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Information card for entry 4034409
Preview
| Coordinates | 4034409.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H24 N P |
|---|---|
| Calculated formula | C24 H24 N P |
| SMILES | P(c1ccccc1)(c1ccccc1)c1cccc2CC[C@]3(NCCC3)c12 |
| Title of publication | Preparation and Application of Amino Phosphine Ligands Bearing Spiro[indane-1,2'-pyrrolidine] Backbone. |
| Authors of publication | Li, Shasha; Zhang, Jinxia; Li, Hongjie; Feng, Lifei; Jiao, Peng |
| Journal of publication | The Journal of organic chemistry |
| Year of publication | 2019 |
| Journal volume | 84 |
| Journal issue | 15 |
| Pages of publication | 9460 - 9473 |
| a | 11.6263 ± 0.0001 Å |
| b | 13.4946 ± 0.0001 Å |
| c | 11.7477 ± 0.0001 Å |
| α | 90° |
| β | 90.512 ± 0.001° |
| γ | 90° |
| Cell volume | 1843.05 ± 0.03 Å3 |
| Cell temperature | 100.01 ± 0.1 K |
| Ambient diffraction temperature | 100.01 ± 0.1 K |
| Number of distinct elements | 4 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.026 |
| Residual factor for significantly intense reflections | 0.0253 |
| Weighted residual factors for significantly intense reflections | 0.0663 |
| Weighted residual factors for all reflections included in the refinement | 0.0669 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.037 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 222940 (current) | 2019-11-04 | cif/ Adding structures of 4034409 via cif-deposit CGI script. |
4034409.cif |
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Users of the data should acknowledge the original authors of the
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