.58 28 -1 0 -0.06 0.46 -28 -1 0 0.62 0.64 28 1 0 1.15 0.63 -28 1 0 0.76 0.66 -28 1 0 0.02 0.57 28 1 0 0.04 0.46 29 -1 0 -1.21 0.54 29 1 0 -0.66 0.47 29 1 0 0.50 0.63 0 -2 0 184.98 7.47 0 2 0 202.33 6.81 0 2 0 178.02 6.95 0 2 0 200.95 7.47 0 2 0 195.60 6.87 0 2 0 202.91 6.93 1 -2 0 0.45 0.05 -1 -2 0 0.62 0.05 -1 -2 0 0.57 0.04 -1 -2 0 0.60 0.04 -1 -2 0 0.56 0.06 -1 -2 0 0.60 0.06 -1 -2 0 0.49 0.04 -1 2 0 0.55 0.05 -1 2 0 0.57 0.06 1 2 0 0.39 0.05 1 2 0 0.38 0.05 1 2 0 0.41 0.05 1 2 0 0.37 0.05 -1 2 0 0.51 0.05 -1 2 0 0.47 0.04 1 2 0 0.31 0.05 -2 -2 0 0.35 0.05 -2 -2 0 0.23 0.04 -2 -2 0 0.27 0.04 -2 -2 0 0.19 0.06 -2 -2 0 0.30 0.04 -2 -2 0 0.26 0.06 2 -2 0 0.21 0.06 2 2 0 0.11 0.06 2 2 0 0.22 0.04 -2 2 0 0.14 0.06 2 2 0 0.18 0.05 2 2 0 0.23 0.05 2 2 0 0.22 0.04 -2 2 0 0.20 0.04 2 2 0 0.22 0.05 -2 2 0 0.21 0.05 -2 2 0 0.15 0.06 3 -2 0 2.36 0.13 -3 -2 0 2.83 0.13 -3 -2 0 2.60 0.17 -3 -2 0 3.03 0.16 -3 -2 0 2.69 0.14 3 -2 0 2.91 0.16 -3 -2 0 2.80 0.12 -3 -2 0 2.73 0.13 3 2 0 2.83 0.13 -3 2 0 2.53 0.14 3 2 0 3.23 0.16 3 2 0 3.10 0.13 -3 2 0 2.41 0.13 -3 2 0 2.42 0.13 -3 2 0 2.32 0.15 3 2 0 2.85 0.15 3 2 0 2.81 0.14 -4 -2 0 8.56 0.33 -4 -2 0 8.29 0.38 -4 -2 0 8.65 0.33 4 -2 0 8.11 0.33 4 -2 0 8.52 0.37 -4 -2 0 8.09 0.32 -4 -2 0 8.17 0.37 4 2 0 8.61 0.32 -4 2 0 8.41 0.34 -4 2 0 7.59 0.38 4 2 0 9.54 0.38 4 2 0 8.35 0.34 -4 2 0 8.84 0.37 4 2 0 8.34 0.34 -5 -2 0 31.45 1.25 -5 -2 0 30.57 1.09 5 -2 0 30.84 1.12 -5 -2 0 29.95 1.10 -5 -2 0 29.39 1.11 5 -2 0 29.89 1.22 5 2 0 30.54 1.14 -5 2 0 27.09 1.24 -5 2 0 33.15 1.23 5 2 0 32.65 1.10 -5 2 0 31.47 1.12 5 2 0 33.30 1.23 5 2 0 30.29 1.12 -6 -2 0 27.35 1.20 -6 -2 0 28.84 1.07 -6 -2 0 29.44 1.09 6 -2 0 31.33 1.20 -6 -2 0 29.24 1.08 -6 -2 0 31.63 1.23 6 -2 0 29.64 1.09 6 2 0 29.13 1.10 -6 2 0 30.52 1.23 6 2 0 29.18 1.20 6 2 0 30.62 1.07 6 2 0 29.92 1.11 -6 2 0 32.24 1.20 -7 -2 0 1.17 0.15 7 -2 0 1.33 0.13 -7 -2 0 0.77 0.14 -7 -2 0 1.53 0.18 -7 -2 0 1.01 0.11 7 -2 0 1.50 0.16 -7 2 0 1.46 0.18 -7 2 0 1.44 0.16 7 2 0 0.87 0.13 7 2 0 1.15 0.15 7 2 0 0.96 0.14 -8 -2 0 0.30 0.15 -8 -2 0 0.09 0.10 -8 -2 0 0.29 0.16 8 -2 0 0.30 0.11 -8 -2 0 0.29 0.14 8 2 0 0.36 0.13 -8 2 0 0.34 0.14 8 2 0 0.15 0.14 8 2 0 0.07 0.12 -8 2 0 0.22 0.16 9 -2 0 13.59 0.62 -9 -2 0 12.95 0.62 -9 -2 0 13.92 0.64 9 -2 0 14.55 0.57 9 -2 0 13.23 0.55 -9 -2 0 13.98 0.54 -9 -2 0 14.27 0.57 -9 2 0 12.56 0.63 9 2 0 13.25 0.57 9 2 0 13.65 0.57 9 2 0 13.10 0.62 -9 2 0 13.87 0.62 10 -2 0 0.47 0.16 -10 -2 0 -0.01 0.18 10 -2 0 0.54 0.16 -10 -2 0 0.41 0.13 -10 -2 0 0.52 0.19 10 -2 0 0.65 0.18 -10 -2 0 0.60 0.17 10 2 0 0.41 0.18 -10 2 0 0.63 0.19 -10 2 0 0.37 0.19 10 2 0 0.35 0.16 10 2 0 0.57 0.16 11 -2 0 27.09 1.16 -11 -2 0 26.79 1.05 -11 -2 0 26.03 1.19 -11 -2 0 27.03 1.02 -11 -2 0 28.90 1.17 11 -2 0 27.63 1.05 11 -2 0 29.34 1.07 -11 2 0 26.45 1.19 11 2 0 26.81 1.05 11 2 0 26.67 1.07 11 2 0 25.50 1.16 -11 2 0 29.39 1.17 12 -2 0 0.01 0.17 -12 -2 0 0.24 0.14 -12 -2 0 -0.21 0.22 12 -2 0 -0.07 0.18 12 -2 0 0.09 0.20 -12 -2 0 -0.17 0.21 -12 -2 0 0.12 0.19 -12 2 0 0.40 0.23 12 2 0 0.03 0.17 12 2 0 0.05 0.21 12 2 0 -0.06 0.17 -12 2 0 0.28 0.21 13 -2 0 0.81 0.24 13 -2 0 1.48 0.23 -13 -2 0 0.88 0.27 13 -2 0 1.37 0.22 -13 -2 0 0.82 0.19 -13 -2 0 0.77 0.16 -13 -2 0 1.03 0.26 13 2 0 0.76 0.21 -13 2 0 1.06 0.26 13 2 0 0.87 0.20 -13 2 0 0.64 0.26 13 2 0 1.11 0.25 -14 -2 0 14.46 0.70 14 -2 0 12.12 0.58 14 -2 0 13.54 0.68 -14 -2 0 11.11 0.69 14 -2 0 13.17 0.62 14 2 0 12.65 0.56 14 2 0 13.00 0.69 -14 2 0 11.95 0.69 14 2 0 13.13 0.60 14 2 0 12.56 0.62 -14 2 0 12.93 0.68 15 -2 0 22.68 0.93 -15 -2 0 23.18 1.06 -15 -2 0 21.97 1.07 15 -2 0 22.59 0.96 15 -2 0 26.32 1.06 -15 2 0 22.25 1.07 15 2 0 21.52 0.88 15 2 0 21.87 0.96 15 2 0 22.03 0.94 15 2 0 22.19 1.05 -15 2 0 22.86 1.05 16 -2 0 2.05 0.33 -16 -2 0 1.48 0.33 16 -2 0 1.65 0.28 -16 -2 0 1.93 0.39 16 -2 0 1.73 0.29 -16 2 0 1.44 0.32 16 2 0 1.59 0.28 -16 2 0 1.96 0.36 16 2 0 1.67 0.22 16 2 0 1.47 0.33 16 2 0 2.07 0.29 17 -2 0 2.46 0.32 17 -2 0 2.83 0.30 -17 -2 0 3.44 0.41 -17 -2 0 2.69 0.41 17 -2 0 2.50 0.39 17 2 0 2.97 0.36 17 2 0 2.78 0.38 17 2 0 2.46 0.27 -17 2 0 3.20 0.40 17 2 0 2.40 0.33 -17 2 0 2.31 0.42 -18 -2 0 1.43 0.42 18 -2 0 1.74 0.32 -18 -2 0 1.79 0.39 18 -2 0 1.62 0.30 18 -2 0 1.86 0.38 18 2 0 2.03 0.35 18 2 0 1.61 0.38 -18 2 0 1.97 0.44 18 2 0 2.51 0.27 -18 2 0 1.60 0.39 18 2 0 1.12 0.31 -19 -2 0 0.81 0.40 19 -2 0 0.82 0.36 -19 -2 0 1.22 0.39 19 -2 0 0.81 0.30 19 -2 0 0.71 0.31 19 2 0 1.77 0.39 19 2 0 0.80 0.31 -19 2 0 0.87 0.41 19 2 0 0.91 0.25 19 2 0 1.27 0.32 -19 2 0 1.34 0.39 -20 -2 0 1.28 0.46 -20 -2 0 0.89 0.43 20 -2 0 1.04 0.31 20 -2 0 1.21 0.34 20 -2 0 1.23 0.39 -20 2 0 1.39 0.41 -20 2 0 1.02 0.46 20 2 0 1.36 0.34 20 2 0 0.61 0.41 20 2 0 0.56 0.32 21 -2 0 2.68 0.41 21 -2 0 2.99 0.38 21 -2 0 3.34 0.49 -21 -2 0 2.69 0.50 -21 -2 0 3.65 0.56 21 2 0 3.28 0.49 -21 2 0 2.74 0.50 21 2 0 3.22 0.42 -21 2 0 4.03 0.54 21 2 0 3.15 0.41 -22 -2 0 0.38 0.47 22 -2 0 0.58 0.37 22 -2 0 0.02 0.36 -22 -2 0 -0.29 0.43 22 -2 0 0.37 0.45 22 2 0 -0.07 0.34 -22 2 0 0.37 0.49 -22 2 0 0.46 0.49 22 2 0 -0.03 0.42 22 2 0 0.72 0.37 23 -2 0 1.65 0.43 -23 -2 0 1.34 0.54 23 -2 0 1.16 0.41 23 -2 0 1.36 0.49 -23 -2 0 1.64 0.50 23 2 0 1.06 0.46 -23 2 0 1.86 0.57 -23 2 0 1.23 0.49 23 2 0 1.73 0.48 23 2 0 1.59 0.40 -24 -2 0 0.64 0.54 24 -2 0 0.23 0.49 -24 -2 0 0.30 0.53 24 -2 0 -0.24 0.39 24 -2 0 0.98 0.35 24 2 0 0.47 0.39 -24 2 0 0.79 0.53 24 2 0 0.01 0.49 24 2 0 0.05 0.46 -24 2 0 0.82 0.52 25 -2 0 0.44 0.42 25 -2 0 1.10 0.42 25 -2 0 0.01 0.50 -25 -2 0 0.53 0.59 -25 -2 0 0.87 0.56 25 2 0 0.47 0.44 -25 2 0 1.20 0.62 25 2 0 1.30 0.56 25 2 0 0.12 0.41 -25 2 0 -0.36 0.50 26 -2 0 0.79 0.46 -26 -2 0 0.40 0.60 26 -2 0 2.52 0.57 -26 -2 0 2.13 0.65 -26 2 0 1.43 0.61 26 2 0 0.93 0.46 26 2 0 1.74 0.46 -26 2 0 0.77 0.55 26 2 0 1.45 0.59 27 -2 0 0.50 0.58 -27 -2 0 0.75 0.63 27 -2 0 0.36 0.45 -27 -2 0 0.85 0.61 -27 2 0 0.71 0.60 27 2 0 -0.03 0.51 27 2 0 1.08 0.60 27 2 0 0.03 0.51 -27 2 0 0.74 0.66 -28 -2 0 1.26 0.64 -28 -2 0 0.71 0.59 28 -2 0 1.39 0.62 28 -2 0 0.02 0.47 28 2 0 1.03 0.58 -28 2 0 1.05 0.59 28 2 0 1.08 0.50 -28 2 0 1.32 0.67 29 -2 0 -0.50 0.49 29 2 0 -0.63 0.58 29 2 0 -0.53 0.55 0 -3 0 -0.34 0.06 0 -3 0 -0.34 0.04 0 -3 0 -0.34 0.04 0 -3 0 -0.31 0.06 0 3 0 -0.36 0.05 0 3 0 -0.36 0.06 0 3 0 -0.31 0.06 0 3 0 -0.42 0.05 0 3 0 -0.25 0.05 -1 -3 0 14.91 0.54 1 -3 0 14.46 0.60 -1 -3 0 13.89 0.60 -1 -3 0 15.35 0.53 -1 -3 0 15.57 0.54 -1 -3 0 15.39 0.61 -1 -3 0 15.38 0.54 -1 3 0 15.34 0.55 -1 3 0 15.71 0.60 1 3 0 15.10 0.56 1 3 0 15.24 0.54 -1 3 0 14.76 0.55 1 3 0 14.60 0.56 -1 3 0 15.27 0.55 1 3 0 14.85 0.55 1 3 0 14.41 0.60 -2 -3 0 18.52 0.66 -2 -3 0 18.25 0.65 2 -3 0 18.32 0.73 -2 -3 0 19.56 0.74 -2 -3 0 17.98 0.65 -2 -3 0 18.32 0.67 -2 -3 0 16.92 0.75 2 3 0 18.50 0.66 -2 3 0 17.12 0.73 -2 3 0 18.14 0.68 -2 3 0 18.44 0.67 2 3 0 18.50 0.73 2 3 0 19.59 0.67 2 3 0 18.57 0.68 -2 3 0 19.33 0.67 2 3 0 18.69 0.68 -3 -3 0 140.76 5.74 -3 -3 0 144.74 5.18 -3 -3 0 147.37 5.08 -3 -3 0 143.81 5.10 -3 -3 0 146.02 5.07 3 -3 0 135.73 5.63 -3 -3 0 153.64 5.63 -3 3 0 148.35 5.17 3 3 0 160.57 5.63 3 3 0 142.13 5.18 -3 3 0 134.67 5.63 -3 3 0 144.26 5.11 -3 3 0 147.21 5.22 3 3 0 147.18 5.11 3 3 0 154.79 5.16 3 3 0 148.13 5.24 3 3 0 150.41 5.23 -4 -3 0 9.57 0.38 4 -3 0 9.54 0.38 -4 -3 0 9.69 0.37 -4 -3 0 9.88 0.44 -4 -3 0 9.64 0.37 4 -3 0 9.68 0.42 -4 -3 0 9.64 0.42 -4 -3 0 9.78 0.37 -4 3 0 10.24 0.37 -4 3 0 9.53 0.38 4 3 0 10.21 0.43 4 3 0 10.26 0.37 4 3 0 9.48 0.39 -4 3 0 9.19 0.42 4 3 0 9.74 0.39 -4 3 0 9.72 0.39 4 3 0 9.85 0.39 4 3 0 9.90 0.37 -5 -3 0 17.27 0.72 5 -3 0 16.41 0.65 -5 -3 0 17.39 0.63 -5 -3 0 17.29 0.64 -5 -3 0 17.78 0.74 5 -3 0 17.12 0.72 -5 -3 0 16.47 0.65 -5 3 0 17.72 0.66 -5 3 0 17.70 0.65 -5 3 0 16.89 0.72 5 3 0 17.16 0.64 5 3 0 19.17 0.73 -5 3 0 18.65 0.74 5 3 0 17.15 0.66 5 3 0 16.82 0.67 6 -3 0 0.97 0.12 -6 -3 0 0.97 0.13 -6 -3 0 1.44 0.16 -6 -3 0 1.25 0.10 -6 -3 0 1.29 0.15 -6 -3 0 1.13 0.12 6 -3 0 1.03 0.13 6 3 0 1.11 0.13 6 3 0 0.94 0.13 -6 3 0 1.23 0.14 -6 3 0 1.30 0.15 -6 3 0 1.55 0.15 6 3 0 1.15 0.10 6 3 0 1.02 0.15 7 -3 0 6.76 0.37 -7 -3 0 7.58 0.32 7 -3 0 7.66 0.33 -7 -3 0 7.75 0.35 -7 -3 0 7.93 0.39 -7 -3 0 7.56 0.33 -7 -3 0 7.46 0.39 7 3 0 7.66 0.33 -7 3 0 6.94 0.38 7 3 0 7.63 0.35 7 3 0 7.41 0.38 7 3 0 7.39 0.32 -7 3 0 7.87 0.38 -8 -3 0 30.07 1.12 -8 -3 0 29.82 1.10 -8 -3 0 33.83 1.28 8 -3 0 30.58 1.24 -8 -3 0 29.85 1.24 8 -3 0 29.52 1.13 8 3 0 30.68 1.10 8 3 0 29.86 1.14 -8 3 0 28.20 1.24 8 3 0 31.11 1.25 -8 3 0 31.45 1.27 8 3 0 30.97 1.15 9 -3 0 5.22 0.34 -9 -3 0 6.09 0.32 -9 -3 0 5.95 0.35 -9 -3 0 5.78 0.27 -9 -3 0 5.40 0.36 9 -3 0 5.75 0.31 9 3 0 5.60 0.31 9 3 0 5.22 0.31 9 3 0 5.45 0.27 -9 3 0 4.96 0.35 9 3 0 4.85 0.34 -9 3 0 5.90 0.34 -10 -3 0 0.28 0.18 -10 -3 0 -0.08 0.12 -10 -3 0 0.18 0.16 -10 -3 0 0.13 0.19 10 -3 0 -0.01 0.13 10 3 0 0.17 0.12 10 3 0 0.53 0.16 -10 3 0 0.18 0.18 10 3 0 -0.05 0.17 -10 3 0 -0.20 0.18 10 3 0 0.27 0.15 -11 -3 0 0.66 0.22 -11 -3 0 0.58 0.13 11 -3 0 0.88 0.18 -11 -3 0 0.67 0.21 -11 -3 0 0.48 0.19 11 -3 0 0.30 0.16 11 -3 0 0.77 0.20 -11 3 0 0.98 0.21 11 3 0 0.95 0.15 11 3 0 1.00 0.19 -11 3 0 0.56 0.21 11 3 0 0.97 0.21 11 3 0 0.85 0.15 12 -3 0 10.90 0.53 -12 -3 0 12.46 0.56 -12 -3 0 10.94 0.61 -12 -3 0 11.67 0.49 12 -3 0 10.99 0.54 -12 -3 0 12.99 0.62 12 -3 0 12.25 0.60 -12 3 0 11.71 0.60 -12 3 0 10.52 0.61 12 3 0 11.34 0.49 12 3 0 11.07 0.52 12 3 0 11.41 0.54 12 3 0 11.77 0.60 -13 -3 0 3.56 0.35 -13 -3 0 3.83 0.27 13 -3 0 4.00 0.29 13 -3 0 4.05 0.36 -13 -3 0 3.58 0.36 13 -3 0 3.77 0.30 -13 -3 0 4.03 0.32 13 3 0 4.25 0.28 13 3 0 3.77 0.30 -13 3 0 4.16 0.39 -13 3 0 3.64 0.36 13 3 0 4.12 0.36 13 3 0 3.36 0.30 14 -3 0 64.71 2.70 14 -3 0 67.73 2.51 -14 -3 0 69.18 2.41 14 -3 0 67.36 2.47 -14 -3 0 70.32 2.78 -14 -3 0 68.61 2.46 -14 -3 0 60.69 2.71 -14 3 0 63.06 2.70 14 3 0 68.84 2.72 14 3 0 67.92 2.48 -14 3 0 70.12 2.77 14 3 0 68.51 2.41 14 3 0 67.02 2.51 15 -3 0 1.05 0.25 -15 -3 0 1.16 0.34 15 -3 0 0.77 0.22 -15 -3 0 0.90 0.30 15 -3 0 1.17 0.28 -15 -3 0 1.02 0.27 15 3 0 1.12 0.25 -15 3 0 0.70 0.29 15 3 0 1.20 0.30 15 3 0 1.07 0.26 15 3 0 0.74 0.20 -15 3 0 1.38 0.34 -16 -3 0 1.61 0.37 -16 -3 0 1.82 0.35 16 -3 0 1.52 0.32 16 -3 0 1.20 0.27 16 -3 0 1.18 0.24 -16 3 0 1.52 0.37 -16 3 0 1.38 0.33 16 3 0 1.07 0.32 16 3 0 1.71 0.28 16 3 0 1.44 0.28 16 3 0 1.07 0.21 -17 -3 0 8.32 0.63 17 -3 0 8.22 0.63 17 -3 0 8.29 0.53 -17 -3 0 8.12 0.62 17 -3 0 8.78 0.54 -17 3 0 9.48 0.68 17 3 0 8.41 0.62 17 3 0 8.20 0.53 17 3 0 8.60 0.55 -17 3 0 8.54 0.65 17 3 0 9.14 0.47 18 -3 0 35.55 1.50 18 -3 0 31.77 1.35 -18 -3 0 31.24 1.48 18 -3 0 31.91 1.31 -18 -3 0 34.53 1.55 18 3 0 30.96 1.47 18 3 0 33.07 1.26 18 3 0 32.93 1.35 -18 3 0 33.71 1.48 18 3 0 34.97 1.34 -18 3 0 30.18 1.52 19 -3 0 -0.53 0.30 19 -3 0 0.54 0.34 19 -3 0 0.21 0.30 -19 -3 0 0.52 0.38 -19 -3 0 -0.03 0.40 19 3 0 0.36 0.35 19 3 0 0.30 0.30 19 3 0 -0.19 0.30 -19 3 0 0.12 0.37 -19 3 0 -0.05 0.41 19 3 0 -0.35 0.23 20 -3 0 3.23 0.40 -20 -3 0 2.28 0.51 20 -3 0 3.00 0.45 -20 -3 0 2.44 0.47 20 -3 0 3.19 0.39 20 3 0 2.99 0.46 20 3 0 2.53 0.39 -20 3 0 2.82 0.47 -20 3 0 3.12 0.53 20 3 0 3.26 0.43 -21 -3 0 0.46 0.42 -21 -3 0 0.53 0.46 21 -3 0 0.52 0.30 21 -3 0 0.23 0.39 21 -3 0 0.13 0.38 21 3 0 -0.20 0.38 21 3 0 0.40 0.40 -21 3 0 0.53 0.44 21 3 0 0.22 0.34 -21 3 0 1.15 0.44 22 -3 0 0.68 0.43 -22 -3 0 0.83 0.47 22 -3 0 0.64 0.37 22 -3 0 0.87 0.33 -22 -3 0 1.27 0.55 22 3 0 1.30 0.39 -22 3 0 0.42 0.45 22 3 0 0.27 0.44 22 3 0 0.38 0.37 -22 3 0 1.15 0.50 23 -3 0 7.90 0.60 -23 -3 0 6.23 0.68 23 -3 0 8.59 0.72 23 -3 0 7.43 0.54 -23 -3 0 7.60 0.75 -23 3 0 7.99 0.76 23 3 0 7.87 0.70 23 3 0 7.33 0.61 -23 3 0 7.91 0.72 23 3 0 7.73 0.59 24 -3 0 7.76 0.59 24 -3 0 5.55 0.65 -24 -3 0 6.55 0.72 -24 -3 0 7.89 0.77 24 -3 0 7.15 0.61 -24 3 0 7.11 0.77 24 3 0 7.47 0.73 -24 3 0 7.34 0.70 24 3 0 7.03 0.63 24 3 0 6.55 0.60 25 -3 0 0.04 0.50 25 -3 0 0.53 0.41 25 -3 0 0.62 0.43 -25 -3 0 0.18 0.61 -25 -3 0 0.81 0.58 25 3 0 0.81 0.42 -25 3 0 0.35 0.52 25 3 0 0.37 0.42 -25 3 0 0.67 0.56 25 3 0 1.50 0.56 -26 -3 0 -0.24 0.63 26 -3 0 -0.18 0.54 26 -3 0 -0.23 0.43 -26 -3 0 0.30 0.55 -26 3 0 -0.14 0.56 -26 3 0 0.45 0.60 26 3 0 0.46 0.44 26 3 0 0.00 0.43 26 3 0 -0.37 0.52 -27 -3 0 1.31 0.67 -27 -3 0 0.41 0.57 27 -3 0 0.51 0.52 27 -3 0 0.75 0.55 27 3 0 2.09 0.60 -27 3 0 2.23 0.69 27 3 0 0.89 0.52 -27 3 0 0.47 0.59 27 3 0 0.97 0.54 -28 -3 0 -0.12 0.58 28 -3 0 -0.13 0.53 -28 -3 0 0.91 0.69 28 3 0 -0.08 0.47 -28 3 0 0.25 0.64 28 3 0 0.29 0.58 -28 3 0 0.06 0.57 29 3 0 2.40 0.67 29 3 0 1.65 0.60 0 -4 0 240.42 9.79 0 -4 0 256.71 8.87 0 -4 0 260.90 9.05 0 -4 0 262.29 8.86 0 4 0 260.44 8.99 0 4 0 261.98 9.12 0 4 0 241.37 9.79 0 4 0 257.66 9.12 0 4 0 258.52 8.91 1 -4 0 38.05 1.51 -1 -4 0 39.58 1.36 -1 -4 0 38.43 1.38 -1 -4 0 38.18 1.37 -1 -4 0 38.42 1.35 -1 -4 0 38.56 1.54 -1 4 0 38.53 1.40 1 4 0 39.30 1.51 -1 4 0 40.89 1.51 -1 4 0 39.05 1.39 1 4 0 37.80 1.40 1 4 0 38.38 1.37 1 4 0 38.98 1.38 1 4 0 38.32 1.41 -1 4 0 38.41 1.37 -2 -4 0 53.64 1.98 2 -4 0 54.06 1.98 -2 -4 0 52.16 1.78 -2 -4 0 46.42 2.02 -2 -4 0 52.34 1.81 -2 -4 0 50.97 1.79 -2 -4 0 51.58 1.77 2 4 0 52.21 1.84 2 4 0 49.23 1.84 -2 4 0 49.86 1.83 2 4 0 47.14 1.98 -2 4 0 50.55 1.82 2 4 0 50.75 1.79 -2 4 0 51.21 1.98 -2 4 0 50.04 1.80 2 4 0 51.81 1.81 -3 -4 0 6.35 0.32 -3 -4 0 6.53 0.26 -3 -4 0 6.74 0.25 3 -4 0 6.86 0.31 -3 -4 0 6.68 0.27 -3 -4 0 6.23 0.30 3 4 0 6.37 0.27 -3 4 0 6.11 0.27 3 4 0 6.23 0.27 3 4 0 6.57 0.27 3 4 0 6.79 0.28 -3 4 0 5.54 0.27 3 4 0 6.49 0.29 -3 4 0 6.74 0.29 -3 4 0 7.00 0.30 -4 -4 0 11.70 0.49 4 -4 0 13.10 0.53 -4 -4 0 12.14 0.54 -4 -4 0 12.58 0.47 -4 -4 0 12.66 0.47 -4 -4 0 12.54 0.47 -4 -4 0 13.19 0.55 -4 4 0 12.92 0.48 4 4 0 13.41 0.50 -4 4 0 12.94 0.49 4 4 0 11.29 0.53 -4 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40.84 1.49 -8 -4 0 38.95 1.67 -8 -4 0 42.87 1.65 -8 4 0 43.48 1.68 -8 4 0 39.90 1.50 -8 4 0 41.37 1.49 8 4 0 39.55 1.64 8 4 0 40.37 1.51 -8 4 0 37.02 1.63 8 4 0 41.81 1.47 8 4 0 41.70 1.52 9 -4 0 1.40 0.19 -9 -4 0 1.95 0.22 -9 -4 0 1.59 0.16 -9 -4 0 2.14 0.24 -9 -4 0 1.48 0.16 9 -4 0 1.25 0.16 -9 -4 0 1.63 0.15 9 4 0 1.92 0.19 -9 4 0 1.30 0.21 9 4 0 1.43 0.18 9 4 0 1.77 0.21 -9 4 0 1.66 0.14 9 4 0 1.42 0.14 -9 4 0 1.53 0.20 10 -4 0 1.41 0.21 -10 -4 0 1.66 0.24 -10 -4 0 1.79 0.21 10 -4 0 1.66 0.18 -10 -4 0 1.83 0.23 -10 -4 0 1.63 0.15 10 4 0 1.65 0.19 10 4 0 1.93 0.16 10 4 0 1.74 0.18 -10 4 0 1.70 0.23 10 4 0 1.50 0.22 -10 4 0 1.48 0.22 11 -4 0 42.64 1.84 -11 -4 0 46.46 1.65 -11 -4 0 46.37 1.86 -11 -4 0 45.11 1.68 11 -4 0 45.73 1.69 -11 -4 0 45.61 1.89 -11 4 0 42.84 1.89 11 4 0 44.85 1.69 11 4 0 45.92 1.71 11 4 0 49.43 1.86 11 4 0 46.09 1.65 -11 4 0 46.17 1.85 -12 -4 0 0.18 0.15 12 -4 0 0.05 0.20 -12 -4 0 -0.05 0.23 -12 -4 0 -0.12 0.22 12 -4 0 -0.08 0.18 -12 -4 0 -0.16 0.19 -12 4 0 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0.89 0.36 -22 -4 0 0.85 0.52 -22 -4 0 0.83 0.51 22 -4 0 0.23 0.31 22 -4 0 0.28 0.43 22 -4 0 0.51 0.36 22 4 0 1.03 0.38 22 4 0 0.81 0.43 22 4 0 0.99 0.49 -22 4 0 -0.26 0.47 -22 4 0 0.03 0.44 -23 -4 0 -0.40 0.47 23 -4 0 -0.43 0.31 -23 -4 0 1.15 0.53 23 -4 0 0.14 0.45 23 -4 0 -0.49 0.36 23 4 0 0.32 0.39 23 4 0 -0.03 0.45 -23 4 0 -0.74 0.46 -23 4 0 -0.04 0.49 23 4 0 -0.30 0.38 -24 -4 0 0.50 0.54 24 -4 0 -0.24 0.46 24 -4 0 -0.50 0.33 -24 -4 0 -0.13 0.56 24 -4 0 -0.23 0.39 24 4 0 0.36 0.40 24 4 0 -0.09 0.39 -24 4 0 0.45 0.50 24 4 0 0.67 0.53 -24 4 0 0.23 0.53 25 -4 0 -0.31 0.41 25 -4 0 0.77 0.55 -25 -4 0 0.41 0.62 -25 -4 0 0.23 0.53 25 4 0 -0.87 0.45 -25 4 0 0.56 0.55 25 4 0 -0.24 0.50 25 4 0 -0.34 0.48 -25 4 0 0.24 0.58 -26 -4 0 1.69 0.62 26 -4 0 0.97 0.59 -26 -4 0 2.20 0.60 26 -4 0 1.25 0.53 -26 4 0 1.70 0.64 26 4 0 1.65 0.54 -26 4 0 0.91 0.59 26 4 0 0.86 0.57 26 4 0 1.25 0.47 -27 -4 0 0.33 0.56 -27 -4 0 -0.64 0.59 27 -4 0 1.26 0.60 27 -4 0 0.17 0.46 27 4 0 1.55 0.55 27 4 0 -0.30 0.53 -27 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111.07 4.49 -3 -5 0 119.27 4.04 -3 -5 0 119.10 4.12 3 5 0 119.78 4.11 3 5 0 114.49 4.07 -3 5 0 118.26 4.08 -3 5 0 109.64 4.49 -3 5 0 117.96 4.16 3 5 0 114.30 4.18 3 5 0 118.36 4.18 3 5 0 116.11 4.49 -3 5 0 114.19 4.13 -4 -5 0 2.02 0.16 -4 -5 0 2.27 0.18 -4 -5 0 2.24 0.13 4 -5 0 2.49 0.18 -4 -5 0 2.28 0.15 -4 -5 0 2.06 0.17 -4 -5 0 2.25 0.13 4 5 0 2.64 0.18 -4 5 0 2.47 0.16 4 5 0 2.37 0.15 -4 5 0 2.45 0.18 -4 5 0 2.18 0.16 -4 5 0 2.47 0.15 4 5 0 2.40 0.15 4 5 0 2.34 0.15 4 5 0 2.42 0.18 4 5 0 2.25 0.18 -5 -5 0 0.57 0.09 -5 -5 0 0.68 0.12 -5 -5 0 0.62 0.09 5 -5 0 0.56 0.12 -5 -5 0 0.69 0.08 -5 -5 0 0.58 0.14 -5 -5 0 0.93 0.14 -5 5 0 0.69 0.13 -5 5 0 0.69 0.13 5 5 0 0.43 0.12 5 5 0 0.72 0.09 5 5 0 0.71 0.09 5 5 0 0.44 0.12 5 5 0 0.57 0.13 5 5 0 0.53 0.10 -5 5 0 0.77 0.09 -5 5 0 0.49 0.12 -6 -5 0 1.15 0.17 -6 -5 0 1.00 0.10 -6 -5 0 0.97 0.12 -6 -5 0 1.08 0.10 6 -5 0 1.04 0.14 -6 -5 0 1.10 0.15 6 5 0 0.83 0.11 6 5 0 1.31 0.11 -6 5 0 1.33 0.15 -6 5 0 1.23 0.15 6 5 0 1.03 0.15 6 5 0 0.97 0.12 6 5 0 1.02 0.14 6 5 0 0.90 0.14 -6 5 0 1.01 0.10 -7 -5 0 27.74 1.00 -7 -5 0 27.84 1.00 7 -5 0 27.17 1.13 -7 -5 0 28.06 1.03 -7 -5 0 27.48 1.13 -7 -5 0 26.74 1.16 -7 5 0 28.34 1.02 7 5 0 28.45 1.01 7 5 0 28.61 1.05 7 5 0 26.19 1.13 -7 5 0 26.56 1.13 7 5 0 28.10 1.01 7 5 0 26.80 1.04 -7 5 0 27.56 1.04 -7 5 0 29.23 1.16 8 -5 0 79.05 3.15 8 -5 0 81.84 2.89 -8 -5 0 80.63 2.82 -8 -5 0 80.67 3.22 -8 -5 0 79.53 2.85 -8 -5 0 80.96 2.83 -8 -5 0 80.48 3.15 -8 5 0 83.85 2.90 8 5 0 77.77 2.90 8 5 0 81.54 2.93 -8 5 0 82.71 3.22 8 5 0 74.61 3.15 -8 5 0 81.74 2.90 -8 5 0 75.00 3.14 8 5 0 84.04 2.87 8 5 0 83.43 2.84 -9 -5 0 16.71 0.66 -9 -5 0 16.77 0.77 9 -5 0 16.87 0.68 -9 -5 0 17.38 0.66 9 -5 0 17.22 0.76 -9 -5 0 17.64 0.80 -9 -5 0 17.31 0.70 9 5 0 17.84 0.67 9 5 0 17.02 0.70 -9 5 0 15.96 0.78 9 5 0 17.22 0.66 -9 5 0 17.45 0.69 9 5 0 18.63 0.78 9 5 0 17.48 0.71 -9 5 0 17.64 0.67 -9 5 0 18.12 0.77 -10 -5 0 0.16 0.19 10 -5 0 -0.15 0.16 -10 -5 0 0.45 0.21 -10 -5 0 0.11 0.17 -10 -5 0 0.22 0.11 10 -5 0 0.14 0.14 -10 -5 0 0.26 0.15 -10 5 0 0.42 0.20 10 5 0 0.27 0.12 10 5 0 0.29 0.16 -10 5 0 0.11 0.10 10 5 0 0.28 0.17 -10 5 0 0.28 0.18 10 5 0 0.24 0.19 -11 -5 0 28.79 1.26 -11 -5 0 30.52 1.30 -11 -5 0 28.45 1.14 11 -5 0 29.84 1.13 -11 -5 0 29.32 1.10 11 -5 0 30.42 1.25 11 5 0 32.85 1.27 11 5 0 28.59 1.15 -11 5 0 29.88 1.11 11 5 0 29.70 1.16 -11 5 0 28.60 1.25 -11 5 0 29.97 1.28 11 5 0 28.79 1.10 -12 -5 0 52.72 2.17 -12 -5 0 53.50 1.88 -12 -5 0 54.94 2.13 -12 -5 0 51.68 1.92 12 -5 0 54.45 1.93 12 -5 0 52.29 2.11 -12 5 0 48.23 2.11 -12 5 0 52.53 1.91 12 5 0 50.22 1.96 -12 5 0 51.98 2.16 12 5 0 52.70 1.94 12 5 0 52.56 1.88 12 5 0 50.51 2.12 -13 -5 0 0.13 0.25 -13 -5 0 -0.03 0.26 -13 -5 0 0.07 0.17 13 -5 0 0.08 0.21 13 -5 0 -0.28 0.20 -13 -5 0 0.15 0.16 13 5 0 0.16 0.20 13 5 0 0.15 0.15 -13 5 0 0.37 0.25 13 5 0 -0.37 0.20 -13 5 0 -0.04 0.13 13 5 0 0.38 0.25 -13 5 0 0.08 0.26 -14 -5 0 0.18 0.31 -14 -5 0 0.43 0.25 -14 -5 0 0.73 0.30 14 -5 0 0.02 0.21 14 -5 0 -0.03 0.24 14 -5 0 0.27 0.20 -14 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0.98 11 6 0 21.90 0.83 11 6 0 20.45 0.87 11 6 0 21.94 0.89 -12 -6 0 1.26 0.17 -12 -6 0 1.19 0.27 12 -6 0 1.21 0.24 12 -6 0 1.91 0.21 -12 -6 0 1.43 0.29 -12 -6 0 1.45 0.25 12 6 0 1.17 0.19 12 6 0 1.39 0.23 -12 6 0 1.21 0.28 12 6 0 1.42 0.18 -12 6 0 1.16 0.15 -12 6 0 1.11 0.25 12 6 0 1.74 0.29 12 6 0 1.38 0.18 -13 -6 0 3.93 0.39 -13 -6 0 3.46 0.26 13 -6 0 5.15 0.38 -13 -6 0 3.57 0.34 13 -6 0 4.15 0.32 -13 -6 0 4.15 0.41 -13 6 0 4.75 0.27 13 6 0 3.70 0.27 13 6 0 4.14 0.39 -13 6 0 4.53 0.41 13 6 0 4.18 0.29 13 6 0 4.31 0.34 -13 6 0 3.98 0.36 13 6 0 3.68 0.33 -14 -6 0 14.80 0.59 -14 -6 0 14.51 0.67 -14 -6 0 12.55 0.73 -14 -6 0 13.28 0.74 14 -6 0 12.22 0.63 14 6 0 14.53 0.59 14 6 0 13.07 0.58 -14 6 0 12.47 0.73 14 6 0 13.03 0.73 -14 6 0 12.88 0.56 14 6 0 13.37 0.66 -14 6 0 14.03 0.72 14 6 0 13.14 0.65 -15 -6 0 32.98 1.55 15 -6 0 36.57 1.38 15 -6 0 35.30 1.41 -15 -6 0 38.10 1.60 15 -6 0 36.05 1.53 -15 -6 0 34.59 1.33 -15 -6 0 36.91 1.40 15 6 0 37.76 1.41 15 6 0 34.16 1.32 15 6 0 37.01 1.56 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3.46 -2 -7 0 88.27 3.14 -2 -7 0 88.47 3.11 2 7 0 91.07 3.17 2 7 0 89.11 3.23 2 7 0 85.58 3.22 -2 7 0 89.90 3.46 2 7 0 89.64 3.46 -2 7 0 88.65 3.15 -2 7 0 90.36 3.18 -2 7 0 87.41 3.21 2 7 0 88.02 3.14 -3 -7 0 90.90 3.19 -3 -7 0 96.79 3.52 3 -7 0 83.71 3.51 -3 -7 0 91.97 3.21 -3 -7 0 92.70 3.16 -3 -7 0 95.15 3.17 -3 -7 0 81.91 3.58 -3 7 0 89.53 3.51 3 7 0 90.31 3.52 -3 7 0 89.62 3.20 3 7 0 87.15 3.27 3 7 0 94.11 3.22 -3 7 0 89.97 3.26 3 7 0 91.05 3.28 3 7 0 90.54 3.19 -3 7 0 92.43 3.23 4 -7 0 8.51 0.39 -4 -7 0 7.89 0.39 -4 -7 0 7.82 0.31 -4 -7 0 7.39 0.35 -4 -7 0 7.25 0.40 -4 -7 0 7.97 0.33 -4 -7 0 7.64 0.32 4 7 0 8.02 0.33 -4 7 0 7.93 0.36 4 7 0 7.24 0.38 -4 7 0 7.98 0.39 4 7 0 7.80 0.36 -4 7 0 7.99 0.36 4 7 0 8.03 0.34 -4 7 0 8.14 0.34 4 7 0 7.73 0.36 -5 -7 0 8.28 0.40 -5 -7 0 7.34 0.40 -5 -7 0 7.28 0.33 -5 -7 0 7.66 0.32 -5 -7 0 7.11 0.31 5 -7 0 7.29 0.38 -5 -7 0 8.16 0.34 -5 7 0 7.17 0.39 -5 7 0 7.33 0.34 5 7 0 7.65 0.40 5 7 0 8.11 0.37 5 7 0 8.01 0.33 5 7 0 8.12 0.36 5 7 0 7.47 0.36 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