#------------------------------------------------------------------------------ #$Date: 2019-11-04 15:06:56 +0200 (Mon, 04 Nov 2019) $ #$Revision: 223098 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/03/46/4034620.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4034620 loop_ _publ_author_name 'Mart\'inez Su\'arez, Jaime F' 'Caram, Jos\'e A' 'Echeverr\'ia, Gustavo A' 'Piro, Oscar E.' 'Gennaro, Ana M.' 'Mir\'ifico, Mar\'ia V' _publ_section_title ; Electrosynthesis of N-Methylisatin. ; _journal_issue 11 _journal_name_full 'The Journal of organic chemistry' _journal_page_first 6879 _journal_page_last 6885 _journal_paper_doi 10.1021/acs.joc.9b00690 _journal_volume 84 _journal_year 2019 _chemical_formula_sum 'C9 H7 N O2' _chemical_formula_weight 161.16 _chemical_name_common N-methylisatin _chemical_name_systematic 1-methylindole-2,3-dione _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 90 _cell_angle_beta 103.2625(19) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 8.33461(16) _cell_length_b 10.7980(2) _cell_length_c 17.6151(3) _cell_measurement_reflns_used 5839 _cell_measurement_temperature 297(2) _cell_measurement_theta_max 72.1360 _cell_measurement_theta_min 4.1260 _cell_volume 1543.03(5) _computing_cell_refinement ; CrysAlisPro, Agilent Technologies, Version 1.171.37.31 (release 14-01-2014 CrysAlis171 .NET) (compiled Jan 14 2014,18:38:05) ; _computing_data_collection ; CrysAlisPro, Agilent Technologies, Version 1.171.37.31 (release 14-01-2014 CrysAlis171 .NET) (compiled Jan 14 2014,18:38:05) ; _computing_data_reduction ; CrysAlisPro, Agilent Technologies, Version 1.171.37.31 (release 14-01-2014 CrysAlis171 .NET) (compiled Jan 14 2014,18:38:05) ; _computing_molecular_graphics 'ORTEP-3 (Farrugia, 1997)' _computing_publication_material 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXS (Sheldrick, 2008)' _diffrn_ambient_temperature 297(2) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 16.0604 _diffrn_detector_type Eos _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Xcalibur, Eos, Gemini' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0271 _diffrn_reflns_av_unetI/netI 0.0174 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 15172 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 70.995 _diffrn_reflns_theta_min 4.840 _diffrn_source 'Enhance (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.827 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.85289 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro, Agilent Technologies, Version 1.171.37.31 (release 14-01-2014 CrysAlis171 .NET) (compiled Jan 14 2014,18:38:05) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour pink _exptl_crystal_density_diffrn 1.387 _exptl_crystal_description fragment _exptl_crystal_F_000 672 _exptl_crystal_size_max 0.316 _exptl_crystal_size_mid 0.280 _exptl_crystal_size_min 0.251 _refine_diff_density_max 0.163 _refine_diff_density_min -0.124 _refine_diff_density_rms 0.033 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.038 _refine_ls_hydrogen_treatment refall _refine_ls_matrix_type full _refine_ls_number_parameters 273 _refine_ls_number_reflns 2980 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.038 _refine_ls_R_factor_all 0.0479 _refine_ls_R_factor_gt 0.0413 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0756P)^2^+0.2187P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1189 _refine_ls_wR_factor_ref 0.1287 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2581 _reflns_number_total 2980 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file jo9b00690_si_002.cif _cod_data_source_block shelx _cod_original_cell_volume 1543.02(5) _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 4034620 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.780 _shelx_estimated_absorpt_t_max 0.819 _shelx_res_file ; shelx.res created by SHELXL-2014/7 TITL N-metil-I_3 in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 1.54184 8.334610 10.797952 17.615121 90.0000 103.2625 90.0000 ZERR 8.00 0.000160 0.000221 0.000343 0.0000 0.0019 0.0000 LATT 1 SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H N O UNIT 72 56 8 16 OMIT -3 142 MERG 2 SIZE 0.251 0.280 0.316 TEMP 24 REM Crystal shape/color: Fragment/pink EQIV $1 -x+1, -y+1, -z+1 HTAB C17 O21_$1 HTAB C19 O22_$1 EQIV $2 -x, -y+2, -z+1 HTAB C27 O11_$2 MPLA 9 C11 > C19 C21 > C29 ACTA FMAP 2 PLAN -5 L.S. 15 WGHT 0.075600 0.218700 FVAR 5.23444 MOLE 1 C11 1 0.379449 0.888039 0.499807 11.00000 0.04506 0.03769 = 0.05123 -0.00342 0.01038 -0.00166 C12 1 0.386201 0.910594 0.587435 11.00000 0.05237 0.04284 = 0.05068 -0.00394 0.01498 -0.00119 C13 1 0.487125 0.809772 0.628386 11.00000 0.04967 0.05111 = 0.05427 0.00730 0.01201 -0.00472 C14 1 0.536035 0.781084 0.706567 11.00000 0.07005 0.08992 = 0.06061 0.02177 0.01275 -0.00798 C15 1 0.630431 0.674832 0.726250 11.00000 0.07569 0.10546 = 0.08867 0.05149 -0.00508 -0.01143 C16 1 0.674241 0.602750 0.669578 11.00000 0.06257 0.06381 = 0.13856 0.04199 -0.00042 0.00340 C17 1 0.627062 0.631028 0.590598 11.00000 0.05264 0.04480 = 0.11284 0.01003 0.00989 0.00398 C18 1 0.531813 0.735572 0.571412 11.00000 0.04160 0.03861 = 0.07063 0.00308 0.01113 -0.00373 C19 1 0.487918 0.729370 0.423841 11.00000 0.06689 0.06837 = 0.07154 -0.02674 0.02129 0.00081 N1 3 0.467035 0.783802 0.496281 11.00000 0.05061 0.04090 = 0.05575 -0.00828 0.01267 0.00036 O11 4 0.307743 0.951862 0.445493 11.00000 0.06563 0.05534 = 0.05366 0.00438 0.00588 0.00600 O12 4 0.316235 0.994960 0.610622 11.00000 0.08556 0.06197 = 0.06700 -0.01272 0.02342 0.01568 H14 2 0.502155 0.833401 0.747406 11.00000 0.10184 H15 2 0.658429 0.653031 0.777277 11.00000 0.10738 H16 2 0.742205 0.526190 0.679378 11.00000 0.12170 H17 2 0.661329 0.576872 0.551894 11.00000 0.09654 H19A 2 0.421817 0.651114 0.418819 11.00000 0.10605 H19B 2 0.461637 0.789310 0.375948 11.00000 0.16317 H19C 2 0.596333 0.699705 0.430948 11.00000 0.10967 MOLE 2 C21 1 0.120806 0.626469 0.532158 11.00000 0.05314 0.04732 = 0.05922 -0.00596 0.02327 -0.00104 C22 1 0.188502 0.563225 0.612267 11.00000 0.05118 0.04108 = 0.07006 -0.00061 0.01987 0.00417 C23 1 0.138173 0.643467 0.669172 11.00000 0.04453 0.03990 = 0.05636 0.00059 0.01341 -0.00113 C24 1 0.164293 0.636699 0.749381 11.00000 0.05695 0.06156 = 0.05624 0.00721 0.00881 -0.00314 C25 1 0.098834 0.728689 0.787858 11.00000 0.07175 0.07915 = 0.05192 -0.00747 0.01542 -0.00474 C26 1 0.011218 0.825197 0.746149 11.00000 0.07306 0.06669 = 0.06522 -0.01907 0.02421 0.00159 C27 1 -0.015122 0.834567 0.665493 11.00000 0.05947 0.04458 = 0.06667 -0.00485 0.01937 0.00620 C28 1 0.049744 0.741408 0.627834 11.00000 0.04402 0.03825 = 0.05000 -0.00193 0.01346 -0.00136 C29 1 -0.051496 0.812304 0.487859 11.00000 0.06091 0.06504 = 0.06009 0.01361 0.01189 0.00691 N2 3 0.040591 0.729856 0.547234 11.00000 0.05409 0.04508 = 0.05002 0.00251 0.01502 0.00501 O21 4 0.137030 0.590921 0.468902 11.00000 0.08381 0.07433 = 0.06601 -0.01296 0.03580 0.00115 O22 4 0.264272 0.467486 0.620480 11.00000 0.08586 0.05424 = 0.10047 0.00204 0.02710 0.02787 H24 2 0.231950 0.571508 0.779324 11.00000 0.08094 H25 2 0.117887 0.728492 0.843732 11.00000 0.09959 H26 2 -0.033535 0.892984 0.775951 11.00000 0.09211 H27 2 -0.080041 0.900021 0.637388 11.00000 0.07339 H29A 2 -0.083908 0.766696 0.439015 11.00000 0.09390 H29B 2 0.013417 0.881426 0.479604 11.00000 0.09412 H29C 2 -0.158940 0.837149 0.502938 11.00000 0.08499 HKLF 4 REM N-metil-I_3 in P2(1)/c REM R1 = 0.0413 for 2581 Fo > 4sig(Fo) and 0.0479 for all 2980 data REM 273 parameters refined using 0 restraints END WGHT 0.0668 0.2499 REM Highest difference peak 0.163, deepest hole -0.124, 1-sigma level 0.033 Q1 1 0.3620 0.7199 0.3851 11.00000 0.05 0.16 Q2 1 0.7040 0.6391 0.7069 11.00000 0.05 0.14 Q3 1 0.1654 0.5224 0.4915 11.00000 0.05 0.14 Q4 1 0.6172 0.7345 0.7099 11.00000 0.05 0.14 Q5 1 0.3651 0.9563 0.6612 11.00000 0.05 0.13 ; _shelx_res_checksum 77026 _shelx_hkl_file ; 0 0 2 174170. 749.944 52 0 0 3 22.2527 14.5032 52 0 0 3 28.0870 22.0090 10 0 0 4 9239.12 353.170 10 0 0 4 9622.23 250.178 52 0 0 5 9.81640 15.6560 52 0 0 -6 17694.2 654.779 1 0 0 6 17329.9 602.241 10 0 0 7 9.03975 44.1814 10 0 0 -7-20.9660 47.0727 1 0 0 -8 45211.0 1253.01 1 0 0 8 43850.0 1161.02 10 0 0 9-20.5877 45.2425 10 0 0 -9 27.1451 44.2668 1 0 0 10-39.4182 51.2726 10 0 0 -10 4.12732 71.5596 1 0 0 -11-120.819 86.9145 1 0 0 11-143.899 88.8004 10 0 0 -12 134.578 95.6594 1 0 0 -13 237.685 127.611 1 0 0 14 188.472 34.0854 25 0 0 14 199.703 32.4555 24 0 0 15-5.65345 21.7321 25 0 0 16 2172.08 100.393 25 0 0 16 2012.05 99.3509 27 0 0 17-6.37879 20.5818 27 0 0 17 28.5139 21.6597 25 0 0 18 1068.78 65.7478 25 0 0 18 1136.92 69.9474 27 0 0 19-19.9799 19.7139 27 0 0 19-4.48577 14.9880 25 0 0 20 47.8226 14.3105 25 0 0 20 28.2628 16.1646 27 0 0 21 29.8465 12.5339 27 0 1 0 441.320 39.5280 6 0 -1 0 581.005 58.6722 58 0 1 -1 460.067 45.5935 1 0 -1 1 465.286 39.0317 60 0 -1 -1 441.760 45.2130 50 0 1 -2 316415. 1600.28 1 0 -1 2 315306. 1152.21 10 0 -1 3 27869.7 540.575 52 0 -1 3 27710.2 449.522 10 0 1 -3 27844.3 581.020 1 0 -1 4 21286.3 476.761 10 0 -1 4 21486.2 514.893 52 0 1 -5 27.4292 37.9661 1 0 -1 -5 37.5027 34.4684 1 0 -1 5 4.06528 29.2744 52 0 1 5 7.43830 34.1486 10 0 -1 5 42.3553 42.0658 10 0 1 6 10662.7 513.313 10 0 1 -6 10805.2 519.212 1 0 -1 -6 10610.0 506.733 1 0 1 -7 343.151 109.575 1 0 1 7 492.031 128.623 10 0 -1 -7 558.255 135.340 1 0 1 8 376.267 120.044 10 0 -1 -8 220.479 96.8960 1 0 1 -8 267.349 116.676 1 0 -1 8 357.081 107.647 10 0 -1 9 2744.92 295.554 10 0 1 9 2657.05 324.342 10 0 -1 -9 3251.70 363.215 1 0 1 -9 2650.31 329.796 1 0 1 10 146.509 86.2181 10 0 -1 10 295.216 105.249 10 0 1 -10 302.266 126.102 1 0 -1 -10 189.484 99.2167 1 0 1 -11 2136.84 343.121 1 0 -1 -11 1817.73 311.168 1 0 1 11 2490.29 354.235 10 0 -1 -12 1060.33 251.120 1 0 1 12 1349.18 275.766 10 0 1 -12 954.347 251.569 1 0 -1 -12 1267.81 286.248 61 0 1 -13 3126.11 457.942 1 0 1 13 3203.56 450.794 10 0 -1 -13 3355.69 468.020 61 0 -1 -13 3058.12 457.437 1 0 1 14 989.124 66.9977 25 0 1 14 930.638 63.2866 17 0 -1 14 1030.78 69.7285 25 0 -1 14 955.664 67.2349 27 0 -1 14 994.976 66.0250 24 0 1 14 1099.30 70.1007 16 0 1 14 966.293 66.3977 19 0 -1 15 3136.20 120.418 25 0 1 15 3207.52 121.884 19 0 -1 15 3310.91 119.699 24 0 -1 15 3061.02 120.579 27 0 1 15 3245.75 120.766 25 0 -1 16 2208.65 103.060 27 0 -1 16 2161.23 100.333 25 0 1 16 2174.41 98.6170 25 0 -1 16 2370.08 100.366 24 0 -1 17 849.936 64.3150 27 0 1 17 893.922 62.9525 25 0 -1 17 904.736 61.6504 24 0 -1 17 958.415 65.9142 25 0 1 18 1.19785 20.3807 27 0 -1 18 2.11310 17.8067 25 0 -1 18-9.75847 22.8436 27 0 1 18-43.0712 19.2565 25 0 -1 19 1166.32 63.2967 27 0 1 19 1148.64 58.6991 25 0 1 19 1124.41 63.9163 27 0 -1 19 1229.35 63.7774 25 0 1 20 329.167 32.0823 27 0 -1 20 353.644 32.9478 27 0 1 21 603.870 33.4788 27 0 -2 0 279389. 1766.10 58 0 -2 0 275971. 1446.79 8 0 -2 -1 32448.3 601.962 61 0 2 1 34588.7 431.278 3 0 -2 -1 31893.8 574.372 8 0 2 -1 34315.0 406.823 1 0 2 1 34085.4 639.099 5 0 2 1 34130.6 615.292 57 0 -2 -1 31322.5 559.928 53 0 -2 1 32223.5 474.426 61 0 -2 -1 34438.8 588.471 50 0 -2 -2 15933.3 383.911 50 0 -2 2 15670.4 316.710 60 0 2 2 15821.4 476.716 5 0 2 2 16051.6 470.536 10 0 2 -2 15889.2 371.598 1 0 -2 -2 14810.2 394.792 53 0 -2 -2 15304.3 309.341 1 0 -2 -3 712.374 87.8566 1 0 2 -3 808.413 103.688 1 0 2 3 728.469 118.424 5 0 -2 3 850.732 122.066 52 0 2 -3 836.270 89.9770 9 0 2 -4 137246. 1519.84 1 0 2 4 134894. 1705.94 56 0 -2 4 135686. 1035.23 10 0 2 -5 15857.1 577.721 1 0 2 5 15065.3 605.276 10 0 -2 5 15854.6 421.252 10 0 2 5 15202.2 631.626 56 0 2 5 15095.8 637.180 4 0 -2 -5 14839.9 537.082 1 0 -2 -6 2598.39 253.600 1 0 2 -6 2422.85 253.718 1 0 -2 6 2737.12 202.214 10 0 2 6 2548.31 275.015 10 0 2 6 2754.36 304.633 4 0 -2 -7 9655.21 532.535 1 0 2 7 10015.9 577.335 10 0 2 -7 10388.2 564.283 1 0 2 -8 1231.11 216.599 1 0 2 8 1536.79 243.266 10 0 -2 -8 1105.43 198.504 1 0 2 9 129.522 81.6174 10 0 -2 -9-58.5727 56.8064 1 0 2 -9 105.209 62.0896 1 0 -2 -10 384.403 132.955 1 0 2 10 474.026 154.118 10 0 2 -10 476.496 159.364 1 0 -2 -11 230.050 123.001 61 0 -2 -11 129.958 90.8201 1 0 2 -11 169.934 104.771 1 0 2 11 388.009 151.494 10 0 -2 -12 2250.52 361.962 1 0 2 12 2262.10 371.348 10 0 2 -12 1736.38 335.621 1 0 -2 -12 2130.39 378.929 61 0 -2 13 227.791 35.6654 27 0 2 13 210.988 30.1138 20 0 -2 13 229.566 34.2631 26 0 -2 13 216.890 34.9873 25 0 2 13 193.673 32.9797 25 0 2 13 214.759 125.307 10 0 2 13 228.133 33.4124 19 0 -2 13 263.627 35.8410 24 0 2 14 11097.5 221.703 16 0 -2 14 10963.7 217.286 24 0 -2 14 10711.3 219.130 27 0 2 14 10948.0 221.409 17 0 2 14 10587.0 219.990 19 0 2 14 11083.4 216.642 25 0 2 14 10729.8 219.965 20 0 -2 14 10939.9 221.952 25 0 2 15 323.685 42.7450 19 0 -2 15 321.117 43.8225 25 0 2 15 348.186 42.4116 16 0 2 15 340.680 42.4078 17 0 -2 15 329.122 43.9252 24 0 -2 15 285.262 40.0359 27 0 2 15 369.806 44.3034 25 0 -2 16 544.967 54.3955 25 0 -2 16 551.157 53.8955 27 0 -2 16 572.099 52.4394 24 0 2 16 557.033 51.9989 16 0 2 16 607.947 54.0531 17 0 2 16 574.940 54.3133 19 0 2 16 522.477 49.0860 25 0 2 17 153.261 30.2680 25 0 2 17 201.978 30.9987 17 0 -2 17 178.513 35.2139 25 0 -2 17 155.953 32.1720 27 0 2 18 230.694 36.5572 27 0 -2 18 243.751 35.7419 27 0 2 18 198.447 28.1482 25 0 -2 18 181.861 31.2038 25 0 2 19 321.056 36.6186 27 0 -2 19 333.452 34.5395 25 0 -2 19 303.318 33.8691 27 0 -2 20 30.5823 15.3603 49 0 -2 20 56.7601 16.3982 27 0 2 20 43.3910 17.0588 27 0 3 0 31.5090 31.1934 57 0 3 0 13.7917 27.8372 6 0 -3 0 4.31950 28.5181 8 0 -3 0 18.3326 37.7187 58 0 -3 0 90.2406 38.3959 61 0 -3 0-6.65104 41.4265 50 0 3 1 1076.27 128.897 10 0 3 -1 1061.93 70.0588 2 0 -3 1 1585.03 134.535 61 0 3 1 1048.85 139.000 5 0 -3 -1 1071.83 126.671 8 0 -3 1 1036.57 102.735 8 0 3 -1 1070.05 122.055 6 0 3 1 1200.64 101.158 3 0 3 1 990.766 142.519 7 0 3 1 870.124 119.703 57 0 -3 -1 1126.82 136.389 50 0 3 2 638.336 114.245 10 0 3 2 767.248 129.365 7 0 -3 -2 529.222 48.7094 1 0 -3 -2 567.767 103.072 50 0 3 2 599.641 112.296 5 0 3 -2 531.107 71.8397 1 0 -3 -3 767.191 133.726 61 0 3 -3 817.156 93.2183 9 0 -3 3 764.862 138.218 53 0 -3 -3 840.676 88.0028 1 0 3 3 807.925 141.280 5 0 3 3 811.566 138.323 10 0 3 -3 850.169 108.698 1 0 3 4 24097.4 779.504 10 0 3 -4 25854.9 567.962 9 0 -3 -4 23052.6 766.176 61 0 -3 -4 23841.5 572.434 1 0 3 4 22222.2 780.327 56 0 3 -4 25882.9 672.575 1 0 3 4 24250.1 787.589 5 0 -3 4 25971.0 539.569 60 0 3 -5 32071.0 839.902 1 0 3 5 32018.4 958.220 10 0 -3 -5 30462.3 946.535 61 0 3 5 31270.3 991.249 56 0 3 5 30964.5 985.892 4 0 -3 5 33192.4 679.154 60 0 3 6 11471.3 643.282 56 0 3 6 11530.4 646.889 4 0 3 6 11400.2 616.633 10 0 3 -6 12841.1 585.751 1 0 -3 -6 11919.7 525.863 1 0 -3 -6 11753.0 630.420 61 0 3 -7 65544.5 1442.68 1 0 3 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331.839 1 -2 3 -9 2183.72 345.080 1 2 -3 8 1133.79 252.415 59 2 3 8 1025.00 237.339 10 2 -3 8 1213.23 243.222 52 -2 3 -8 919.042 212.928 1 2 -3 7 11377.7 731.627 59 2 -3 7 13264.5 767.861 52 2 3 7 11575.5 760.058 4 2 3 7 12349.7 778.569 10 2 -3 6 13590.2 757.731 59 2 3 6 14734.8 810.134 4 2 3 6 14391.7 708.702 56 -2 3 -6 14420.7 737.737 9 2 -3 6 14335.4 771.365 52 2 3 6 14823.4 802.313 10 2 3 5 43893.0 1341.16 5 2 -3 5 42833.7 1256.52 59 2 -3 5 44614.6 1250.82 53 -2 3 -5 43252.7 1214.21 9 2 -3 5 43409.3 1288.06 52 2 3 5 41455.3 1144.61 56 2 3 5 42373.5 1296.09 4 2 3 4 5688.76 459.957 5 2 3 4 6631.24 365.548 59 -2 3 -4 5747.99 425.782 9 2 -3 4 5929.98 441.516 59 2 3 4 5264.22 432.654 4 2 3 4 5801.10 406.368 56 2 -3 4 5960.89 458.316 52 -2 -3 -4 6064.45 435.917 58 -2 -3 -4 6033.32 469.895 8 2 -3 4 5702.33 434.534 53 -2 -3 -3 4864.56 398.006 8 2 -3 3 4381.48 354.618 59 -2 -3 -3 4721.76 374.637 58 2 3 3 5020.57 299.272 59 2 3 3 4463.28 386.345 5 2 3 3 4363.02 379.651 57 2 -3 3 5215.99 416.020 52 2 -3 3 4399.10 362.087 53 -2 -3 -2 3207.84 295.638 58 2 -3 2 3056.30 281.588 59 2 3 2 3133.50 306.502 57 -2 -3 -2 2858.68 291.376 8 2 3 2 3447.79 240.075 59 2 3 2 3111.60 310.518 5 2 -3 2 3205.88 302.645 53 2 -3 1 143525. 1971.94 53 2 3 1 145722. 1909.97 3 2 3 1 140732. 2014.80 5 2 3 1 144139. 2022.02 57 2 -3 1 142809. 1791.94 59 2 3 1 141310. 1937.78 7 -2 -3 -1 145713. 1968.08 58 -2 -3 -1 142502. 1981.32 8 2 -3 0 311.532 82.0543 59 2 -3 0 576.669 134.873 61 -2 3 0 351.935 66.9565 10 -2 3 0 548.441 106.278 56 2 -3 0 525.801 141.931 53 -2 -3 0 483.821 125.227 8 2 -3 0 384.974 63.8236 58 -2 3 0 564.116 89.4629 7 2 3 0 517.606 122.957 7 2 3 0 502.065 128.996 3 2 -3 -1 7730.04 450.941 53 2 -3 -1 6946.83 435.134 61 -2 3 1 7946.22 403.372 56 2 3 -1 7274.94 425.937 3 -2 3 1 7560.84 350.917 10 2 -3 -2 25065.5 834.049 61 2 3 -2 26041.5 714.810 2 -2 3 2 26029.2 719.382 10 -2 3 2 25837.9 785.503 56 2 -3 -2 25471.8 827.394 53 2 3 -2 25823.1 812.369 3 2 -3 -3 23.0884 54.3153 61 -2 3 3 9.33620 44.9148 10 2 3 -3-7.05661 39.1583 2 2 -3 -3 9.54262 62.1131 53 2 -3 -3-20.8223 36.2002 52 -2 3 3 112.725 55.1533 4 2 -3 -4 1403.24 207.554 61 -2 3 4 1881.58 246.625 56 2 3 -4 1596.32 197.492 2 2 3 -4 1278.68 200.011 6 -2 -3 4 1522.81 213.794 60 -2 3 4 1891.51 229.173 10 -2 3 5 3886.73 346.958 10 2 -3 -5 4099.62 299.872 2 2 -3 -5 3697.39 352.683 61 -2 3 5 4469.71 349.733 4 2 3 -5 4130.17 336.563 2 2 3 -5 3824.13 360.050 6 -2 -3 5 3682.12 327.855 60 -2 -3 6 7140.93 473.215 60 -2 3 6 6463.65 476.258 10 2 -3 -6 6059.72 393.869 2 2 -3 -6 6238.93 486.760 61 2 3 -6 6353.61 439.984 2 2 3 -6 6596.66 495.060 6 -2 -3 7 141.583 86.0265 60 2 3 -7 153.394 96.2076 6 -2 3 7 86.2636 79.5720 10 2 3 -7 21.0824 53.2839 2 2 -3 -7 175.602 93.6365 61 2 -3 -7 156.634 76.6266 2 -2 3 8 3477.34 395.551 10 2 -3 -8 3278.50 384.397 61 2 -3 -8 3539.76 347.363 2 2 3 -8 3314.73 364.409 2 -2 -3 8 2996.34 341.371 60 2 3 -8 3398.03 396.405 6 -2 -3 9 931.876 210.079 60 -2 3 9 1017.57 227.356 10 2 -3 -9 1240.25 260.004 61 2 3 -9 1034.13 231.246 6 2 -3 -9 1002.61 198.749 2 2 3 -9 885.669 206.179 2 -2 3 10 153.449 104.360 10 2 -3 -10 164.780 88.9801 2 -2 -3 10 160.623 78.1704 60 2 3 -10-171.510 115.531 2 2 -3 -10 24.6653 65.5925 61 2 3 -10 153.767 97.5103 6 -2 3 11 9709.39 774.369 10 2 -3 -11 9591.66 752.642 61 2 3 -11 8307.50 682.353 2 2 -3 -11 10113.9 713.877 2 2 3 -11 9082.29 744.528 6 -2 -3 11 10094.2 722.511 60 2 -3 -12 248.017 128.773 2 2 -3 -12 253.039 127.070 61 2 3 -12 235.245 128.333 6 2 3 -12-51.6135 81.5689 2 -2 3 13 570.379 52.6019 16 -2 -3 13 642.482 52.6559 13 -2 -3 13 602.068 51.4782 25 -2 3 13 480.987 47.9053 11 -2 3 13 554.329 51.8248 19 -2 -3 13 553.807 52.0381 27 -2 3 13 546.099 51.0568 17 -2 3 14 19884.5 306.337 16 -2 -3 14 20555.8 295.301 13 -2 3 14 20589.0 310.551 19 -2 3 14 20261.7 304.446 11 -2 -3 14 20484.2 302.673 27 -2 3 14 20067.7 307.533 17 -2 -3 14 20165.3 294.134 25 -2 3 15-2.23011 20.5415 11 -2 3 15-21.1439 23.7644 16 -2 -3 15-11.7105 27.0303 27 -2 -3 15 12.6639 19.5204 13 -2 3 15 2.05453 23.0150 19 -2 3 15 3.70448 20.0918 17 -2 3 16 1746.44 93.0741 16 -2 3 16 1759.16 91.9174 21 -2 -3 16 1820.45 89.5575 13 -2 -3 16 1841.00 94.7274 27 -2 3 16 1933.84 98.0065 19 -2 3 16 1954.18 95.6410 11 -2 3 16 1765.26 89.5307 18 -2 3 16 1780.79 94.1098 17 -2 -3 17 805.286 60.7141 49 -2 -3 17 880.396 60.9465 13 -2 -3 17 884.204 65.0402 27 -2 3 17 761.164 56.4107 18 -2 3 17 839.450 61.5870 21 -2 3 17 721.337 60.3621 17 -2 -3 18 441.157 46.0267 27 -2 3 18 511.460 46.5549 27 -2 3 18 419.782 44.1519 17 -2 -3 18 471.760 43.4672 49 -2 3 18 412.978 40.7112 21 -2 -3 19 571.526 46.4712 27 -2 -3 19 580.405 43.5380 49 -2 3 19 570.588 41.7110 21 -2 3 19 591.075 46.1397 27 -2 3 20 534.769 39.2007 27 -2 -3 20 519.990 40.5249 27 -2 -3 20 542.244 36.4264 49 -2 3 21 123.859 17.8207 27 -2 -3 21 119.638 18.5653 27 2 -4 18 261.972 26.1073 49 2 4 18 239.200 25.0007 27 2 4 18 228.354 23.4814 25 2 -4 17 35.4933 16.5462 49 -2 -4 -17-4.42389 16.4138 62 2 4 17 30.7824 16.8734 25 2 4 16-2.70591 17.0606 25 2 -4 16 2.08035 18.3966 25 2 4 16 23.8384 16.3381 17 2 -4 15 17.1941 23.1891 24 2 4 15 46.2198 22.5606 25 2 -4 15 18.7365 23.9833 25 2 4 15 19.3113 15.1598 19 2 4 15 29.1299 19.6578 20 2 4 14 3521.61 127.434 28 2 4 14 3664.89 124.616 19 2 4 14 3400.29 121.801 55 2 -4 14 3508.95 126.371 25 2 -4 14 3553.67 130.124 24 2 4 14 3359.03 123.643 42 2 4 14 3353.15 122.015 20 2 4 13 321.217 43.2347 28 2 -4 13 353.533 43.5003 26 2 4 13 312.868 42.4186 55 2 -4 13 340.385 43.8829 25 2 4 13 318.329 43.9211 42 2 4 13 283.253 42.0021 45 2 -4 13 339.802 44.1507 24 2 4 13 279.018 40.4760 20 2 4 13 324.060 41.6123 19 2 4 12 955.213 69.0153 28 2 -4 12 1005.63 70.8828 24 2 -4 12 1078.93 71.3079 26 -2 -4 -12 885.162 66.0142 22 2 4 12 932.096 67.1507 43 2 4 12 957.293 69.5701 42 2 -4 12 1023.07 70.3763 25 2 4 12 1032.64 69.9055 20 2 4 12 1076.88 73.1713 45 2 4 12 928.968 65.9764 55 2 -4 11 332.542 41.5764 25 2 -4 11 341.120 42.3615 26 2 4 11 293.178 39.0005 28 2 -4 11 351.807 42.8812 24 2 4 11 357.357 41.8738 43 2 4 11 373.669 45.4803 42 2 4 11 306.533 40.6316 45 2 4 11 292.183 37.8314 55 2 4 11 299.577 41.4878 31 -2 -4 -11 352.483 41.8826 22 2 4 10 28.9372 19.9429 28 2 -4 10 60.8134 26.0877 26 -2 -4 -10 53.3009 21.4857 22 2 4 10 67.1432 21.0199 43 2 -4 10 7.80746 19.0551 24 2 4 10 45.2706 21.6342 46 2 4 10 11.6961 18.7379 45 2 4 10 60.9831 21.3622 42 2 4 10 57.9122 21.1154 31 -2 -4 -9-261.742 145.286 58 2 4 9-68.2036 69.9786 10 2 4 8 7634.99 672.856 10 -2 -4 -8 8440.23 670.246 58 -2 4 -8 7934.86 628.582 1 2 4 8 7956.40 702.030 4 2 -4 8 9178.81 718.494 52 2 4 7 18581.4 1006.31 10 -2 -4 -7 18627.9 964.136 58 2 -4 7 18413.9 970.886 59 -2 4 -7 18636.1 901.207 1 2 -4 7 19101.2 996.762 52 2 4 7 17827.2 1004.63 4 2 4 6 1431.20 248.890 56 2 4 6 1310.22 255.347 10 -2 4 -6 1277.52 224.904 9 2 -4 6 1189.77 243.506 52 -2 -4 -6 1212.91 224.381 58 2 4 6 1166.61 255.006 4 2 -4 6 1262.54 243.576 59 2 4 5 24683.7 1076.68 5 -2 -4 -5 25609.3 1034.36 58 2 -4 5 21873.7 993.428 52 -2 4 -5 24645.8 953.361 9 2 4 5 23440.8 1047.39 4 2 4 5 23068.7 957.995 56 2 -4 5 23562.9 1001.96 53 2 -4 5 24428.9 998.188 59 2 4 5 22519.1 1009.29 10 2 4 4 1226.85 218.169 56 2 -4 4 1333.57 220.344 59 -2 -4 -4 1313.86 229.781 58 2 -4 4 1439.25 246.396 52 -2 -4 -4 1188.59 225.450 8 2 -4 4 1182.52 228.483 53 -2 4 -4 1110.36 201.839 9 2 4 4 795.062 197.993 5 2 4 3 8617.02 591.988 5 -2 -4 -3 9763.99 601.782 58 2 -4 3 9213.55 538.529 59 2 4 3 9598.36 609.451 57 2 -4 3 9897.74 613.512 53 2 -4 3 9166.60 603.514 52 -2 -4 -3 9336.86 597.347 8 2 -4 2 24870.1 955.013 52 2 4 2 22732.9 924.105 5 -2 -4 -2 23616.3 913.673 8 2 -4 2 22332.1 896.181 53 2 4 2 23237.7 915.947 57 -2 -4 -2 23522.8 910.159 58 2 -4 2 24274.6 824.697 59 2 4 1 54833.4 1407.94 5 2 -4 1 56283.5 1177.55 59 -2 -4 -1 60072.4 1413.71 8 -2 -4 -1 56173.8 1386.81 58 2 4 1 54877.6 1375.16 57 -2 4 -1 60921.4 1117.97 7 2 4 1 56507.3 1392.86 7 2 4 1 57470.2 1281.71 3 2 -4 1 58355.2 1415.25 52 2 -4 1 55926.8 1384.58 53 2 -4 0 26960.1 929.657 61 2 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1362.45 4 -2 4 5 2373.16 291.926 10 2 -4 -5 2655.98 333.100 61 -2 4 5 2309.69 305.944 56 2 -4 -5 2266.78 297.499 53 2 4 -5 2278.66 255.841 2 2 4 -5 2453.62 314.829 6 -2 4 5 2852.74 304.149 4 2 4 -6 665.271 179.087 6 2 -4 -6 725.445 186.384 61 2 4 -6 684.625 155.063 2 -2 -4 6 806.626 180.342 60 -2 4 6 651.451 171.998 10 -2 4 6 788.329 179.499 4 -2 -4 7 2562.39 308.430 60 -2 4 7 2474.34 331.523 10 2 -4 -7 2512.84 348.090 61 2 4 -7 2742.62 317.791 2 2 4 -7 2821.49 362.881 6 2 -4 -8 711.864 184.998 61 -2 -4 8 974.491 201.438 60 -2 4 8 936.865 222.374 10 2 4 -8 915.163 198.876 2 2 4 -8 1046.86 236.996 6 2 4 -9 1292.15 243.844 2 2 -4 -9 1412.39 287.679 61 -2 -4 9 1515.44 261.108 60 2 4 -9 1132.81 257.741 6 -2 4 9 1026.34 248.822 10 2 4 -10-85.0441 98.9416 6 2 4 -10 184.887 79.3088 2 2 -4 -10 66.2150 64.8486 61 -2 4 10 57.4699 78.9205 10 -2 4 11 42.2894 77.6197 10 2 -4 -11-259.078 140.361 61 2 4 -11-164.393 114.443 2 2 4 -11-235.776 145.819 6 -2 4 12 989.781 67.1934 16 -2 -4 12 962.023 65.9216 27 2 4 -12 777.263 235.177 2 -2 4 12 974.746 62.7496 45 -2 4 12 895.661 62.3749 20 -2 4 12 916.527 64.1413 19 -2 -4 12 975.119 63.3080 49 -2 4 12 957.547 65.9025 17 -2 4 13 2275.71 103.761 16 -2 -4 13 2189.52 99.5709 27 -2 -4 13 2159.90 96.3150 13 -2 -4 13 2212.10 97.6000 49 -2 4 13 2187.28 96.9122 45 -2 4 13 2295.95 104.730 19 -2 4 13 2103.18 98.4919 11 -2 4 13 2327.20 105.296 17 -2 4 14 347.153 46.8942 16 -2 -4 14 326.442 42.8164 49 -2 -4 14 311.499 42.8376 27 -2 4 14 378.484 46.7568 19 -2 -4 14 363.310 41.9174 13 -2 4 14 394.861 46.4270 11 -2 4 14 292.153 40.9856 17 -2 -4 15 11.1775 20.6192 13 -2 4 15 23.2802 21.8547 16 -2 -4 15 115.341 31.2836 49 -2 4 15 23.3010 21.4816 19 -2 -4 15 50.5747 23.8996 27 -2 4 15 58.6848 26.7572 11 -2 4 15 79.5878 27.6250 17 -2 4 16 1438.26 83.9062 16 -2 -4 16 1402.25 82.8066 27 -2 -4 16 1523.82 81.0063 49 -2 4 16 1450.40 82.6243 11 -2 -4 16 1560.70 80.0658 13 -2 4 16 1503.97 86.0449 19 -2 4 16 1613.58 85.4677 18 -2 4 16 1579.64 88.8771 17 -2 4 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404.174 4 3 5 4 2639.69 390.536 5 3 -5 4 2246.36 341.892 59 -3 -5 -4 2501.45 367.027 58 3 -5 4 2340.18 354.124 53 3 -5 4 2459.25 392.839 52 -3 5 -4 2165.73 328.844 9 -3 -5 -4 2077.95 342.899 8 3 5 4 1952.59 341.380 4 3 -5 3 1903.61 300.235 59 3 5 3 1522.76 287.184 57 3 -5 3 1770.41 314.472 53 3 5 3 1662.27 313.459 5 3 -5 3 1814.58 321.806 52 -3 -5 -3 1666.52 304.955 8 3 5 2 738.458 203.343 57 3 -5 2 851.085 213.561 53 3 -5 2 700.634 195.543 52 3 -5 2 922.981 195.922 59 -3 -5 -2 1005.11 225.507 8 3 5 2 1174.33 249.701 5 3 5 1 3395.27 419.896 5 3 -5 1 3586.55 365.770 59 3 5 1 3338.47 418.641 57 3 -5 1 3115.81 404.263 53 3 -5 1 3888.85 446.606 52 -3 -5 -1 3754.31 433.960 8 3 5 1 3646.36 405.287 3 3 5 0 5044.27 504.953 5 3 5 0 5110.18 503.226 57 3 -5 0 4992.38 497.072 53 3 -5 0 4910.46 485.714 52 3 5 0 5226.41 500.163 7 3 5 0 5737.99 502.251 3 -3 -5 0 4827.10 478.087 8 3 5 -1 16997.5 918.830 5 3 -5 -1 16354.3 894.268 53 3 -5 -1 17471.0 886.349 52 -3 -5 1 18209.9 920.622 8 3 5 -1 16690.1 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20.6963 21 -4 6 14 53.1801 24.9534 18 -4 6 14 35.7974 22.1819 11 -4 6 15 0.03451 18.7409 16 -4 -6 15 60.2881 24.7655 51 -4 -6 15 58.5652 22.5450 49 -4 6 15 30.3389 22.9787 21 -4 6 15 9.96195 19.2866 11 -4 6 15 23.5206 23.2878 18 -4 -6 16 697.387 49.6775 51 -4 -6 16 676.508 46.3700 49 -4 6 16 686.369 49.7401 12 -4 6 16 663.643 51.5956 21 -4 6 16 660.291 51.6352 11 -4 6 16 679.971 52.4548 18 -4 -6 17 258.068 29.9473 51 -4 -6 17 243.977 27.3956 49 -4 6 17 266.188 32.4545 21 -4 6 17 243.670 28.9381 12 -4 6 17 286.501 33.1857 18 -4 -6 18 309.072 27.4934 51 -4 6 18 287.169 25.8575 12 -4 6 18 311.475 30.9859 21 -4 6 18 290.935 28.7396 18 -4 -7 -14 16.5080 10.9666 62 -4 -7 -13 239.724 28.6591 62 4 7 13 269.104 28.0409 55 -4 -7 -13 174.706 21.7301 14 4 7 13 262.678 27.3701 20 -4 -7 -12 497.815 41.7089 62 4 7 12 451.534 40.1417 28 4 7 12 523.633 41.3723 55 4 7 12 509.738 40.4038 42 4 7 12 496.904 40.2285 20 4 7 11 815.030 56.3492 28 4 7 11 842.869 56.3792 55 -4 -7 -11 924.715 53.2450 48 4 7 11 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51.2727 13 -5 -2 16 451.211 43.8825 12 -5 2 16 563.475 52.4661 12 -5 2 16 487.109 51.6285 21 -5 2 16 476.266 49.7549 18 -5 -2 17 14.5383 21.4544 13 -5 2 17 24.8310 20.0383 21 -5 -2 17 40.5036 18.3310 12 -5 2 17 37.9868 22.5593 12 -5 -2 18 182.948 31.8341 13 -5 2 18 149.701 28.8819 21 -5 2 18 165.448 25.6438 12 -5 -2 19 156.755 26.7882 13 -5 2 19 108.256 22.6418 13 -5 2 19 109.321 19.2003 12 5 2 -19 101.985 20.7132 37 -5 -2 20-24.1211 16.3950 51 -5 -2 20-1.63051 12.6631 13 -5 2 20 12.2925 13.1480 13 -5 -3 -15 4.68247 11.1730 62 5 3 15 26.0838 13.4124 25 5 3 15 18.3241 12.0435 24 5 -3 14-14.0802 18.5345 26 5 3 14 16.1432 17.0371 25 5 -3 14 3.53920 13.0007 24 5 -3 13 524.115 44.9872 26 5 3 13 608.666 43.2130 26 5 -3 13 545.033 44.2001 24 5 3 13 555.732 46.8367 25 5 -3 12 56.6259 24.0269 26 5 3 12 100.740 23.4337 26 5 -3 12 101.082 24.8358 24 -5 -3 -12 76.1023 22.6442 22 5 3 11 456.980 42.8100 28 5 -3 11 463.394 48.2055 26 5 3 11 517.501 45.0655 55 5 3 11 511.997 47.2134 26 5 -3 11 506.229 48.1441 24 -5 -3 -11 504.295 46.3815 22 5 3 11 526.078 46.6483 43 5 3 10 93.7020 26.8745 28 5 -3 10 132.631 30.9025 26 5 3 10 126.114 29.9726 26 5 -3 10 158.747 31.3778 24 5 3 10 164.032 31.9007 55 5 3 10 160.213 29.1748 43 -5 -3 -10 148.120 31.1757 22 5 3 9 4981.61 142.387 28 5 -3 9 4869.19 146.821 26 5 3 9 4986.98 147.235 26 5 -3 9 4739.38 143.245 24 -5 -3 -9 4992.76 145.322 22 5 3 9 5052.97 142.616 43 5 3 9 5068.26 144.816 31 5 3 8 7828.87 180.146 28 5 -3 8 7268.12 177.937 26 5 -3 8 7442.75 178.509 24 5 -3 8 7563.91 180.903 23 -5 -3 -8 7892.93 181.467 22 5 3 8 7724.00 177.439 43 5 3 8 7811.67 186.127 26 5 3 8 7489.66 176.812 31 5 -3 7 605.970 53.8960 26 5 -3 7 681.120 58.8005 23 5 3 7 597.379 53.1170 46 -5 -3 -7 596.926 52.5654 22 5 3 7 599.256 50.7739 43 5 3 7 521.259 50.9937 33 5 3 7 683.443 55.9777 31 5 -3 6 1994.50 91.0707 26 5 -3 6 1988.40 92.0241 23 5 3 6 1875.82 89.9183 46 -5 -3 -6 2129.69 94.2286 22 5 3 6 2003.60 95.3211 41 5 3 6 1874.86 89.5851 33 5 3 6 1837.59 87.6431 31 5 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3 5 3 -3 1149.66 266.484 3 5 -3 -3 1470.60 281.172 59 5 3 -3 1134.10 242.786 59 5 -3 -3 1376.95 278.030 53 5 3 -3 1262.89 253.464 5 5 -3 -4 12913.6 827.844 59 5 3 -4 12342.4 798.880 5 5 -3 -4 13359.0 844.622 53 5 3 -4 13245.2 876.159 3 5 3 -5 11.1725 37.9774 3 5 -3 -5 55.3451 81.2948 59 5 3 -6-154.546 99.3542 3 5 -3 -6 122.496 107.654 59 5 -3 -6-41.4609 85.7348 53 5 -3 -7 1367.36 295.444 61 -5 3 7 1113.00 262.427 10 5 -3 -7 1321.46 281.570 59 5 3 -7 1370.26 294.488 3 5 -3 -7 977.774 250.179 53 5 -3 -8 4004.46 519.184 61 5 3 -8 4554.64 548.236 3 -5 3 8 3691.65 493.338 10 5 -3 -9 199.565 127.911 61 -5 -3 9 86.0133 119.420 60 -5 3 9 237.683 144.826 10 5 3 -9 1.23055 46.9264 3 -5 -3 10 2053.18 92.3000 13 -5 -3 10 1866.18 89.3175 12 -5 3 10 1981.11 93.1605 21 -5 3 10 1814.65 86.4022 11 -5 3 10 2060.63 95.0673 18 -5 -3 11 508.660 49.2864 13 -5 -3 11 528.640 51.5506 12 -5 3 11 584.012 53.3999 12 -5 3 11 531.148 51.3070 21 -5 3 11 556.930 51.3937 11 -5 3 11 499.407 49.7849 18 -5 -3 12 656.444 56.3925 13 -5 -3 12 599.465 54.6213 12 -5 3 12 636.401 55.7890 12 -5 3 12 699.331 59.4214 21 -5 3 12 658.346 56.5272 11 -5 3 12 613.045 56.3618 18 -5 -3 13 1040.62 70.9667 13 -5 -3 13 973.579 68.1611 12 -5 3 13 1173.24 74.7933 12 -5 3 13 1186.21 77.3597 21 -5 3 13 1254.48 77.8992 11 -5 3 13 1050.56 74.0114 18 -5 -3 14 2513.82 108.708 13 -5 -3 14 2535.73 105.316 12 -5 3 14 2631.39 108.339 12 -5 3 14 2559.11 111.936 21 -5 3 14 2462.66 110.583 18 -5 -3 15 3586.55 126.399 13 -5 -3 15 3432.55 118.359 12 -5 3 15 3293.22 118.622 12 -5 3 15 3406.69 127.002 21 -5 3 15 3257.33 123.163 18 -5 -3 16 47.3328 28.1379 13 -5 -3 16 74.6178 26.4436 12 -5 3 16 65.3972 26.8986 21 -5 3 16 67.1777 27.1408 12 -5 3 16 67.3151 26.6469 18 -5 -3 17 2094.82 90.4464 13 -5 3 17 2057.75 85.4477 12 -5 3 17 2154.03 92.9675 21 -5 3 17 2148.25 93.2839 18 -5 -3 18 44.0181 22.4825 13 -5 3 18 38.4104 19.5842 21 -5 3 18 35.8838 17.9893 12 -5 -3 19 347.421 32.3749 51 -5 3 19 338.821 31.5752 13 -5 3 19 347.609 29.1486 12 -5 3 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45.8265 24.5357 32 6 -2 2 3123.98 112.594 54 6 -2 2 3255.47 115.086 23 6 2 2 3309.60 114.566 23 6 2 2 3245.14 111.923 44 -6 -2 -2 3428.95 116.325 22 6 2 2 3368.23 115.174 41 6 2 2 3189.47 114.494 39 6 2 2 3471.60 117.633 36 6 2 2 3299.92 115.059 34 6 2 2 3390.63 113.888 33 6 2 2 3081.44 110.379 32 6 2 2 3309.69 112.514 30 6 2 1 108.563 24.2304 30 6 2 1 196.178 31.4269 29 6 -2 1 116.959 26.7792 54 6 -2 1 115.843 26.5192 23 6 2 1 161.571 32.5051 23 6 2 1 131.387 27.7240 44 -6 -2 -1 187.239 146.453 8 6 2 1 88.5965 22.7795 39 6 2 1 94.2712 24.5090 36 6 2 1 110.736 26.8337 34 6 2 1 127.915 27.8175 32 6 -2 0 551.135 222.381 59 6 2 0 547.052 193.662 59 -6 2 0 359.185 156.552 9 -6 -2 0 291.348 150.645 8 6 -2 -1 4725.51 562.805 59 6 2 -1 4693.32 548.283 59 -6 2 1 4290.81 527.749 9 -6 -2 1 4893.53 552.544 8 6 -2 -2 1669.42 341.234 59 6 2 -2 1869.11 357.477 59 -6 -2 2 2084.09 367.436 8 6 -2 -3 1451.50 313.229 59 6 2 -3 2000.35 380.004 59 6 -2 -4 322.887 149.896 59 6 2 -4 284.491 97.5144 3 6 2 -5 766.779 235.685 3 6 -2 -5 1299.48 309.546 59 6 2 -5 889.514 269.017 59 6 2 -6 27.5682 52.9111 3 6 -2 -6 42.0762 88.3851 59 -6 -2 7 3383.71 110.434 51 -6 -2 7 3573.67 119.543 12 -6 2 7 3327.87 112.681 12 -6 2 7 3536.83 118.520 21 6 2 -7 3192.83 114.914 40 6 2 -7 3581.05 119.711 37 6 2 -7 3463.85 117.195 35 -6 -2 8 230.778 31.6438 51 -6 -2 8 190.551 29.1985 13 6 2 -8 199.459 33.4802 40 -6 2 8 238.755 33.5640 21 -6 -2 8 241.724 35.1829 12 6 2 -8 235.847 36.5952 37 -6 2 8 183.151 31.8480 12 -6 2 8 255.547 34.9271 18 -6 -2 9 414.892 42.9225 51 -6 -2 9 396.355 42.6895 13 -6 2 9 388.719 44.3912 12 -6 2 9 486.480 47.2190 21 6 2 -9 496.070 50.1773 40 -6 -2 9 359.982 42.1141 12 6 2 -9 374.095 43.9896 37 -6 2 9 373.130 41.8186 18 -6 -2 10 98.4379 24.4367 51 -6 -2 10 107.504 26.5143 13 6 2 -10 117.667 31.9518 40 -6 2 10 66.8859 24.6883 21 -6 -2 10 74.3829 25.2606 12 6 2 -10 63.5444 23.1206 37 -6 2 10 62.9978 23.6668 12 -6 2 10 122.310 24.7489 18 -6 -2 11 35.5469 20.4642 51 -6 -2 11 105.626 25.8732 13 6 2 -11 80.8961 28.7656 40 -6 2 11 54.7199 23.7107 21 -6 -2 11 30.2215 23.6040 12 -6 2 11 49.2931 25.3699 12 -6 2 11 63.0669 22.3604 18 -6 -2 12 1938.70 92.3494 13 -6 -2 12 1822.27 91.7044 12 -6 2 12 1875.21 93.1051 12 -6 2 12 1792.30 93.7957 21 6 2 -12 1930.30 93.3834 40 -6 2 12 1871.07 94.5286 18 -6 -2 13 478.157 49.9594 13 -6 -2 13 485.832 49.6015 12 -6 2 13 486.797 50.3219 12 -6 2 13 461.076 49.7558 21 6 2 -13 536.388 51.9456 40 -6 2 13 449.828 50.9503 18 -6 -2 14 345.508 43.5837 13 -6 2 14 403.403 41.9794 13 -6 2 14 385.772 47.0438 21 6 2 -14 432.288 46.5156 40 -6 -2 14 335.526 43.7631 12 -6 2 14 338.991 44.8668 12 -6 2 14 427.944 46.0864 18 -6 -2 15 3312.73 116.733 13 -6 2 15 3400.37 112.171 13 -6 -2 15 3347.42 116.206 12 -6 2 15 3190.56 114.277 12 -6 2 15 3314.30 122.037 21 6 2 -15 3369.14 111.941 40 6 2 -15 3234.83 113.440 37 -6 -2 16 1890.75 86.1990 13 -6 2 16 1798.32 79.8183 13 -6 -2 16 1852.67 83.2850 12 -6 2 16 1687.71 80.4936 12 -6 2 16 1813.10 87.3190 21 6 2 -16 1778.88 82.6657 37 -6 -2 17 1574.41 71.8372 51 -6 -2 17 1599.78 74.3645 13 -6 2 17 1476.87 68.3779 13 -6 -2 17 1518.19 70.3141 12 -6 2 17 1555.10 72.8610 12 6 2 -17 1508.85 70.4717 37 -6 -2 18 188.627 26.6551 51 -6 -2 18 166.103 27.6073 13 -6 2 18 168.883 25.8010 13 -6 -2 18 169.393 24.1152 12 -6 2 18 123.358 22.8367 12 6 2 -18 163.280 25.0322 37 -6 -2 19 371.992 29.9832 51 -6 2 19 341.804 28.6565 13 -6 2 19 371.081 28.6987 12 6 2 -19 301.669 25.8950 37 -6 -3 -13 462.757 31.1823 62 6 3 13 463.618 29.2270 26 6 3 13 439.127 30.6094 25 6 -3 12 2033.82 74.2937 26 6 3 12 1998.65 70.0988 26 6 3 12 1944.07 71.9957 25 6 -3 12 1868.95 65.8729 24 6 -3 11 630.492 47.2926 26 6 3 11 586.205 43.8273 26 6 3 11 568.953 44.3193 25 6 -3 11 507.786 39.4621 24 -6 -3 -11 643.856 45.9708 22 6 -3 10 1922.04 83.8012 26 6 3 10 1964.73 84.7041 26 6 -3 10 1824.03 76.7273 24 -6 -3 -10 1850.85 79.8228 22 6 -3 9 49.2415 22.8748 26 6 3 9 21.1609 23.3804 26 -6 -3 -9 10.2379 21.1492 22 6 -3 8 3250.75 115.187 26 6 3 8 3392.29 121.764 26 6 -3 8 3555.26 121.526 23 -6 -3 -8 3708.10 121.885 22 6 3 8 3282.55 111.176 31 6 -3 7 899.423 63.7152 26 6 3 7 846.145 65.4982 26 6 -3 7 927.732 65.8095 23 -6 -3 -7 1011.42 66.8640 22 6 3 7 903.383 59.9710 43 6 3 7 947.739 62.5787 31 6 -3 6 24.1575 17.1191 26 6 3 6 52.0979 20.2332 43 -6 -3 -6 64.3488 24.7194 22 6 3 6 47.6567 26.7569 33 6 3 6 55.0847 20.6497 31 6 -3 5 132.956 31.2848 23 6 3 5 74.0958 25.0533 46 -6 -3 -5 106.127 29.1556 22 6 3 5 120.451 30.4655 33 6 3 5 112.313 26.1432 31 6 -3 4 3.14343 14.1449 26 6 -3 4 17.1811 21.3510 23 6 3 4 75.0649 26.2516 46 -6 -3 -4-19.4901 23.9468 22 6 3 4-26.6207 25.5230 41 6 3 4-0.48185 20.5098 33 6 3 4-2.32726 23.8225 32 6 3 4 17.2620 21.4025 30 6 -3 3 500.775 48.4193 54 6 -3 3 493.453 48.3284 23 6 3 3 512.138 46.0558 23 -6 -3 -3 595.237 53.0128 22 6 3 3 556.005 52.3813 41 6 3 3 506.070 49.2087 39 6 3 3 520.172 48.6342 33 6 3 3 507.811 49.3853 32 6 3 3 516.717 50.6600 30 6 3 2 4.69040 20.7181 30 6 -3 2-26.5096 27.7704 54 6 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1994.77 371.989 59 6 -3 -2 2326.78 97.5409 54 6 3 -2 2069.45 89.9022 44 6 3 -2 2163.50 93.8743 40 6 3 -2 2369.25 99.2023 39 6 3 -2 2273.31 95.2372 38 6 3 -2 2285.42 96.6113 36 6 3 -2 2321.04 95.9259 35 6 3 -2 2387.61 98.0132 34 6 3 -3 1532.77 79.3389 29 6 -3 -3 1228.74 291.089 59 6 3 -3 845.609 277.760 59 6 3 -3 1451.79 78.5477 40 6 3 -3 1428.37 76.0373 38 6 3 -3 1780.98 84.2541 37 6 3 -3 1983.45 88.3242 35 6 3 -3 1461.61 76.9193 34 6 3 -4 1564.48 80.2092 29 6 3 -4 1610.68 82.3560 40 6 3 -4 1365.41 74.1407 38 6 3 -4 1659.49 80.9716 37 6 3 -4 1487.89 77.4647 35 6 -3 -5 1685.10 347.553 53 -6 -3 5 1962.82 85.3166 51 -6 -3 5 2046.06 89.7247 12 6 3 -5 1880.20 90.6302 40 6 3 -5 1730.18 84.7856 38 6 3 -5 1956.45 89.8660 37 6 3 -5 1720.08 84.1210 35 -6 -3 6 9367.07 185.196 51 -6 -3 6 9262.82 192.373 12 6 3 -6 8960.64 193.214 40 6 3 -6 9344.74 193.856 37 6 3 -6 8853.88 187.492 35 -6 -3 7 219.972 36.1036 51 6 3 -7 250.667 41.7209 40 -6 -3 7 236.460 35.9612 12 6 3 -7 248.840 38.0626 37 -6 3 7 176.528 29.8043 12 6 3 -7 188.986 35.2485 35 -6 -3 8 8133.50 179.792 51 -6 -3 8 8460.10 188.998 12 -6 3 8 8252.37 182.408 12 -6 3 8 8669.10 188.984 21 6 3 -8 7956.72 187.109 40 6 3 -8 7850.38 183.677 37 6 3 -8 8033.92 183.263 35 -6 3 8 8673.62 186.879 18 -6 -3 9 36.9428 23.0685 51 6 3 -9-27.0374 25.4662 40 -6 3 9 67.0469 23.7740 21 -6 -3 9 79.3889 29.1212 12 6 3 -9 47.0850 27.0523 37 -6 3 9 29.5271 21.1974 12 -6 3 9 2.26937 19.0833 18 -6 -3 10 12395.2 223.801 51 -6 -3 10 12670.3 231.651 13 -6 -3 10 12572.4 234.323 12 -6 3 10 11788.7 226.188 12 -6 3 10 12276.7 234.227 21 6 3 -10 11735.7 228.244 40 6 3 -10 12428.1 232.044 37 -6 3 10 12608.9 234.741 18 -6 -3 11 803.275 63.0153 51 -6 -3 11 909.916 65.3938 13 -6 -3 11 800.664 62.7754 12 -6 3 11 804.383 63.9507 12 -6 3 11 767.973 61.6230 21 -6 3 11 719.416 60.6497 18 -6 -3 12 6988.26 171.529 51 -6 -3 12 7058.64 176.719 13 -6 -3 12 6849.50 174.271 12 -6 3 12 7111.60 175.872 12 -6 3 12 6861.35 177.157 21 -6 3 12 7211.04 180.597 18 -6 -3 13 4575.60 136.831 51 -6 -3 13 4762.74 143.239 13 -6 -3 13 4625.91 141.772 12 -6 3 13 4410.70 139.425 12 -6 3 13 4580.61 145.809 21 -6 3 13 4458.38 142.579 18 -6 -3 14 2147.76 93.9387 51 -6 -3 14 1907.91 91.6886 13 -6 -3 14 1844.62 89.8407 12 -6 3 14 1993.61 92.2089 12 -6 3 14 1958.06 94.5441 21 6 3 -14 1981.91 92.1042 40 -6 3 14 2015.19 95.4855 18 -6 -3 15 503.460 51.1441 51 -6 -3 15 508.847 48.7870 13 -6 -3 15 419.785 44.1118 12 -6 3 15 438.781 48.2138 12 -6 3 15 500.294 51.0369 21 6 3 -15 452.337 45.8755 40 -6 3 15 526.416 51.3425 18 -6 -3 16 744.588 53.9261 51 -6 -3 16 699.561 54.8719 13 -6 3 16 577.674 44.5644 13 -6 -3 16 670.552 50.9150 12 -6 3 16 602.794 49.2994 12 -6 3 16 677.193 55.3130 21 6 3 -16 668.854 49.3983 40 6 3 -16 656.367 52.6598 37 -6 -3 17 30.4581 19.8536 51 -6 3 17-8.00824 18.4399 13 6 3 -17 66.9854 20.2051 40 -6 -3 17 29.1609 17.1109 12 -6 3 17 50.5565 20.9394 21 -6 3 17 53.6740 20.9169 12 6 3 -17 28.1661 19.8998 37 -6 -3 18 1.52987 15.4388 51 -6 3 18 8.84678 14.6790 13 -6 -3 18-29.4323 14.4547 12 -6 3 18 3.14042 14.5362 12 6 3 -18-13.0165 18.8970 37 -6 -3 19 12.5217 12.4644 51 -6 3 19 8.49736 11.8994 12 6 3 -19 44.1329 14.6604 37 6 3 -19 4.12865 13.5974 35 -6 -4 -12 71.9757 17.3640 62 6 4 12 61.7699 14.1539 26 6 4 12 67.2615 17.1553 25 -6 -4 -11 317.415 31.4935 62 6 -4 11 313.254 32.1350 26 6 4 11 330.705 32.6387 26 6 4 11 351.553 35.2989 25 -6 -4 -11 347.054 34.5145 22 -6 -4 -10 449.437 40.3114 62 6 -4 10 482.530 40.9033 26 6 4 10 430.017 36.3569 55 6 4 10 496.634 42.1295 26 -6 -4 -10 502.966 43.4932 22 6 4 10 437.447 36.7873 43 -6 -4 -9 16.1734 17.4662 62 6 4 9-6.18583 16.5671 55 6 -4 9 0.58878 18.1727 26 6 4 9-3.37329 20.7923 26 6 4 9 12.2433 15.5376 43 -6 -4 -9-5.98164 22.1675 22 6 4 9-13.8081 17.9187 31 6 -4 8 442.503 43.1391 26 6 4 8 436.239 46.3702 26 -6 -4 -8 407.777 44.8488 22 6 4 8 465.609 43.5950 43 6 4 8 460.511 44.1873 31 6 -4 7 2380.80 96.6492 26 6 4 7 2397.35 103.205 26 6 -4 7 2437.44 101.561 23 -6 -4 -7 2483.56 102.823 22 6 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8 99.0122 25.5782 51 6 4 -8 144.003 35.2469 40 -6 -4 8 78.2087 24.5006 12 6 4 -8 155.741 34.5588 37 -6 4 8 186.212 34.7595 12 6 4 -8 84.3704 26.8852 35 -6 -4 9 515.400 50.0479 51 -6 -4 9 493.974 51.3793 12 -6 4 9 517.440 51.2188 12 -6 4 9 468.929 46.5498 21 6 4 -9 569.248 57.4331 40 6 4 -9 463.211 49.9187 37 6 4 -9 485.353 48.5699 35 -6 4 9 472.270 45.9206 18 -6 -4 10 606.142 54.2445 51 -6 -4 10 563.462 53.1662 12 -6 4 10 679.214 58.1674 12 -6 4 10 685.743 56.8460 21 6 4 -10 569.377 55.9557 37 6 4 -10 652.834 58.0208 35 -6 4 10 665.750 55.6772 18 -6 -4 11 662.598 55.7993 51 -6 -4 11 731.564 61.1688 12 -6 4 11 729.483 60.9800 12 -6 4 11 786.286 60.8359 21 -6 4 11 760.339 60.1434 18 -6 -4 12 481.332 48.8569 51 -6 -4 12 453.721 48.6649 12 -6 4 12 582.958 52.7906 12 -6 4 12 513.156 51.1895 21 -6 4 12 545.955 52.9092 18 -6 -4 13 44.9301 24.5955 51 -6 -4 13 98.2095 29.3005 12 -6 4 13 83.7384 25.9176 21 -6 4 13 61.9214 24.2450 12 -6 4 13 70.3110 27.8972 18 -6 -4 14 53.8810 26.4126 51 -6 -4 14 37.0765 22.3682 12 -6 4 14 28.5637 25.0792 21 -6 4 14 29.2606 24.5155 12 -6 4 14 35.8309 23.5331 18 -6 -4 15 13.1281 20.2289 51 -6 -4 15 1.05014 19.3514 12 6 4 -15 44.0324 25.0168 40 -6 4 15 21.0458 20.9694 21 -6 4 15 10.8685 19.9623 12 -6 4 15 3.10360 18.1730 18 -6 -4 16 102.812 26.4200 51 -6 -4 16 99.9968 23.9937 12 6 4 -16 76.0520 24.6674 40 -6 4 16 90.2234 24.9504 21 6 4 -16 120.072 29.0391 37 -6 4 16 99.3718 28.6201 12 -6 4 16 98.7568 24.1379 18 -6 -4 17 63.3993 20.4576 51 -6 -4 17 39.3704 15.4150 12 6 4 -17 21.8442 17.6250 40 -6 4 17 42.2567 18.5369 21 -6 4 17 40.4468 18.5434 12 6 4 -17 27.8554 19.1823 37 6 4 -17 31.4498 18.2249 35 -6 -4 18 36.8755 17.0925 51 6 4 -18 64.2492 15.5328 40 -6 4 18 48.9967 16.0196 12 6 4 -18 12.9721 16.4171 37 6 4 -18 27.1841 14.8732 35 -6 -5 -12 2.48275 9.96743 62 6 5 12-11.5811 12.4592 25 -6 -5 -11 214.558 24.3446 62 6 5 11 214.863 22.9139 55 -6 -5 -10 189.561 27.2613 62 6 5 10 189.905 24.9055 28 6 5 10 177.276 24.8092 55 6 5 10 145.817 24.0423 26 6 5 10 172.556 23.9595 43 -6 -5 -10 185.433 27.2220 22 -6 -5 -9 119.163 24.8160 62 6 5 9 98.0141 20.4813 28 6 -5 9 83.8302 19.4232 26 6 5 9 96.1158 21.8982 55 6 5 9 112.529 24.0702 26 6 5 9 94.5174 23.2894 43 -6 -5 -9 69.9750 24.5650 22 6 5 9 82.6304 22.0836 31 -6 -5 -8 297.607 35.7223 62 6 5 8 350.916 36.9041 28 6 -5 8 320.497 34.5942 26 6 5 8 398.571 40.9775 26 6 5 8 365.083 39.3162 43 -6 -5 -8 344.389 39.8429 22 6 5 8 333.903 37.7163 31 -6 -5 -7 262.010 33.6164 62 6 5 7 282.939 36.1686 28 6 5 7 234.164 35.3500 26 6 5 7 262.498 36.0744 43 -6 -5 -7 261.324 38.2081 22 6 5 7 250.759 35.0295 31 -6 -5 -6 462.368 44.1886 62 6 5 6 469.047 49.3538 46 -6 -5 -6 494.433 49.5083 22 6 5 6 454.749 47.5708 33 6 5 6 507.955 49.7998 31 -6 -5 -5 191.971 31.5243 62 6 -5 5 241.416 38.9513 23 6 5 5 164.553 34.1176 46 -6 -5 -5 185.260 38.1548 22 6 5 5 172.110 36.8756 41 6 5 5 150.916 34.2338 33 6 5 5 237.606 36.6728 31 -6 -5 -4 1979.63 87.2444 62 6 -5 4 2148.95 95.8485 23 -6 -5 -4 2327.24 93.6605 47 6 5 4 2048.42 96.2807 46 -6 -5 -4 2043.35 95.1919 22 6 5 4 1981.70 97.9340 41 6 5 4 2135.94 97.5520 33 6 5 4 1868.09 91.6585 32 6 5 4 2008.58 93.6440 30 6 -5 3 451.974 42.1406 54 6 -5 3 631.343 54.5668 23 -6 -5 -3 623.170 52.2033 47 6 5 3 608.606 55.1483 46 -6 -5 -3 566.448 52.6841 22 6 5 3 596.232 57.0332 41 6 5 3 461.773 47.9799 39 6 5 3 516.498 52.5634 33 6 5 3 561.574 55.2827 32 6 5 3 525.927 50.8084 30 6 5 2 351.255 43.8225 30 6 -5 2 284.748 33.8506 54 6 -5 2 340.501 41.9255 23 -6 -5 -2 315.058 38.0375 47 6 5 2 366.851 46.7077 46 -6 -5 -2 384.430 43.7557 22 6 5 2 331.640 45.4013 41 6 5 2 253.378 37.2987 39 6 5 2 244.187 33.8373 36 6 5 2 223.230 32.9777 34 6 5 2 322.454 45.4343 33 6 5 2 341.422 44.4971 32 6 5 1 2475.27 103.125 29 6 -5 1 2464.43 100.044 54 6 -5 1 2551.02 101.878 23 -6 -5 -1 2641.52 102.818 47 6 5 1 2431.99 101.262 44 -6 -5 -1 2362.99 101.890 22 6 5 1 2590.17 111.056 41 6 5 1 2491.25 107.820 39 6 5 1 2481.41 103.293 36 6 5 1 2441.64 101.256 34 6 5 1 2484.58 106.369 32 6 5 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8 33.2750 17.3287 43 6 6 8 71.6802 21.5154 31 -6 -6 -7 501.430 41.6699 62 6 6 7 546.220 46.5294 28 6 6 7 542.137 45.5386 26 6 6 7 503.368 45.9255 46 -6 -6 -7 483.506 43.9894 22 6 6 7 548.819 46.8145 43 6 6 7 482.563 45.1595 31 -6 -6 -6 70.4653 20.5102 62 -6 -6 -6 86.1951 22.6465 48 6 6 6 102.581 29.3132 46 6 6 6 86.1731 26.4182 43 -6 -6 -6 64.9858 22.5001 22 6 6 6 111.365 28.8967 33 6 6 6 70.4178 23.3878 31 -6 -6 -5 99.1792 25.0468 62 -6 -6 -5 98.8338 25.3245 48 6 6 5 121.952 31.6491 46 -6 -6 -5 106.894 31.1987 22 6 6 5 98.4359 34.0901 41 6 6 5 149.929 33.1108 33 6 6 5 142.814 32.3723 31 -6 -6 -4 530.236 47.4039 62 6 6 4 525.705 51.7191 46 -6 -6 -4 510.776 50.9639 22 6 6 4 567.262 57.4035 41 6 6 4 507.492 50.3876 33 6 6 4 460.171 48.3418 32 6 -6 3 5838.44 150.390 23 -6 -6 -3 5904.18 150.695 47 6 6 3 5680.32 158.287 46 -6 -6 -3 5613.42 154.095 22 6 6 3 5686.97 161.419 41 6 6 3 5834.85 158.215 39 6 6 3 5586.34 156.355 33 6 6 3 5697.70 154.982 32 6 6 3 5718.88 154.732 30 6 -6 2 4823.46 136.371 23 -6 -6 -2 4769.11 138.058 47 6 6 2 4716.06 144.473 46 -6 -6 -2 4596.66 140.423 22 6 6 2 4789.64 148.985 41 6 6 2 4961.03 146.674 39 6 6 2 5100.92 143.838 36 6 6 2 4818.20 144.654 33 6 6 2 4756.47 142.987 32 6 6 2 4661.71 140.494 30 -6 -6 -1 10292.7 201.228 47 6 6 1 10094.6 202.490 44 -6 -6 -1 9798.25 200.813 22 6 6 1 9953.04 213.359 41 6 6 1 9946.54 208.804 39 6 6 1 9954.67 203.896 36 6 6 1 10244.3 200.557 34 6 6 1 9642.69 203.197 32 6 6 1 9975.50 205.764 30 6 6 0 1293.83 79.8018 29 6 -6 0 1360.29 75.0816 54 -6 -6 0 1301.06 79.1039 47 6 6 0 1334.78 79.1590 44 -6 -6 0 1346.17 77.7501 22 6 6 0 1395.64 88.0842 41 6 6 0 1464.83 86.5043 39 6 6 0 1236.94 76.4253 36 6 6 0 1123.04 71.6270 34 6 6 0 1366.03 82.5245 32 6 6 0 1419.48 83.0676 30 6 6 -1 30508.9 349.757 29 6 -6 -1 29166.0 339.958 54 -6 -6 1 29462.3 345.773 47 6 6 -1 29877.1 348.955 44 -6 -6 1 29045.9 345.156 22 6 6 -1 29535.5 362.682 39 6 6 -1 29896.6 355.003 36 6 6 -1 30009.0 348.460 34 6 6 -1 29143.6 354.059 32 6 6 -1 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99.4965 22 7 -1 7 1176.76 69.5968 26 7 1 7 1186.78 72.9495 26 7 -1 7 1289.09 71.7696 23 7 1 7 1304.59 68.5571 23 -7 -1 -7 1293.10 67.1788 22 7 -1 6 37.9206 21.6491 26 7 1 6 63.9211 27.4993 26 7 -1 6 58.2776 27.5009 23 7 1 6 60.5128 25.4406 23 -7 -1 -6 22.9498 19.0520 22 7 -1 5 128.444 29.5651 26 7 1 5 137.942 32.6233 26 7 -1 5 127.469 31.7260 23 7 1 5 163.243 31.8417 23 -7 -1 -5 174.484 30.6705 22 7 -1 4 1283.99 75.4691 26 7 1 4 1279.80 78.1957 26 7 -1 4 1286.87 76.7714 23 7 1 4 1364.62 76.1876 23 -7 -1 -4 1358.32 75.1349 22 7 -1 3-6.09504 17.1825 26 7 1 3 10.7809 18.8284 26 7 -1 3-14.8588 22.1633 23 7 1 3 5.72591 24.2481 23 -7 -1 -3-12.4260 21.4529 22 7 -1 2 9.66294 22.5506 54 7 -1 2 12.1618 17.4487 26 7 -1 2 31.1994 24.0937 23 7 1 2 22.5608 21.8002 23 -7 -1 -2 13.8798 18.7323 22 7 1 2 18.0059 19.2579 32 7 1 2 11.8173 17.1048 30 7 1 1 179.170 30.8005 30 7 -1 1 120.691 32.2861 54 7 -1 1 73.4625 26.2091 23 7 1 1 162.641 33.1657 23 7 1 1 140.550 28.6218 44 7 1 1 165.352 31.7514 32 7 1 0 73.5289 23.0245 30 7 1 0 78.0204 28.8763 54 7 -1 0 133.103 31.3176 54 7 -1 0 27.7576 24.7555 23 7 1 0 149.104 33.7070 23 7 1 0 61.7162 24.4135 44 7 1 0 40.1366 21.4327 32 7 1 -1 719.801 57.4918 29 7 1 -1 762.859 58.9521 54 7 -1 -1 766.597 59.8287 54 7 -1 -1 666.887 56.8320 23 7 1 -1 776.592 62.8038 23 7 1 -1 678.693 53.4740 44 7 1 -1 735.087 58.3047 36 7 1 -1 730.214 53.7560 32 7 1 -1 799.817 55.9053 30 7 1 -2 953.449 64.4004 29 7 1 -2 1251.66 72.3630 54 7 -1 -2 1078.00 70.1377 54 7 -1 -2 1151.79 72.9046 23 7 1 -2 1022.07 64.8747 44 7 1 -2 1107.59 67.3931 39 7 1 -2 1010.19 65.5713 36 7 1 -2 1005.23 65.7032 34 7 1 -2 1024.30 63.6756 30 7 1 -3 840.582 60.9274 29 7 1 -3 905.587 61.2425 54 7 -1 -3 873.946 63.3462 54 7 -1 -3 835.041 61.9248 23 7 1 -3 834.252 59.3229 44 7 1 -3 835.527 61.4168 38 7 1 -3 891.990 61.7644 36 7 1 -3 830.550 60.1200 34 7 1 -4 96.1854 26.0317 29 7 1 -4 116.864 27.7289 54 7 -1 -4 113.004 31.7230 54 7 -1 -4 129.587 30.1020 23 7 1 -4 109.949 29.3212 38 7 1 -4 142.086 28.4371 36 7 -1 -4 105.770 26.8533 35 7 1 -4 111.076 28.5942 34 7 1 -5 5804.74 154.775 29 7 -1 -5 5904.19 158.817 54 7 1 -5 6006.18 157.807 38 7 1 -5 5788.33 150.177 36 7 -1 -5 5941.79 153.315 35 7 1 -5 5847.52 155.933 35 7 1 -5 5823.16 153.913 34 7 1 -6 4843.30 140.933 29 -7 -1 6 5145.33 142.065 12 7 1 -6 5007.43 147.189 40 7 1 -6 4818.50 141.450 38 7 1 -6 4695.62 144.279 37 7 -1 -6 5101.12 141.881 35 7 1 -6 4697.52 142.248 35 7 1 -6 4885.94 140.580 34 7 1 -7 1155.95 69.9490 29 -7 -1 7 1202.73 71.7979 12 7 1 -7 1113.07 72.1564 40 7 1 -7 1245.82 74.3957 38 7 1 -7 1255.85 75.8113 37 7 -1 -7 1123.75 68.9331 35 7 1 -7 1137.96 72.4228 35 7 1 -7 1180.13 71.7158 34 7 1 -8 2378.89 99.5366 29 -7 -1 8 2718.79 107.247 12 -7 1 8 2700.82 104.589 12 7 1 -8 2469.18 104.563 40 7 1 -8 2518.03 105.523 38 7 -1 -8 2551.00 103.879 37 7 1 -8 2390.56 103.742 37 7 -1 -8 2404.12 100.128 35 7 1 -8 2531.81 106.330 35 7 1 -9 254.085 39.7841 40 -7 -1 9 209.060 35.3170 12 7 1 -9 198.363 34.5150 38 -7 1 9 252.946 37.6177 12 7 -1 -9 233.606 37.2294 37 7 1 -9 247.574 40.1063 37 7 -1 -9 236.515 33.9678 35 7 1 -9 248.340 38.6358 35 7 1 -10 30.5182 23.3687 40 -7 -1 10 56.3325 24.1619 12 7 1 -10 29.5341 22.6496 38 -7 1 10 48.8236 22.6224 12 7 -1 -10 30.7397 23.3968 37 7 1 -10 30.0183 24.8555 37 7 -1 -10 30.9131 22.4972 35 7 1 -10 23.2975 22.0645 35 -7 -1 11 705.058 56.4294 12 -7 1 11 696.217 58.4827 12 7 1 -11 793.536 60.3807 40 7 -1 -11 691.833 54.1948 37 7 1 -11 699.766 61.0639 37 7 -1 -11 725.980 56.8515 35 7 1 -11 782.009 60.5903 35 -7 -1 12 606.141 49.6260 13 -7 -1 12 491.624 49.1401 12 -7 1 12 475.904 47.7196 12 7 1 -12 561.669 50.3478 40 7 -1 -12 544.693 47.7008 37 7 1 -12 592.004 53.9105 37 7 -1 -12 610.371 51.9446 35 7 1 -12 535.679 53.6894 35 -7 -1 13 33.3550 20.0756 13 7 1 -13 36.5477 23.1582 40 -7 -1 13 81.7532 27.2122 12 -7 1 13 72.3360 27.9205 12 7 1 -13 55.0156 27.9118 37 7 -1 -13 69.4479 27.0993 35 -7 -1 14 3507.25 106.927 51 -7 -1 14 3499.63 113.207 13 -7 -1 14 3181.35 113.178 12 -7 1 14 3500.09 116.764 12 7 1 -14 3348.56 112.677 37 7 -1 -14 3456.06 111.106 35 -7 -1 15 6.99607 17.0258 51 -7 -1 15 14.4881 18.5016 13 -7 -1 15-16.5078 22.4256 12 -7 1 15 13.4911 21.1401 12 7 1 -15 21.5940 21.0109 37 7 -1 -15 27.0019 18.9483 35 -7 -1 16 2330.78 79.0408 51 -7 -1 16 2232.30 82.6509 13 -7 -1 16 2199.70 84.4100 12 -7 1 16 2236.23 85.3500 12 7 1 -16 2263.64 80.4573 37 7 -1 -16 2159.59 78.6692 35 7 1 -16 2227.86 84.4808 35 -7 -1 17 305.443 28.6119 51 -7 1 17 305.414 29.4343 13 -7 -1 17 288.839 31.1855 12 -7 1 17 323.624 32.0839 12 7 1 -17 308.857 30.1637 38 7 1 -17 316.447 29.3249 37 7 -1 -17 283.296 28.1053 35 7 1 -17 306.107 31.7796 35 -7 -1 18 52.2931 13.6390 51 -7 1 18 24.0360 13.0969 13 -7 -1 18 12.1656 13.1909 12 -7 1 18 40.4981 16.2513 12 7 1 -18 10.6055 11.5891 38 7 -1 -18-5.81940 12.8017 35 7 1 -18-2.51684 14.5358 35 7 -2 11 5.89410 14.3486 26 7 2 11 75.8157 17.3900 26 7 -2 10 339.673 32.4660 26 7 2 10 348.441 33.7016 26 -7 -2 -10 314.762 28.1534 22 7 -2 9 1242.46 62.5934 26 7 2 9 1245.37 65.3241 26 -7 -2 -9 1249.18 59.4358 22 7 -2 8 630.874 48.2068 26 7 2 8 729.846 54.2417 26 7 -2 8 781.043 54.1729 23 -7 -2 -8 659.600 48.2611 22 7 -2 7 4.62770 20.5319 26 7 2 7-1.92785 24.2436 26 7 -2 7 35.5089 27.5691 23 -7 -2 -7 26.0654 19.0180 22 7 -2 6 24.5837 19.4330 26 7 2 6 28.3425 26.4110 26 7 -2 6 42.4441 27.5430 23 7 2 6 54.6836 21.9554 23 -7 -2 -6 27.6909 22.5363 22 7 -2 5 455.808 45.7786 26 7 2 5 519.257 52.4828 26 7 -2 5 519.598 51.4079 23 7 2 5 523.646 48.5667 23 -7 -2 -5 479.368 47.0450 22 7 -2 4 56.0525 21.4264 26 7 2 4 45.7714 24.0550 26 7 -2 4 12.5804 25.3468 23 7 2 4 20.9830 19.6998 23 -7 -2 -4 18.0129 19.5776 22 7 2 4 69.1226 25.5232 33 7 -2 3 15.5162 15.4798 26 7 -2 3 3.51964 22.7716 23 7 2 3 14.2980 21.3304 23 -7 -2 -3-3.52041 19.7586 22 7 2 3 26.7344 19.3313 33 7 -2 2 1724.39 88.1923 54 7 -2 2 1705.97 87.9617 23 7 2 2 1929.92 91.2747 23 -7 -2 -2 1755.27 88.5315 22 7 2 2 1921.60 89.3096 33 7 2 2 1829.78 89.0806 32 7 2 2 1921.72 88.5251 30 7 2 1 216.693 35.5159 30 7 -2 1 244.924 39.0322 54 7 -2 1 247.976 38.2989 23 7 2 1 250.161 39.5129 23 7 2 1 270.187 39.1594 44 -7 -2 -1 232.782 35.5194 22 7 2 1 267.275 35.9475 33 7 2 1 257.133 37.4097 32 7 -2 0 4124.40 132.938 54 7 -2 0 4072.06 132.702 23 7 2 0 4294.11 137.605 23 7 2 0 3903.36 128.273 44 7 2 0 4086.47 132.380 39 7 2 0 3986.95 131.127 36 7 2 0 4034.95 131.463 34 7 2 0 4204.58 128.635 33 7 2 0 4147.89 131.012 32 7 2 0 4306.39 132.017 30 7 2 -1 958.607 66.6247 29 7 -2 -1 940.964 65.9434 54 7 -2 -1 836.221 62.8135 23 7 2 -1 935.459 67.6008 23 7 2 -1 811.448 60.5918 44 7 2 -1 1007.66 68.0865 39 7 2 -1 863.252 62.9040 36 7 2 -1 936.304 66.6787 34 7 2 -1 901.604 62.4245 32 7 2 -1 945.793 63.8844 30 7 2 -2 786.681 60.3070 29 7 2 -2 801.391 57.3709 54 7 -2 -2 764.441 59.9313 54 7 -2 -2 783.711 59.7979 23 7 2 -2 634.723 53.4926 44 7 2 -2 857.912 61.9018 39 7 2 -2 735.998 57.9810 36 7 2 -2 832.990 61.2935 34 7 2 -2 790.589 59.5180 32 7 2 -2 719.321 54.9605 30 7 2 -3 156.242 31.7821 29 7 -2 -3 136.177 31.8514 54 7 -2 -3 147.874 29.6258 23 7 2 -3 159.122 35.5701 44 7 2 -3 138.319 29.4754 39 7 2 -3 136.404 32.7346 38 7 2 -3 130.500 31.6110 36 7 2 -3 138.204 30.7588 34 7 2 -3 161.439 30.9377 32 7 2 -4 482.239 48.5924 29 7 -2 -4 451.404 47.1109 54 7 -2 -4 451.223 45.3544 23 7 2 -4 501.084 47.4705 39 7 2 -4 354.005 43.3749 38 7 2 -4 475.452 48.2153 36 7 2 -4 429.390 48.2023 35 7 2 -4 421.243 46.8877 34 7 2 -5 86.8346 29.2447 29 7 -2 -5 72.5917 24.0069 23 7 2 -5 54.5803 27.5113 40 7 2 -5 105.465 28.4127 38 7 2 -5 110.622 31.1055 37 7 2 -5 103.142 30.3923 36 7 2 -5 99.6654 29.1186 35 7 2 -5 54.6849 26.1667 34 7 2 -6 720.505 58.7119 29 7 -2 -6 871.946 60.7979 23 -7 -2 6 698.300 54.2723 12 7 2 -6 756.305 61.7236 40 7 2 -6 692.428 58.1811 38 7 2 -6 771.335 60.8181 37 7 2 -6 740.781 57.7248 36 7 2 -6 725.943 60.1308 35 7 2 -6 775.840 61.1763 34 7 2 -7 597.969 54.5674 29 -7 -2 7 651.455 55.2754 12 7 2 -7 574.570 54.9472 40 7 2 -7 616.643 56.1868 38 7 2 -7 591.072 56.8353 37 7 2 -7 556.356 54.0860 35 -7 -2 8 495.107 50.1653 12 -7 2 8 422.559 45.8515 12 7 2 -8 433.308 49.8617 40 7 2 -8 450.035 48.7174 38 7 2 -8 389.005 46.8447 37 -7 -2 9 3531.34 116.783 51 -7 -2 9 3378.67 121.441 12 -7 2 9 3453.75 119.585 12 7 2 -9 3141.52 119.799 40 7 2 -9 3143.96 118.585 38 7 2 -9 3283.78 121.566 37 7 2 -9 3056.28 117.709 35 -7 -2 10 1297.84 71.7263 51 -7 -2 10 1228.82 76.6893 12 -7 2 10 1280.20 75.5285 12 7 2 -10 1188.91 75.9483 40 7 2 -10 1112.71 74.7550 37 7 2 -10 1120.24 73.6456 35 -7 -2 11 3793.89 120.884 51 -7 -2 11 3462.57 123.958 12 -7 2 11 3701.78 124.886 12 7 2 -11 3407.20 122.432 40 7 2 -11 3436.96 125.028 37 7 2 -11 3633.75 125.074 35 -7 -2 12 146.464 30.1631 51 7 2 -12 151.668 35.2377 40 -7 -2 12 193.379 35.8904 12 -7 2 12 168.260 32.0213 12 7 2 -12 183.056 35.9117 37 7 -2 -12 158.836 28.0957 35 7 2 -12 173.634 36.9015 35 -7 -2 13 1352.80 71.7372 51 -7 -2 13 1164.85 71.1019 12 -7 2 13 1282.72 74.6902 12 7 2 -13 1369.84 74.4513 40 7 2 -13 1270.97 74.5905 37 7 -2 -13 1431.42 70.8458 35 7 2 -13 1361.24 77.2496 35 -7 -2 14 2143.85 85.9916 51 -7 -2 14 1830.97 85.6733 12 -7 2 14 2010.61 87.6310 12 7 2 -14 1974.39 83.6301 40 7 2 -14 1904.95 86.7750 37 7 -2 -14 2054.71 81.3270 35 7 2 -14 2076.41 89.6293 35 -7 -2 15 286.048 35.7557 51 7 2 -15 239.148 30.2663 40 -7 -2 15 220.316 33.2351 12 -7 2 15 254.420 34.8033 12 7 2 -15 263.651 36.0989 37 7 2 -15 231.932 34.0851 35 -7 -2 16 241.005 29.5494 51 -7 -2 16 249.334 31.9405 12 -7 2 16 202.563 28.2172 12 7 2 -16 230.533 32.4894 37 7 2 -16 223.606 31.0833 35 -7 -2 17 7.55134 14.1178 51 -7 -2 17 8.56538 14.7713 12 -7 2 17 2.08584 17.2673 12 7 2 -17 26.8081 17.3276 37 7 2 -17-1.50137 16.8705 35 -7 -2 18-12.6561 10.9420 51 -7 -2 18 1.21594 12.1780 12 -7 2 18 11.5137 13.7893 12 7 2 -18-18.3421 13.1079 38 7 2 -18-15.9487 15.3819 35 7 -3 11-12.0824 13.1127 26 7 3 11-0.54060 10.2274 26 7 -3 10 33.1815 12.9215 26 7 3 10 70.1050 17.9694 26 -7 -3 -10 38.0276 14.6802 22 7 -3 9-17.2801 15.9719 26 7 3 9 9.94814 15.3906 26 -7 -3 -9-9.64748 15.4358 22 7 -3 8 64.8644 20.0259 26 7 3 8 80.7008 23.5649 26 -7 -3 -8 74.4021 21.8671 22 7 -3 7 1918.61 80.4468 26 7 3 7 1985.52 89.1659 26 7 -3 7 2212.00 91.4653 23 -7 -3 -7 2181.78 87.4465 22 7 -3 6 3282.33 106.900 26 7 3 6 3437.09 119.869 26 7 -3 6 3568.15 118.462 23 -7 -3 -6 3663.39 117.126 22 7 -3 5 410.743 41.0003 26 7 3 5 403.954 49.7307 26 7 -3 5 494.371 48.5132 23 -7 -3 -5 441.842 45.7499 22 7 -3 4 1565.59 82.7733 23 -7 -3 -4 1588.77 81.6566 22 7 3 4 1547.20 80.0805 33 7 -3 3 457.415 47.5804 23 7 3 3 583.409 51.1965 23 -7 -3 -3 493.371 49.7966 22 7 3 3 558.092 50.9697 33 7 3 3 548.009 52.6493 32 7 3 3 564.847 52.5711 30 7 -3 2 2821.23 110.250 54 7 -3 2 2801.97 109.249 23 7 3 2 2909.99 110.464 23 -7 -3 -2 2948.14 112.209 22 7 3 2 2860.30 110.174 41 7 3 2 2747.77 107.406 33 7 3 2 2902.11 110.979 32 7 3 2 2853.61 109.684 30 7 3 1 72.0814 25.9486 30 7 -3 1-6.60446 26.8193 54 7 -3 1 7.77581 21.8179 23 7 3 1 63.2518 28.4258 23 7 3 1 38.3069 27.1045 44 -7 -3 -1 39.6411 24.5347 22 7 3 1 0.96610 24.0848 41 7 3 1 3.19176 29.5649 39 7 3 1 0.22648 32.1363 36 7 3 1 65.7547 25.5957 33 7 3 1-1.63204 22.4535 32 7 -3 0 539.381 52.3877 54 7 -3 0 603.288 53.6244 23 7 3 0 518.302 50.3474 23 7 3 0 570.545 52.2361 44 7 3 0 583.671 51.1993 41 7 3 0 541.619 54.0756 39 7 3 0 522.229 52.0218 36 7 3 0 539.170 52.9237 34 7 3 0 587.407 52.3687 33 7 3 0 614.293 54.6256 32 7 3 0 593.849 53.2360 30 7 3 -1 1593.62 84.8812 29 7 -3 -1 1523.23 82.4842 54 7 -3 -1 1551.11 81.9715 23 7 3 -1 1614.70 83.8514 44 7 3 -1 1635.82 86.8850 39 7 3 -1 1485.50 81.8973 36 7 3 -1 1539.97 82.8634 34 7 3 -1 1519.48 83.0048 32 7 3 -1 1635.47 85.2541 30 7 3 -2 1771.25 88.9848 29 7 -3 -2 1821.21 90.5710 54 7 -3 -2 1991.50 91.2137 23 7 3 -2 1779.66 89.1937 44 7 3 -2 2230.10 99.3058 39 7 3 -2 1859.99 91.4896 36 7 3 -2 1995.98 94.0848 34 7 3 -2 2058.61 94.8950 32 7 3 -2 1804.71 90.9345 30 7 3 -3 169.814 35.4835 29 7 -3 -3 156.905 33.8423 54 7 -3 -3 168.090 31.0781 23 7 3 -3 187.027 35.1249 44 7 3 -3 191.803 33.5770 39 7 3 -3 151.272 33.7556 38 7 3 -3 263.208 40.6390 36 7 3 -3 182.165 36.2591 34 7 3 -4 171.897 34.8118 29 7 -3 -4 148.442 30.4489 54 7 -3 -4 152.597 29.6222 23 7 3 -4 121.350 27.0741 44 7 3 -4 131.269 30.4162 40 7 3 -4 159.809 34.7783 39 7 3 -4 146.472 30.0465 38 7 3 -4 110.049 29.6007 36 7 3 -4 160.517 32.3047 35 7 3 -4 160.468 35.5256 34 7 3 -5 55.6720 29.0573 29 -7 -3 5 64.9399 20.6596 51 7 3 -5 108.207 30.5464 40 -7 -3 5 32.7112 20.9609 12 7 3 -5 80.3628 28.0302 39 7 3 -5 38.9303 28.0732 38 7 3 -5 37.9400 23.5926 37 7 3 -5 13.9245 24.3326 36 7 3 -5 74.1150 26.3574 35 7 3 -5 38.8529 25.4085 34 7 3 -6 651.998 57.8172 29 -7 -3 6 646.245 52.7620 51 -7 -3 6 582.975 51.7473 12 7 3 -6 581.522 54.8664 40 7 3 -6 760.697 59.1576 39 7 3 -6 661.119 58.3366 38 7 3 -6 619.863 56.6524 37 7 3 -6 606.524 54.0776 35 7 3 -6 587.149 55.1630 34 7 3 -7 64.2553 27.6284 29 -7 -3 7 97.0562 25.2784 51 7 3 -7 132.965 34.4445 40 -7 -3 7 83.7201 24.2559 12 7 3 -7 100.023 26.5743 39 7 3 -7 62.2405 28.8037 38 7 3 -7 104.726 31.4563 37 7 3 -7 74.5609 28.0526 35 -7 -3 8 1559.50 79.0694 51 -7 -3 8 1390.02 78.3918 12 7 3 -8 1308.34 81.3877 40 7 3 -8 1404.53 81.1946 38 7 3 -8 1377.27 81.4690 37 7 3 -8 1357.31 79.3870 35 -7 -3 9 123.720 27.3050 51 7 3 -9 74.7819 30.7074 40 -7 -3 9 45.7375 25.1440 12 7 3 -9 118.873 34.6245 38 7 3 -9 96.1589 35.7270 37 -7 3 9 94.4329 23.1796 12 7 3 -9 109.228 30.4840 35 -7 -3 10 7.09272 20.0402 51 7 3 -10-26.4795 27.8937 40 -7 -3 10-23.9709 23.0575 12 7 3 -10 20.5524 28.6367 38 7 3 -10 39.5780 30.2762 37 -7 3 10-4.70225 26.7376 12 7 3 -10 28.3173 28.1859 35 -7 -3 11 45.1720 24.0334 51 7 3 -11 54.7623 28.8765 40 -7 -3 11 44.4584 22.7083 12 7 3 -11 78.4413 30.5675 37 -7 3 11 71.6128 26.1392 12 7 3 -11 81.1969 30.2264 35 -7 -3 12 58.3645 23.1084 51 7 3 -12 95.5939 29.3170 40 -7 -3 12 49.5819 26.6549 12 7 3 -12 80.6992 33.2377 37 -7 3 12 96.7496 27.8366 12 7 3 -12 71.0970 26.9745 35 -7 -3 13 6.91753 20.5215 51 7 3 -13 18.2056 23.8599 40 -7 -3 13 26.4821 23.7128 12 -7 3 13 44.1332 24.2328 12 7 3 -13 39.9994 25.8522 37 7 3 -13-5.92384 25.7114 35 -7 -3 14 198.883 31.8793 51 7 3 -14 184.236 31.5374 40 -7 -3 14 225.021 34.7419 12 -7 3 14 230.941 34.1562 12 7 3 -14 196.324 35.5417 37 7 3 -14 193.162 32.2597 35 -7 -3 15 32.7261 20.0779 51 7 3 -15 42.0418 21.7959 40 -7 -3 15 16.7742 20.7429 12 -7 3 15-31.1132 25.0399 12 7 3 -15 7.66070 21.7525 37 7 3 -15 10.6750 20.7166 35 -7 -3 16 256.507 30.2140 51 7 3 -16 214.655 27.3033 40 -7 -3 16 173.965 26.1134 12 -7 3 16 178.036 26.8733 12 7 3 -16 237.935 30.9214 37 7 3 -16 219.199 28.6115 35 -7 -3 17 106.466 19.9951 51 -7 -3 17 101.446 19.4097 12 -7 3 17 76.6013 19.4179 12 7 3 -17 105.475 20.2724 38 7 3 -17 93.9326 19.2394 37 7 3 -17 113.608 20.7832 35 -7 3 18-15.7471 11.8267 12 7 3 -18-15.7742 12.0933 38 7 3 -18 0.81907 11.5563 35 7 4 10 52.8967 14.4362 26 -7 -4 -10 75.2306 16.7403 22 7 -4 9 436.209 32.0756 26 7 4 9 506.355 37.5529 26 7 4 9 397.775 31.4463 25 -7 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32.6794 39 7 4 1 36.1512 34.3793 36 7 4 1 53.7346 26.0111 33 7 4 1 88.3467 28.7271 32 7 -4 0 1342.58 76.7125 54 7 -4 0 1408.37 77.8393 23 7 4 0 1534.91 81.7828 23 7 4 0 1372.90 78.6812 44 -7 -4 0 1316.01 75.9861 22 7 4 0 1471.86 80.6845 41 7 4 0 1385.35 80.3440 39 7 4 0 1364.27 80.6172 36 7 4 0 1507.00 82.0246 34 7 4 0 1371.54 77.5752 33 7 4 0 1452.24 80.9140 32 7 4 0 1389.72 78.4152 30 7 4 -1 53.9976 26.9104 30 7 4 -1 41.0782 26.3019 29 7 -4 -1 25.7823 24.6151 54 7 -4 -1 42.9078 21.6414 23 7 4 -1 33.2802 27.0458 44 7 4 -1 81.3620 28.6148 41 7 4 -1 44.6666 26.7819 39 7 4 -1 26.6863 28.7805 36 7 4 -1 36.1048 26.9536 34 7 4 -1 41.6915 27.4422 32 7 4 -2 1403.65 81.2905 29 7 -4 -2 1332.37 78.5247 54 7 -4 -2 1335.90 73.4874 23 7 4 -2 1350.51 78.2896 44 7 4 -2 1417.84 78.5735 41 7 4 -2 1344.39 80.9849 39 7 4 -2 1399.74 81.2154 36 7 4 -2 1366.20 79.1769 34 7 4 -2 1463.14 81.5129 32 7 4 -2 1408.95 79.3757 30 7 4 -3 619.441 59.5475 29 7 -4 -3 636.540 58.7020 54 7 4 -3 613.753 56.2568 44 7 4 -3 726.057 61.7875 39 7 4 -3 661.864 58.4813 38 7 4 -3 660.805 61.2620 36 7 4 -3 558.955 56.7608 34 7 4 -4 898.798 66.4507 29 7 -4 -4 977.811 68.7497 54 -7 -4 4 970.031 63.9220 12 7 4 -4 846.187 63.1086 44 7 4 -4 967.270 67.9012 40 7 4 -4 875.598 68.2571 39 7 4 -4 904.627 66.8549 38 7 4 -4 919.314 70.2764 36 7 4 -4 885.360 66.4013 34 7 4 -5 5948.17 161.825 29 -7 -4 5 6446.48 160.125 51 -7 -4 5 6570.23 162.551 12 7 4 -5 6232.24 165.194 40 7 4 -5 6094.77 163.980 39 7 4 -5 6231.64 164.237 38 7 4 -5 6479.01 163.466 37 7 4 -5 5886.91 162.691 36 7 4 -5 6060.30 161.769 35 7 4 -5 5795.06 159.264 34 7 4 -6 483.806 51.4387 29 -7 -4 6 484.168 47.5826 51 -7 -4 6 480.990 48.3194 12 7 4 -6 466.752 52.3916 40 7 4 -6 529.596 52.7217 39 7 4 -6 422.112 48.4465 38 7 4 -6 494.151 50.4327 37 7 4 -6 507.497 51.9019 35 7 4 -6 527.534 54.5955 34 7 4 -7 787.296 64.0604 29 -7 -4 7 906.743 62.7006 51 -7 -4 7 825.844 61.6651 12 7 4 -7 908.925 67.6521 40 7 4 -7 910.588 65.2145 39 7 4 -7 793.810 62.3029 38 7 4 -7 868.214 65.5061 37 7 4 -7 817.911 62.5613 35 -7 -4 8 2319.07 97.5243 51 -7 -4 8 2097.84 95.6056 12 7 4 -8 2075.82 99.3379 40 7 4 -8 2004.33 95.2867 38 7 4 -8 2113.58 96.4104 37 7 4 -8 2156.54 96.4870 35 -7 -4 9 3318.94 114.895 51 -7 -4 9 3244.88 117.514 12 -7 4 9 3302.10 112.727 12 7 4 -9 3339.17 122.534 40 7 4 -9 3302.74 120.021 38 7 4 -9 3278.54 118.856 37 7 4 -9 3211.75 116.474 35 -7 -4 10 6296.45 156.550 51 -7 -4 10 6074.20 160.695 12 -7 4 10 6404.73 156.903 12 7 4 -10 6085.48 162.995 40 7 4 -10 5948.33 159.214 38 7 4 -10 5932.47 160.849 37 7 4 -10 6273.13 160.012 35 -7 -4 11 3796.58 122.139 51 -7 -4 11 3610.33 123.614 12 -7 4 11 3773.11 121.913 12 7 4 -11 3819.77 128.742 40 7 4 -11 3711.16 123.354 38 7 4 -11 3766.97 126.854 37 7 4 -11 3856.55 124.352 35 -7 -4 12 381.324 43.3465 51 -7 -4 12 388.326 44.2698 12 -7 4 12 361.658 42.7623 12 7 4 -12 368.183 45.4550 40 7 4 -12 263.684 39.5926 38 7 4 -12 328.309 44.2471 37 7 4 -12 276.362 37.9573 35 -7 -4 13 4.40264 19.3649 51 -7 -4 13 10.4706 20.0193 12 7 4 -13-30.6716 26.8961 40 7 4 -13-8.99676 24.8691 37 -7 4 13-9.04861 18.5573 12 7 4 -13-17.8834 23.5738 35 -7 -4 14 239.480 32.6591 51 -7 -4 14 251.206 34.0426 12 7 4 -14 229.726 32.9361 40 7 4 -14 218.441 33.1992 37 -7 4 14 283.917 34.6824 12 7 4 -14 269.672 33.9338 35 -7 -4 15 16.5637 17.1359 51 -7 -4 15-11.8410 16.3992 12 7 4 -15-3.65328 19.4558 40 7 4 -15-2.31018 19.5330 38 -7 4 15 23.3486 18.9377 12 7 4 -15-11.2033 19.0559 37 7 4 -15 6.24226 16.0384 35 -7 -4 16 154.658 23.6495 51 -7 -4 16 121.129 21.5562 12 7 4 -16 159.935 24.6784 40 7 4 -16 153.804 25.8718 38 -7 4 16 149.796 24.2357 12 7 4 -16 145.090 26.1526 37 7 4 -16 134.527 21.9133 35 -7 -4 17 130.804 19.1845 51 -7 -4 17 151.695 19.4383 12 7 4 -17 103.437 19.7032 38 -7 4 17 124.764 19.5752 12 7 4 -17 129.218 19.9381 37 7 4 -17 114.480 18.6400 35 7 5 9 4.16342 10.9704 26 7 5 9-2.73684 11.0882 25 -7 -5 -9-5.98366 13.2396 22 7 5 8 229.275 24.4767 55 7 5 8 226.535 26.9444 26 7 5 8 250.359 24.0588 43 -7 -5 -8 255.632 28.3864 22 7 5 7 957.041 55.6952 26 -7 -5 -7 979.175 55.5116 22 7 5 7 910.748 49.1329 43 7 5 7 970.169 52.1338 31 7 5 6 868.754 56.4547 26 -7 -5 -6 985.687 58.6027 22 7 5 6 805.903 49.9450 43 7 5 6 869.491 53.1376 31 7 5 5 82.1478 23.2621 26 7 5 5 54.2648 20.8385 43 -7 -5 -5 63.2357 23.7809 22 7 5 5 65.7916 21.2173 31 7 -5 4 19.6589 21.9438 23 7 5 4 15.3065 17.8894 46 -7 -5 -4 66.3989 24.5818 22 7 5 4 18.9927 23.7725 33 7 5 4 68.5211 24.9787 31 7 -5 3 149.134 29.7754 23 7 5 3 113.735 25.2218 46 -7 -5 -3 126.035 28.3057 22 7 5 3 145.823 32.2490 41 7 5 3 122.537 29.2303 33 7 5 3 96.9092 30.7569 32 7 5 3 134.108 29.1957 30 7 -5 2 474.430 46.2997 23 7 5 2 406.365 42.2645 46 -7 -5 -2 451.324 47.1381 22 7 5 2 501.129 50.3069 41 7 5 2 449.103 47.6742 33 7 5 2 470.470 49.9153 32 7 5 2 515.546 49.9903 30 7 5 1-21.3257 28.4999 30 7 -5 1-5.88306 21.8398 54 7 -5 1 18.0013 20.3631 23 -7 -5 -1-4.36124 22.6351 47 -7 -5 -1 15.0235 27.1474 22 7 5 1-13.4860 31.2669 41 7 5 1-6.18289 34.7443 39 7 5 1 15.5512 29.1116 36 7 5 1 71.6404 30.1952 33 7 5 1 14.1771 29.3770 32 7 -5 0 2335.49 99.9664 54 7 -5 0 2304.42 93.3955 23 -7 -5 0 2425.64 95.1489 47 7 5 0 2230.74 98.6007 44 -7 -5 0 2267.65 97.9105 22 7 5 0 2311.92 101.997 41 7 5 0 2254.35 102.558 39 7 5 0 2370.10 103.022 36 7 5 0 2294.66 99.9478 34 7 5 0 2279.37 99.4384 33 7 5 0 2250.24 100.693 32 7 5 0 2205.21 98.3776 30 7 5 -1 482.498 55.8282 29 7 -5 -1 490.782 50.5940 54 -7 -5 1 495.707 48.8815 47 7 5 -1 451.461 50.5074 44 -7 -5 1 483.257 50.2012 22 7 5 -1 500.083 51.5247 41 7 5 -1 562.220 60.6734 39 7 5 -1 506.248 53.8079 36 7 5 -1 502.102 55.0266 34 7 5 -1 541.113 57.7412 32 7 5 -1 473.518 54.0175 30 7 5 -2 7681.58 180.010 29 7 -5 -2 7622.22 178.699 54 -7 -5 2 7910.13 173.969 47 7 5 -2 7387.47 176.835 44 -7 -5 2 7654.21 177.128 22 7 5 -2 7706.30 180.948 41 7 5 -2 7297.68 181.669 39 7 5 -2 7479.70 180.383 36 7 5 -2 7776.68 180.451 34 7 5 -2 7392.39 178.804 32 7 5 -2 7510.49 178.891 30 7 5 -3 3655.40 124.870 29 7 -5 -3 3639.53 125.216 54 -7 -5 3 3760.76 120.671 12 7 5 -3 3501.84 122.431 44 7 5 -3 3705.93 125.917 41 7 5 -3 3591.61 128.440 39 7 5 -3 3545.72 125.206 36 7 5 -3 3533.40 125.511 34 7 5 -3 3613.88 126.791 32 7 5 -4 805.562 64.7051 29 7 -5 -4 832.860 65.2903 54 -7 -5 4 949.061 65.1616 12 7 5 -4 793.684 61.6824 44 7 5 -4 934.336 66.9451 40 7 5 -4 835.691 69.1380 39 7 5 -4 800.374 64.5602 38 7 5 -4 813.141 65.0000 36 7 5 -4 814.333 63.9444 34 7 5 -5 815.612 65.3921 29 7 -5 -5 870.963 65.3116 54 -7 -5 5 916.420 64.4026 12 7 5 -5 830.125 61.8658 44 7 5 -5 957.332 67.5527 40 7 5 -5 922.273 68.6776 39 7 5 -5 820.554 61.5143 38 7 5 -5 939.042 67.7930 36 7 5 -5 830.073 64.3905 34 7 5 -6 2437.99 104.514 29 -7 -5 6 2592.15 102.982 51 -7 -5 6 2771.55 106.909 12 7 5 -6 2381.89 101.013 44 7 5 -6 2683.39 108.083 40 7 5 -6 2546.04 107.032 39 7 5 -6 2655.74 106.657 38 7 5 -6 2682.87 103.758 37 7 5 -6 2542.43 104.183 35 7 5 -6 2418.73 105.037 34 7 5 -7 5863.75 158.028 29 -7 -5 7 5927.40 156.016 51 -7 -5 7 6114.26 158.307 12 7 5 -7 5895.28 158.656 40 7 5 -7 5749.49 156.490 38 7 5 -7 6061.78 154.943 37 7 5 -7 5907.71 155.611 35 7 5 -8 5733.51 156.218 29 -7 -5 8 5800.77 152.139 51 -7 -5 8 6067.32 157.601 12 7 5 -8 5937.94 159.325 40 7 5 -8 5876.02 155.354 38 7 5 -8 5994.05 155.669 37 7 5 -8 5862.32 153.887 35 -7 -5 9 1825.83 86.3488 51 -7 -5 9 1832.92 87.6569 12 7 5 -9 1747.10 91.1795 40 7 5 -9 1756.46 86.4271 38 7 5 -9 1825.90 86.9886 37 7 5 -9 1697.01 83.8472 35 -7 -5 10 18.6643 24.3351 51 -7 -5 10-18.3321 26.5668 12 7 5 -10 0.45753 30.3141 40 7 5 -10-28.2417 31.3638 38 7 5 -10 11.4892 26.7762 37 -7 5 10 18.1914 21.0322 12 7 5 -10-13.9016 25.0212 35 -7 -5 11 4.68712 21.8179 51 -7 -5 11 54.3818 26.4020 12 7 5 -11 11.0077 26.5739 40 7 5 -11-8.02228 27.2523 38 7 5 -11 7.18593 22.6308 37 -7 5 11 2.17911 19.3874 12 7 5 -11 36.3986 25.1304 35 -7 -5 12 523.990 44.9095 51 -7 -5 12 479.971 45.4598 12 -7 5 12 573.648 46.6175 12 7 5 -12 609.760 51.1624 40 7 5 -12 584.078 50.4896 38 7 5 -12 585.627 50.4624 37 7 5 -12 497.567 43.5406 35 -7 -5 13 306.045 35.5781 51 -7 -5 13 299.486 37.0002 12 7 5 -13 363.471 41.8179 40 7 5 -13 304.250 36.9530 38 7 5 -13 352.870 40.1952 37 -7 5 13 285.043 32.9819 12 7 5 -13 416.313 40.4719 35 -7 -5 14 208.708 28.4484 51 -7 -5 14 173.617 27.2304 12 7 5 -14 218.899 32.8094 40 7 5 -14 163.610 27.4532 38 7 5 -14 177.156 28.3799 37 -7 5 14 188.678 27.8389 12 7 5 -14 202.154 27.2687 35 -7 -5 15 290.117 30.0958 51 -7 -5 15 272.096 29.8225 12 -7 5 15 336.760 31.6995 12 7 5 -15 330.243 33.0520 40 7 5 -15 280.085 30.5452 38 7 5 -15 291.113 31.4567 37 7 5 -15 285.579 28.2088 35 -7 -5 16 68.3065 17.5457 51 -7 -5 16 38.0861 14.2962 12 7 5 -16 63.3490 17.0461 40 7 5 -16 53.7729 17.3798 38 -7 5 16 38.7568 14.4775 12 7 5 -16 87.7010 19.2305 37 7 5 -16 79.5220 15.9567 35 7 6 8 233.746 22.4942 55 7 6 8 273.520 24.3106 26 -7 -6 -8 292.298 27.3980 22 7 6 7 97.8641 20.7677 26 7 6 7 79.3937 16.7184 43 -7 -6 -7 84.2126 19.3778 22 7 6 7 101.533 19.7946 31 7 6 6 7.67071 16.4410 26 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44.8942 30.5446 38 8 3 -9 48.7780 24.9280 36 8 3 -9 32.2422 25.1648 35 8 3 -9 68.3488 29.1609 34 8 3 -10 2937.60 104.084 29 -8 -3 10 3123.30 99.0838 51 -8 -3 10 2825.68 101.892 12 -8 3 10 2906.79 97.3699 12 8 3 -10 2949.73 106.987 40 8 3 -10 3013.42 107.752 38 8 3 -10 2930.84 109.033 37 8 3 -10 2789.26 96.4015 36 8 3 -10 2852.87 106.396 35 8 3 -10 2821.49 101.528 34 8 3 -11 605.091 49.7430 29 -8 -3 11 642.969 46.6237 51 -8 -3 11 608.300 50.3648 12 -8 3 11 589.051 47.3534 12 8 3 -11 585.192 51.9519 40 8 3 -11 539.567 48.4842 38 8 3 -11 651.033 56.3667 37 8 3 -11 535.536 42.3637 36 8 3 -11 643.885 51.1582 35 8 3 -11 532.362 45.2989 34 8 3 -12 2883.60 95.4816 29 -8 -3 12 2984.02 91.3608 51 -8 -3 12 2917.23 99.0642 12 -8 3 12 2982.16 94.6663 12 8 3 -12 2884.16 97.7258 40 8 3 -12 2863.74 97.5909 38 8 3 -12 2970.24 99.8673 37 8 3 -12 2983.76 100.923 35 8 3 -12 2838.25 92.3956 34 8 3 -13 31.5487 19.1594 29 -8 -3 13 106.176 21.7048 51 8 3 -13 86.2113 24.9961 40 -8 -3 13 66.5231 21.5572 12 -8 3 13 50.4768 20.2186 12 8 3 -13 38.8527 20.4826 38 8 3 -13 59.8129 24.8298 37 8 3 -13 52.2574 21.4963 35 8 3 -13 29.3839 16.8023 34 8 3 -14 5.83281 15.6589 29 -8 -3 14-11.1188 14.6568 51 -8 -3 14 9.19397 16.3265 12 -8 3 14-5.83475 15.6562 12 8 3 -14 16.0087 17.8663 38 8 3 -14 10.6323 20.2516 37 8 3 -14-1.07383 15.9375 35 8 3 -14 5.74121 14.4356 34 8 3 -15 634.849 36.1236 29 8 -3 -15 720.661 39.2163 54 -8 -3 15 668.911 36.4247 51 -8 -3 15 669.995 41.3243 12 -8 3 15 649.526 39.8489 12 8 3 -15 755.618 42.7283 38 8 3 -15 708.317 42.0834 37 8 3 -15 709.815 42.0625 35 -8 -3 16 236.585 24.0632 12 -8 3 16 234.234 24.0584 12 8 3 -16 267.084 24.3708 38 8 3 -16 240.240 31.6536 35 8 4 7 56.0622 16.2296 26 -8 -4 -7 89.9014 17.7867 22 8 4 6 357.775 32.9183 26 -8 -4 -6 324.142 30.3415 22 8 4 5 57.5741 20.4281 26 -8 -4 -5 43.6244 17.6864 22 8 4 4 349.269 37.9908 26 8 -4 4 387.313 36.6376 23 -8 -4 -4 414.050 38.1958 22 8 4 3 363.690 41.1333 26 8 -4 3 444.829 41.7292 23 -8 -4 -3 370.276 39.3702 22 8 -4 2 3566.82 109.130 23 -8 -4 -2 3747.17 113.362 22 8 4 2 3645.96 108.770 33 8 -4 1 2640.13 95.8325 23 8 4 1 2678.53 93.0075 23 -8 -4 -1 2748.17 100.446 22 8 4 1 2558.12 93.8105 33 8 4 1 2774.48 100.209 32 8 4 1 2728.55 98.6101 30 8 -4 0 4906.66 136.039 54 8 -4 0 5055.12 131.038 23 8 4 0 4986.04 130.424 23 -8 -4 0 5053.99 136.456 22 8 4 0 5135.57 133.685 33 8 4 0 5123.04 136.781 32 8 4 0 4949.26 133.442 30 8 -4 -1 885.522 63.0473 54 8 -4 -1 745.281 53.0587 23 8 4 -1 813.232 58.9096 23 -8 -4 1 728.988 58.7942 22 8 4 -1 765.258 54.6606 33 8 4 -1 950.007 63.1287 32 8 4 -1 895.119 60.8103 30 8 4 -2 78.3847 27.5224 30 8 -4 -2 125.237 31.7225 54 8 -4 -2 102.467 23.3836 23 8 4 -2 176.678 34.1390 23 8 4 -2 134.713 33.0339 44 -8 -4 2 149.093 30.8053 22 8 4 -2 122.840 31.4645 39 8 4 -2 81.9650 31.0980 36 8 4 -2 115.976 35.4163 34 8 4 -2 134.079 29.5723 33 8 4 -2 90.2752 28.9073 32 8 4 -3 341.772 41.0910 30 8 4 -3 519.671 52.1063 29 8 -4 -3 485.885 50.0700 54 8 -4 -3 327.882 34.7880 23 8 4 -3 490.343 48.9584 23 8 4 -3 397.423 43.9201 44 8 4 -3 506.068 49.1125 39 8 4 -3 420.002 47.5023 36 8 4 -3 396.807 47.9523 34 8 4 -3 463.404 44.5054 33 8 4 -3 452.313 46.4915 32 8 4 -4 778.049 60.4429 29 8 -4 -4 849.792 62.4942 54 8 4 -4 873.343 61.9273 44 8 4 -4 818.282 58.8136 39 8 4 -4 879.207 62.7217 36 8 4 -4 870.538 63.3380 34 8 4 -4 931.023 62.2849 32 8 4 -4 777.533 58.8602 30 8 4 -5 82.4223 27.7412 30 8 4 -5 66.1076 29.3276 29 8 -4 -5 72.5873 28.6103 54 8 4 -5 51.4752 27.5853 44 8 4 -5 106.526 27.7501 39 8 4 -5 106.206 33.6975 36 8 4 -5 92.5815 32.6651 34 8 4 -5 97.7278 27.9693 32 8 4 -6 2.03151 26.8664 29 8 -4 -6 17.3720 26.8852 54 8 4 -6-15.9096 25.7690 44 -8 -4 6 13.9910 17.3821 12 8 4 -6-1.38745 23.0423 39 8 4 -6-12.5180 31.4662 38 8 4 -6-12.0321 25.3816 36 8 4 -6-4.67107 24.1962 34 8 4 -6 15.5275 26.8555 32 8 4 -7 442.446 47.6593 29 8 -4 -7 480.805 52.3224 54 -8 -4 7 401.625 42.9780 12 8 4 -7 400.061 45.8401 44 8 4 -7 385.434 41.2173 39 8 4 -7 368.534 47.3385 38 8 4 -7 417.016 45.5190 36 8 4 -7 430.132 46.8444 34 8 4 -8 60.3311 26.9844 29 8 -4 -8 89.1952 31.0619 54 -8 -4 8 121.719 27.1071 51 8 4 -8 113.256 29.2568 44 -8 -4 8 149.294 31.7684 12 8 4 -8 150.774 40.7504 40 8 4 -8 113.623 27.3044 39 8 4 -8 104.395 35.8630 38 8 4 -8 113.828 31.9041 36 8 4 -8 150.928 32.8801 35 8 4 -8 111.126 32.6052 34 8 4 -9 539.952 49.4116 29 8 -4 -9 550.334 50.3645 54 -8 -4 9 533.975 45.2545 51 -8 -4 9 520.949 46.0818 12 8 4 -9 586.130 53.7018 40 8 4 -9 577.466 51.2217 38 8 4 -9 568.085 48.4343 36 8 4 -9 555.132 49.8685 35 8 4 -9 510.276 48.0609 34 8 4 -10 130.626 29.4214 29 -8 -4 10 154.195 28.0975 51 -8 -4 10 167.882 29.5288 12 8 4 -10 169.826 36.1633 40 8 4 -10 167.690 34.2352 38 8 4 -10 232.727 36.0382 37 8 4 -10 159.362 29.1418 36 8 4 -10 169.999 34.7261 35 8 4 -10 171.023 30.8357 34 8 4 -11-5.88973 21.3408 29 -8 -4 11 14.3390 17.4620 51 -8 -4 11 33.9686 20.3917 12 8 4 -11 4.40763 23.0420 40 8 4 -11 32.6017 22.9900 38 -8 4 11 6.38083 16.9955 12 8 4 -11 76.9456 26.5666 37 8 4 -11-18.4245 21.9884 36 8 4 -11 62.0051 23.4395 35 8 4 -11 12.0454 22.0796 34 8 4 -12-4.22932 20.9326 29 -8 -4 12 11.9874 16.8403 51 -8 -4 12 7.53721 17.4796 12 8 4 -12-7.25440 20.3753 40 8 4 -12 21.0305 23.1306 38 -8 4 12-12.6583 18.0287 12 8 4 -12 10.0020 23.2765 37 8 4 -12-34.0795 18.3996 36 8 4 -12-4.85984 18.5099 35 8 4 -12-40.2563 24.3271 34 8 4 -13-1.55871 17.9535 29 -8 -4 13 20.1806 16.5897 51 -8 -4 13 8.09931 16.3601 12 8 4 -13 45.4393 20.3187 40 8 4 -13 33.4922 19.7416 38 -8 4 13 17.0596 14.8424 12 8 4 -13 25.5764 19.7534 37 8 4 -13 2.12335 15.2592 36 8 4 -13 9.82088 16.9529 35 8 4 -13-3.39642 16.9830 34 8 4 -14-15.7614 16.9915 29 8 -4 -14-16.2298 16.8343 54 -8 -4 14 18.8035 13.2062 51 -8 -4 14 3.14049 14.7073 12 8 4 -14 8.50831 15.8912 40 -8 4 14-3.38005 14.4360 12 8 4 -14-20.8504 17.0966 38 8 4 -14-17.0060 18.5183 37 8 4 -14-6.38027 14.0831 35 8 4 -14 3.46349 13.4566 34 8 4 -15 58.8361 16.4725 29 8 -4 -15 49.1041 14.8413 54 -8 -4 15 67.3752 15.3669 51 -8 -4 15 70.1221 17.1654 12 -8 4 15 82.4766 17.3020 12 8 4 -15 51.7989 16.6983 38 8 4 -15 68.0334 17.6579 37 8 4 -15 86.0876 17.7922 35 8 5 6 109.190 18.2379 26 -8 -5 -6 98.2363 17.7082 22 8 5 5 38.1045 16.2891 26 -8 -5 -5 52.4078 16.8278 22 8 5 4 172.146 27.2566 26 -8 -5 -4 186.957 26.3621 22 8 5 4 158.169 21.7700 31 8 5 3 647.327 47.2939 26 -8 -5 -3 646.175 47.1114 22 8 5 3 624.496 40.5019 31 8 -5 2 479.901 38.3249 23 -8 -5 -2 490.189 42.5055 22 8 5 2 478.944 39.4152 33 8 5 2 549.704 41.2344 31 8 -5 1 137.311 24.0201 23 -8 -5 -1 90.7834 25.3401 22 8 5 1 85.6074 22.3081 33 8 5 1 86.0898 22.7591 32 8 5 1 112.233 25.1737 30 8 -5 0 64.2624 21.4390 54 8 -5 0 93.0048 20.7816 23 -8 -5 0 67.5077 23.9232 22 8 5 0 58.6941 21.8282 33 8 5 0 67.4283 26.2776 32 8 5 0 103.968 27.3630 30 8 5 -1 307.687 39.8876 30 8 -5 -1 357.742 39.2494 54 8 5 -1 321.681 36.7859 23 -8 -5 1 335.404 40.2628 22 8 5 -1 318.208 35.8688 41 8 5 -1 322.298 39.9860 33 8 5 -1 355.341 41.5233 32 8 -5 -2 8031.79 168.786 54 8 5 -2 7744.73 158.703 23 -8 -5 2 7931.94 151.656 47 8 5 -2 7794.10 167.260 44 -8 -5 2 8237.09 168.922 22 8 5 -2 8175.49 171.224 39 8 5 -2 7859.61 170.808 36 8 5 -2 7906.92 168.538 34 8 5 -2 7800.76 163.405 33 8 5 -2 7942.53 168.269 32 8 5 -2 7949.41 167.342 30 8 -5 -3 2841.98 102.925 54 8 5 -3 2891.22 100.433 23 -8 -5 3 3046.28 96.9324 47 8 5 -3 2881.51 105.233 44 -8 -5 3 2923.66 101.816 22 8 5 -3 2898.98 105.859 39 8 5 -3 3180.44 111.389 36 8 5 -3 3044.30 108.886 34 8 5 -3 2918.26 102.597 33 8 5 -3 3039.29 106.868 32 8 5 -3 2899.20 104.356 30 8 5 -4 707.737 58.3332 29 8 -5 -4 735.697 56.6675 54 -8 -5 4 686.797 49.3510 47 8 5 -4 650.128 53.5894 44 -8 -5 4 757.352 55.8456 22 8 5 -4 658.744 52.9238 39 8 5 -4 708.544 57.4502 36 8 5 -4 736.086 56.8086 34 8 5 -4 662.940 52.5705 32 8 5 -4 648.666 53.0773 30 8 5 -5-50.5048 30.4070 30 8 5 -5-1.57093 25.5998 29 8 -5 -5-1.45612 23.1456 54 -8 -5 5-16.4198 20.6257 47 8 5 -5-46.0219 29.8142 44 -8 -5 5 20.9868 20.4223 12 -8 -5 5-15.9126 21.8981 22 8 5 -5 14.0399 22.7580 39 8 5 -5-13.2902 26.8428 36 8 5 -5 15.5219 26.3760 34 8 5 -5-19.3087 31.2013 32 8 5 -6 506.089 47.5717 29 8 -5 -6 512.501 47.2976 54 -8 -5 6 640.152 48.8469 12 8 5 -6 559.558 49.1924 44 8 5 -6 508.880 46.6339 39 8 5 -6 585.832 50.8479 36 8 5 -6 499.566 45.9278 34 8 5 -6 529.584 46.7881 32 8 5 -7 15.2300 25.7679 29 8 -5 -7 21.1576 22.8541 54 8 5 -7 3.07835 24.9552 44 -8 -5 7 29.8636 20.9080 12 8 5 -7 0.23629 19.9940 39 8 5 -7 13.0772 23.4417 38 8 5 -7 27.7368 23.1425 36 8 5 -7 13.7939 23.9570 34 8 5 -8 192.503 33.9816 29 8 -5 -8 251.097 37.2376 54 8 5 -8 176.861 30.5753 44 -8 -5 8 219.132 32.3728 12 8 5 -8 276.312 33.7895 39 8 5 -8 201.696 36.0965 38 8 5 -8 218.097 33.1441 36 8 5 -8 211.290 35.0241 34 8 5 -9 1146.26 64.5273 29 8 -5 -9 1093.22 63.3481 54 -8 -5 9 1028.03 59.6666 12 8 5 -9 1051.78 60.5574 44 8 5 -9 1060.28 62.4908 40 8 5 -9 935.971 53.4003 39 8 5 -9 1129.42 64.3837 38 8 5 -9 1080.98 61.3121 36 8 5 -9 1044.13 61.4566 34 8 5 -10 193.123 30.5514 29 8 -5 -10 249.000 34.0804 54 -8 -5 10 250.031 31.4666 51 8 5 -10 197.328 29.6222 44 -8 -5 10 220.004 31.5118 12 8 5 -10 213.021 34.3622 40 8 5 -10 218.691 34.2292 38 8 5 -10 228.736 32.3639 36 8 5 -10 184.610 30.7999 34 8 5 -11 1063.02 57.9398 29 8 -5 -11 1175.84 61.4900 54 -8 -5 11 1067.94 55.6079 51 -8 -5 11 1024.62 55.5264 12 8 5 -11 1087.90 56.5345 44 8 5 -11 1159.16 60.4303 40 8 5 -11 1216.42 61.4913 38 8 5 -11 1060.56 55.6713 36 8 5 -11 1154.47 59.2474 34 8 5 -12 5.47672 17.9357 29 8 -5 -12 38.3767 19.0706 54 -8 -5 12 18.4939 14.3270 51 8 5 -12 20.1376 17.0427 44 -8 -5 12 9.43622 16.4374 12 8 5 -12 50.5104 21.0632 40 8 5 -12 18.2390 18.0743 38 8 5 -12 30.6868 17.9776 37 -8 5 12-3.96896 14.8587 12 8 5 -12 18.5148 14.9987 36 8 5 -12 19.3710 15.9360 35 8 5 -12 26.5471 20.1567 34 8 5 -13 319.052 30.3579 29 8 -5 -13 363.048 32.2251 54 -8 -5 13 365.556 30.1652 51 -8 -5 13 318.329 30.5117 12 -8 5 13 310.943 26.6063 12 8 5 -13 342.271 29.9101 44 8 5 -13 337.059 31.6832 40 8 5 -13 335.909 30.9128 38 8 5 -13 304.381 26.8367 36 8 5 -13 344.087 30.7090 34 8 5 -14 75.8353 18.4581 29 8 -5 -14 62.9667 15.6323 54 -8 -5 14 73.0389 15.6393 51 8 5 -14 64.6020 16.2851 44 -8 -5 14 62.8343 16.6047 12 8 5 -14 68.4370 16.9778 38 8 5 -14 62.2598 15.0746 34 8 6 5 26.4125 13.5225 26 -8 -6 -5-20.1460 11.9214 22 8 6 4 74.6203 17.5247 26 -8 -6 -4 76.6058 17.2317 22 8 6 4 46.0659 13.5098 31 8 6 3 239.015 27.0931 26 -8 -6 -3 321.718 30.3419 22 8 6 3 334.189 27.8273 43 8 6 3 325.390 28.3369 31 -8 -6 -2 6.65050 14.0599 22 8 6 2-2.02658 13.3467 31 -8 -6 -1-21.7522 14.6951 48 -8 -6 -1 17.0378 16.8164 22 8 6 1-26.8249 22.5055 33 8 6 1 5.91707 14.4588 31 -8 -6 0 287.200 31.5682 22 8 6 0 250.636 31.6713 33 8 6 0 263.247 32.8448 32 8 6 0 280.709 33.9940 30 8 -6 -1 1766.40 70.6806 54 -8 -6 1 1892.02 70.3508 47 -8 -6 1 1725.92 73.4357 22 8 6 -1 1794.41 73.1462 41 8 6 -1 1778.32 75.0547 33 8 6 -1 1967.09 79.5911 32 8 6 -1 1833.19 77.2218 30 8 -6 -2 3694.82 103.648 54 -8 -6 2 3666.67 99.5398 47 -8 -6 2 3537.88 103.796 22 8 6 -2 3462.58 100.430 41 8 6 -2 3734.50 112.859 39 8 6 -2 3909.32 111.701 36 8 6 -2 3588.34 106.758 33 8 6 -2 3660.06 110.092 32 8 6 -2 3623.61 107.837 30 8 -6 -3 6241.76 137.355 54 8 6 -3 5718.68 124.789 23 -8 -6 3 6208.25 132.195 47 8 6 -3 6167.63 139.397 44 -8 -6 3 6216.88 135.466 22 8 6 -3 5809.34 128.440 41 8 6 -3 6435.51 144.422 39 8 6 -3 6344.95 143.743 36 8 6 -3 6271.00 139.338 34 8 6 -3 6070.42 137.385 33 8 6 -3 6283.63 142.709 32 8 6 -3 6168.01 141.488 30 8 -6 -4 940.898 56.7814 54 8 6 -4 869.486 51.8382 23 -8 -6 4 896.223 53.8347 47 8 6 -4 979.640 61.6932 44 -8 -6 4 873.028 53.6310 22 8 6 -4 944.718 61.3002 39 8 6 -4 951.276 59.9917 36 8 6 -4 1072.84 62.9735 34 8 6 -4 903.654 56.2101 33 8 6 -4 936.736 60.0946 32 8 6 -4 860.576 57.0922 30 8 6 -5 261.991 34.4095 30 8 6 -5 332.376 39.8288 29 8 -6 -5 270.592 34.1575 54 -8 -6 5 267.752 33.0179 47 8 6 -5 299.498 36.0535 44 -8 -6 5 237.618 30.0527 22 8 6 -5 301.416 38.7586 39 8 6 -5 304.119 38.1502 36 8 6 -5 318.060 37.8565 34 8 6 -5 223.323 31.3622 32 8 6 -6 8.65984 27.4012 30 8 6 -6 111.678 26.0712 29 8 -6 -6 49.8125 19.8920 54 -8 -6 6 68.3308 20.8152 12 -8 -6 6 80.1772 22.7724 47 8 6 -6 73.2654 22.1789 44 -8 -6 6 46.1078 16.2088 22 8 6 -6 64.0783 22.7307 39 8 6 -6 77.7599 26.3045 36 8 6 -6 88.4451 24.5733 34 8 6 -6-5.01249 26.9042 32 8 6 -7 187.221 25.6977 30 8 6 -7 276.055 36.1150 29 8 -6 -7 245.296 30.7858 54 8 6 -7 229.254 29.6016 44 -8 -6 7 218.340 29.3693 12 -8 -6 7 255.085 27.8429 22 8 6 -7 274.763 33.1471 39 8 6 -7 245.504 33.5250 36 8 6 -7 300.766 34.9941 34 8 6 -7 214.553 29.4303 32 8 6 -8 186.433 29.7746 29 8 -6 -8 174.262 28.0649 54 8 6 -8 152.948 26.5216 44 -8 -6 8 169.109 26.0736 12 -8 -6 8 126.969 20.0584 22 8 6 -8 159.867 28.5672 39 8 6 -8 182.706 30.4252 36 8 6 -8 191.409 29.6964 34 8 6 -8 181.744 27.7059 32 8 6 -9 669.254 46.1666 29 8 -6 -9 691.685 46.8805 54 -8 -6 9 709.301 46.6383 12 8 6 -9 702.975 45.5607 44 8 6 -9 682.074 43.4100 39 8 6 -9 727.756 47.2253 38 8 6 -9 679.309 46.5601 36 8 6 -9 674.177 45.2718 34 8 6 -10 198.365 27.3386 29 8 -6 -10 198.646 27.1392 54 8 6 -10 209.678 27.3214 44 -8 -6 10 175.804 26.8799 12 8 6 -10 172.823 23.6669 39 8 6 -10 209.046 28.0260 38 8 6 -10 183.799 26.2994 36 8 6 -10 139.046 24.4334 34 8 6 -11 155.567 24.5925 29 8 -6 -11 165.206 25.7450 54 8 6 -11 141.943 22.9877 44 -8 -6 11 153.536 23.4766 12 8 6 -11 128.185 22.2023 38 8 6 -11 157.179 24.9040 36 8 6 -11 170.324 24.8370 34 8 6 -12-6.52053 14.9216 29 8 -6 -12-17.0476 15.6514 54 8 6 -12-17.7321 13.4253 44 -8 -6 12 4.78679 14.5163 12 8 6 -12-8.72664 13.5148 38 8 6 -12 11.7583 14.8090 36 8 6 -12 14.4512 14.2471 34 8 6 -13 7.69864 12.4702 29 8 -6 -13 20.5944 13.5835 54 -8 -6 13 33.4981 13.7692 12 8 6 -13 9.33704 13.1001 38 8 6 -13-10.5957 13.1345 34 8 7 3 17.9377 11.4128 26 8 7 2-21.5217 13.6073 26 8 7 2 5.59685 11.4568 43 -8 -7 -2 14.5794 11.5273 22 8 7 2 2.98899 10.8248 31 -8 -7 -1 22.1633 13.4871 48 -8 -7 -1 17.7608 13.0555 22 8 7 1-8.48724 15.8992 33 8 7 1 44.3352 16.3138 31 -8 -7 0 1278.65 53.2505 48 -8 -7 0 1168.40 49.9756 22 8 7 0 1193.91 55.1111 33 8 7 0 1290.66 56.2270 32 8 7 0 1205.30 54.6143 31 -8 -7 1 1385.17 55.1893 22 8 7 -1 1351.68 57.9692 41 8 7 -1 1400.70 60.8569 33 8 7 -1 1364.08 60.0309 32 8 7 -1 1364.08 60.1091 30 -8 -7 2 753.001 43.6386 47 -8 -7 2 704.585 41.5133 22 8 7 -2 665.504 42.4417 41 8 7 -2 726.115 46.8951 33 8 7 -2 728.701 47.4192 32 8 7 -2 717.548 45.3273 30 8 -7 -3 1643.28 60.2186 54 -8 -7 3 1772.47 66.9415 47 -8 -7 3 1774.08 62.3087 22 8 7 -3 1595.19 62.8679 41 8 7 -3 1863.29 72.6533 39 8 7 -3 1941.57 72.0494 36 8 7 -3 1755.34 69.4880 33 8 7 -3 1740.96 70.0675 32 8 7 -3 1701.57 68.0169 30 8 -7 -4 609.742 39.0746 54 -8 -7 4 608.657 41.8879 47 8 7 -4 513.031 36.5407 41 8 7 -4 617.452 45.6407 39 8 7 -4 569.042 42.7339 36 8 7 -4 692.847 45.2866 34 8 7 -4 661.811 44.3805 33 8 7 -4 555.527 42.7263 32 8 7 -4 584.031 42.0980 30 8 -7 -5 1443.90 58.6344 54 -8 -7 5 1342.71 59.1957 47 8 7 -5 1485.50 61.4011 44 8 7 -5 1360.23 61.8266 39 8 7 -5 1372.49 62.4591 36 8 7 -5 1408.43 60.2306 34 8 7 -5 1329.76 60.9223 33 8 7 -5 1361.60 61.0892 32 8 7 -5 1263.77 58.6471 30 8 7 -6 360.934 32.6103 30 8 7 -6 475.255 37.5699 29 8 -7 -6 453.172 34.6701 54 8 7 -6 398.638 30.8641 23 -8 -7 6 452.984 35.8540 47 8 7 -6 484.630 37.0207 44 8 7 -6 531.684 40.5547 39 8 7 -6 455.068 38.2620 36 8 7 -6 438.090 36.3488 34 8 7 -6 429.981 37.2327 32 8 7 -7-12.6191 20.9693 30 8 7 -7 1.62229 16.1484 29 8 -7 -7 15.7099 13.8246 54 -8 -7 7 3.90231 15.5695 47 8 7 -7 30.1543 18.0796 44 8 7 -7 2.11722 16.7964 39 8 7 -7 19.4511 18.4538 36 8 7 -7 12.2291 16.2072 34 8 7 -7-46.4676 22.9309 32 8 7 -8 251.102 27.5489 30 8 7 -8 330.220 30.2770 29 8 -7 -8 330.106 29.6756 54 -8 -7 8 338.413 30.8179 47 8 7 -8 327.740 28.8276 44 8 7 -8 347.538 31.1335 39 8 7 -8 342.999 32.5597 36 8 7 -8 310.705 30.1212 34 8 7 -8 248.830 28.3077 32 8 7 -9 116.654 20.9358 30 8 7 -9 119.759 20.8443 29 8 -7 -9 126.582 19.5491 54 -8 -7 9 141.489 21.6156 47 8 7 -9 127.458 20.1568 44 8 7 -9 137.451 20.0604 39 8 7 -9 152.470 23.5530 36 8 7 -9 143.358 22.4827 34 8 7 -9 99.0584 20.5671 32 8 7 -10 18.5894 13.1201 30 8 7 -10 28.6719 15.4009 29 8 -7 -10 0.13564 12.8610 54 -8 -7 10 24.2435 13.3335 47 8 7 -10 7.53300 11.2858 44 8 7 -10 17.4108 14.8800 36 8 7 -10 24.5323 16.3604 34 8 7 -10 24.5535 15.1911 32 8 7 -11 239.074 22.9039 29 -8 -7 11 245.525 23.2967 47 8 7 -11 272.589 24.1980 36 8 7 -11 233.492 22.7142 34 8 7 -11 285.625 24.5026 32 8 7 -11 231.262 22.1115 30 8 8 0 48.1958 14.2570 33 -8 -8 1 601.441 34.4924 48 8 8 -1 562.638 33.8291 33 8 8 -1 608.518 35.0620 31 -8 -8 2 3408.84 79.2028 48 8 8 -2 3552.59 82.1921 33 8 8 -2 3392.25 79.0071 32 -8 -8 3 1218.05 47.5339 47 8 8 -3 1104.56 47.6144 33 8 8 -3 1129.88 47.6496 32 8 8 -3 1211.74 48.6518 30 -8 -8 4 313.494 26.6959 47 8 8 -4 297.351 27.9834 39 8 8 -4 224.762 23.7918 33 8 8 -4 264.194 25.8496 32 8 8 -4 294.491 26.6769 30 8 8 -5-12.9760 13.9128 30 -8 -8 5-2.36292 12.7089 47 8 8 -5 13.2272 15.4121 39 8 8 -5-27.5150 15.8939 33 8 8 -5-5.13685 15.4864 32 8 8 -6 30.6080 12.6785 30 -8 -8 6 25.4092 12.6722 47 8 8 -6 23.0590 13.2011 39 8 8 -6 38.5794 15.0757 36 8 8 -6 4.52968 14.1173 33 8 8 -6 9.34580 13.0628 32 8 8 -7 36.5878 12.0637 30 -8 -8 7 52.6021 13.9897 47 8 8 -7 37.2012 14.1601 39 8 8 -7 50.3501 14.8168 36 8 8 -7 22.0733 12.4709 33 8 8 -7 54.7841 15.1467 32 -8 -8 8 126.551 17.0707 47 9 0 5 39.0808 14.3223 23 9 0 4 316.766 26.4732 26 9 0 4 403.920 33.2219 23 9 0 3 29.5690 12.9939 26 9 0 3 21.3284 16.3235 23 9 0 2 423.280 37.1117 23 9 0 1-30.6759 21.2538 23 9 0 0 1500.69 72.2248 23 -9 0 0 1542.80 65.7057 22 9 0 -1-29.5024 22.9937 23 -9 0 1 3.79859 15.2815 22 9 0 -2 959.614 59.7704 23 -9 0 2 1041.40 57.8027 22 9 0 -3 12.6975 21.1733 23 -9 0 3 12.5708 16.9619 22 9 0 -4 46.9432 22.9993 54 9 0 -4 12.2042 18.6541 23 9 0 -5 19.0696 18.9342 54 9 0 -5-3.58867 19.1368 23 9 0 -6 789.230 51.9485 54 9 0 -6 709.555 52.1440 23 9 0 -7 32.2159 18.4923 54 9 0 -7 4.95507 18.4377 23 9 0 -8 14.2044 15.7408 54 9 0 -8 14.2984 16.7044 23 9 0 -9-19.7801 16.8953 23 9 0 -10 31.9689 16.1107 23 9 0 -11 4.02526 12.9272 23 -9 0 11-59.7606 20.6676 12 -9 0 12 474.210 34.7748 12 -9 0 13-18.7705 15.0637 12 -9 0 14 1131.72 45.6805 12 9 1 5 686.876 35.8210 26 9 -1 5 811.769 40.5069 23 9 1 5 784.000 36.9491 23 9 1 4 22.2813 14.2584 26 9 -1 4 16.6803 15.6437 23 9 1 4 33.3055 15.9637 23 9 -1 3 648.240 43.0060 23 9 1 3 603.100 40.2781 23 -9 -1 -3 658.639 38.6589 22 9 1 2 40.4629 16.1690 26 9 -1 2 21.8692 17.2525 23 9 1 2 20.9256 16.7340 23 -9 -1 -2-14.4681 15.5100 22 9 1 1 95.0943 21.0538 26 9 -1 1 104.474 23.7887 23 9 1 1 133.567 25.5618 23 -9 -1 -1 101.128 20.7567 22 9 -1 0 125.672 26.6005 23 9 1 0 153.776 27.5673 23 -9 -1 0 152.101 25.7362 22 9 -1 -1 145.304 29.3682 23 9 1 -1 129.610 28.9453 23 -9 -1 1 133.222 25.4400 22 9 -1 -2 1558.53 73.4109 23 9 1 -2 1473.87 73.5693 23 -9 -1 2 1519.99 71.3899 22 9 -1 -3 43.4650 24.5636 54 9 -1 -3 9.00078 19.6944 23 9 1 -3-18.5506 22.4177 23 -9 1 3 22.4261 17.9391 22 -9 -1 3 16.4958 17.8593 22 9 -1 -4 293.205 35.0988 54 9 -1 -4 350.496 37.5220 23 9 1 -4 291.731 36.3731 23 9 -1 -5 63.9639 21.3468 54 9 -1 -5 63.3881 22.9925 23 9 1 -5 29.1186 23.2156 23 9 1 -5 55.6615 20.7326 44 9 -1 -6 60.9263 21.5905 54 9 -1 -6 95.4813 23.5111 23 9 1 -6 108.504 28.2439 23 9 1 -6 82.4860 21.9847 44 9 -1 -7 245.845 31.4924 54 9 1 -7 311.017 36.7699 23 9 -1 -7 255.742 30.9215 23 9 1 -7 286.485 31.3873 44 9 -1 -8 67.4539 20.0464 54 9 -1 -8 19.3248 14.7125 23 9 1 -8 40.1492 20.7537 23 9 1 -8 78.1986 19.9491 44 9 -1 -9-11.0763 15.7797 54 9 -1 -9-6.96123 14.0871 23 9 1 -9 19.1000 18.2169 23 9 1 -9 10.6779 14.3662 44 9 -1 -10 3.61427 16.7998 54 9 1 -10 62.1358 20.2437 23 9 1 -10 60.1238 18.8917 44 -9 -1 10 12.3617 19.5618 12 9 1 -11 47.0647 18.4011 23 9 1 -11 28.8687 14.4191 44 -9 -1 11-4.84648 17.2082 12 9 1 -12 21.1117 13.6379 23 9 1 -12 0.95525 12.2256 44 -9 -1 12-7.78552 15.7096 12 -9 1 12 11.4768 15.3492 12 -9 -1 13 296.780 28.0144 12 -9 1 13 291.790 26.7083 12 -9 -1 14 1236.81 47.7914 12 -9 1 14 1225.31 45.8287 12 9 2 5 28.7671 12.5982 26 9 2 4 238.809 25.3132 26 9 -2 4 305.360 29.8870 23 9 2 4 255.251 22.6758 23 -9 -2 -4 311.171 26.3652 22 9 2 3 88.5313 19.6397 26 9 -2 3 111.264 21.5598 23 9 2 3 119.707 21.2694 23 -9 -2 -3 133.602 22.0074 22 9 2 2 85.3676 19.9523 26 9 -2 2 109.071 23.1008 23 9 2 2 86.6669 18.8628 23 -9 -2 -2 98.7048 20.4195 22 9 2 1-4.79093 16.6093 26 9 -2 1 26.3890 18.9586 23 9 2 1 42.1591 24.3927 23 -9 -2 -1-15.5798 14.5927 22 9 2 0 76.9835 19.7646 26 9 -2 0 136.135 25.6607 23 9 2 0 94.7881 21.8127 23 -9 -2 0 162.652 27.5844 22 9 2 -1 56.1331 18.8348 26 9 -2 -1 17.4861 18.0000 23 9 2 -1 18.3064 19.1612 23 -9 -2 1 7.29939 17.7258 22 9 2 -2 171.603 26.3149 26 9 -2 -2 141.337 26.2641 23 9 2 -2 168.471 30.9945 23 -9 -2 2 165.594 28.9551 22 9 -2 -3 889.598 57.6313 54 9 -2 -3 827.493 53.4286 23 9 2 -3 852.306 57.2533 23 -9 -2 3 774.741 53.2596 22 9 -2 -4-6.58767 23.5158 54 9 -2 -4 10.8058 18.2272 23 9 2 -4 26.0774 21.5855 23 9 2 -4 11.7783 17.7405 44 9 -2 -5 1278.87 67.4256 54 9 -2 -5 1161.50 59.7388 23 9 2 -5 1301.37 69.8735 23 9 2 -5 1298.67 64.0721 44 9 -2 -6 470.359 44.1202 54 9 -2 -6 486.193 39.0717 23 9 2 -6 425.690 43.3731 23 9 2 -6 439.619 39.6166 44 9 -2 -7 283.923 35.1909 54 9 -2 -7 266.061 29.0647 23 9 2 -7 295.984 37.6150 23 9 2 -7 290.308 33.7702 44 9 2 -7 262.948 31.0723 34 9 2 -8-6.66394 18.5528 29 9 -2 -8-14.6817 19.6842 54 9 2 -8 22.7476 21.9234 23 9 2 -8 16.2926 18.5837 44 9 2 -8-30.8552 17.5043 34 9 2 -9 1280.66 58.7886 29 9 -2 -9 1282.27 62.8863 54 9 2 -9 1276.43 64.1195 23 -9 -2 9 1304.10 58.4393 12 9 2 -9 1297.24 60.6628 44 9 2 -9 1221.88 56.2443 34 9 2 -10 2279.49 74.0969 29 9 -2 -10 2379.37 80.5425 54 9 2 -10 2305.34 80.7040 23 -9 -2 10 2245.33 74.7331 12 9 2 -10 2262.60 76.6185 44 9 2 -11 599.428 37.3802 29 9 -2 -11 606.187 40.4919 54 9 2 -11 630.044 41.7998 23 -9 -2 11 575.964 39.2995 12 9 2 -11 593.837 39.2549 44 9 -2 -12 1141.95 48.4612 54 9 2 -12 1071.52 48.8473 23 -9 -2 12 1103.76 50.2116 12 9 2 -12 1173.91 50.2795 44 9 2 -13 30.3746 12.5553 23 9 2 -13-12.9793 11.7759 44 -9 -2 13-16.5168 13.7724 12 -9 2 13 15.0171 11.7980 12 -9 -2 14 32.5654 13.6962 12 9 3 4 9.77621 11.8838 26 -9 -3 -4 18.6141 12.8447 22 9 3 3 97.4767 18.7336 26 9 -3 3 136.621 20.9054 23 -9 -3 -3 156.792 22.2085 22 9 3 2 68.5245 19.3832 26 9 3 2 54.7639 16.2790 23 -9 -3 -2 86.0071 18.0093 22 9 3 1 196.490 26.8728 26 9 -3 1 237.758 27.9643 23 9 3 1 173.408 23.8267 23 -9 -3 -1 241.999 29.3287 22 9 3 0 67.1405 20.9034 26 9 -3 0 60.5228 19.3227 23 9 3 0 48.8907 19.5561 23 -9 -3 0 40.9692 18.5644 22 9 3 -1 338.298 34.0290 26 9 -3 -1 390.283 36.4186 23 9 3 -1 402.610 37.4360 23 -9 -3 1 392.897 37.0538 22 9 -3 -2 439.788 37.2176 23 9 3 -2 422.146 39.9156 23 -9 -3 2 410.329 40.9151 22 9 3 -2 336.897 32.2425 30 9 -3 -3 53.9865 25.4290 54 9 -3 -3 45.4872 17.7390 23 9 3 -3 32.9601 20.3801 23 -9 -3 3 44.9805 20.7572 22 9 3 -3 97.7587 20.3588 32 9 3 -3-14.9557 19.9058 30 9 -3 -4 1622.50 74.9440 54 9 -3 -4 1540.13 64.6411 23 9 3 -4 1617.58 73.7074 23 9 3 -4 1523.89 69.3525 44 -9 -3 4 1580.10 71.3902 22 9 3 -4 1537.34 63.7808 32 9 3 -4 1478.63 64.9463 30 9 3 -5 42.3616 17.2185 30 9 -3 -5 87.6066 25.2813 54 9 3 -5 85.5918 26.7136 23 9 3 -5 67.4443 22.2573 44 9 3 -6 73.4761 20.1514 30 9 -3 -6 188.187 31.9044 54 9 3 -6 204.979 32.3328 23 9 3 -6 160.679 28.9130 44 9 3 -6 173.386 30.5290 34 9 3 -7 4025.10 109.063 29 9 -3 -7 4267.56 115.369 54 9 3 -7 3970.57 112.188 23 9 3 -7 4050.01 108.932 44 9 3 -7 3877.92 102.213 36 9 3 -7 4158.24 109.597 34 9 3 -7 3942.36 102.284 30 9 3 -8 2754.84 89.0628 29 9 -3 -8 2711.58 91.7174 54 9 3 -8 2819.09 92.6264 23 9 3 -8 2820.31 90.0359 44 9 3 -8 2661.23 81.4347 36 9 3 -8 2706.89 86.2155 34 9 3 -8 2622.34 81.7998 30 9 3 -9 324.608 34.2885 29 9 -3 -9 346.742 35.1235 54 9 3 -9 404.684 38.3473 23 -9 -3 9 386.244 33.5399 12 9 3 -9 302.625 32.7924 44 9 3 -9 343.015 32.8610 34 9 3 -9 288.725 29.0908 30 9 3 -10 1203.12 55.0953 29 9 -3 -10 1210.06 58.0413 54 -9 -3 10 1154.94 53.2324 12 9 3 -10 1147.65 54.5225 44 9 3 -10 1187.77 53.1124 34 9 3 -10 1121.61 49.6760 30 9 3 -11 12.4530 11.7098 30 9 3 -11 43.2632 16.3631 29 9 -3 -11 64.5070 19.1183 54 9 3 -11 61.8702 18.2826 44 -9 -3 11 43.0699 16.4714 12 9 3 -11 64.6661 16.4739 34 9 3 -12 203.307 21.5115 29 9 -3 -12 254.679 25.5708 54 9 3 -12 207.416 23.5491 23 9 3 -12 239.424 24.3944 44 -9 -3 12 205.647 24.5974 12 9 3 -13 5.62720 10.8631 44 -9 -3 13-0.71033 13.4884 12 9 4 3 143.352 19.9435 26 -9 -4 -3 182.892 21.4446 22 9 4 2 25.8253 15.1195 26 -9 -4 -2 58.7368 17.2309 22 9 4 1 157.290 23.1508 26 9 -4 1 185.584 22.6194 23 -9 -4 -1 187.670 24.6314 22 9 4 0 1.85482 13.7287 26 9 -4 0-3.06627 12.8816 23 9 4 0 6.11643 13.0207 23 -9 -4 0 17.2155 16.8551 22 9 4 -1 59.9034 19.6519 26 9 -4 -1 58.2161 15.9963 23 9 4 -1 93.8677 20.9957 23 -9 -4 1 64.8737 19.8917 22 9 -4 -2 94.9191 18.7444 23 9 4 -2 116.880 23.9622 23 -9 -4 2 118.943 24.1610 22 9 4 -2 102.243 22.9534 30 9 -4 -3 705.064 48.9146 54 9 4 -3 636.548 44.2998 23 -9 -4 3 753.464 48.4366 22 9 4 -3 732.367 45.1431 32 9 4 -3 630.861 42.8134 30 9 -4 -4 810.176 52.5704 54 9 4 -4 769.813 49.1743 23 -9 -4 4 760.545 49.3863 22 9 4 -4 802.575 46.6144 32 9 4 -4 737.081 45.8949 30 9 4 -5-9.65192 18.0874 30 9 -4 -5 71.3917 23.0754 54 9 4 -5 17.2869 19.1942 23 9 4 -5 27.4818 19.2085 44 -9 -4 5 21.2920 16.5109 22 9 4 -5 7.29289 16.8694 32 9 4 -6 146.414 24.0593 30 9 -4 -6 159.941 28.1579 54 9 4 -6 185.245 28.5571 23 9 4 -6 153.391 26.8679 44 -9 -4 6 155.423 25.3723 22 9 4 -6 175.833 28.0394 36 9 4 -6 186.053 28.7116 34 9 4 -6 153.055 22.9516 32 9 4 -7 6.00539 15.4229 30 9 -4 -7-15.6532 20.6038 54 9 4 -7 2.27335 19.2464 23 9 4 -7-15.7002 18.2356 44 9 4 -7-6.75497 17.2494 36 9 4 -7-8.86485 18.0723 34 9 4 -7-9.80681 16.3803 32 9 4 -8 71.0206 19.6334 30 9 4 -8 83.6063 22.5341 29 9 -4 -8 44.6495 19.7049 54 9 4 -8 62.7313 21.9402 23 9 4 -8 70.9201 20.8378 44 9 4 -8 55.7406 18.7058 36 9 4 -8 93.4504 23.3415 34 9 4 -8 88.7273 18.8082 32 9 4 -9 9.36247 16.5749 30 9 4 -9 23.3904 19.1409 29 9 -4 -9 27.6865 18.7348 54 9 4 -9 30.8638 19.6333 44 -9 -4 9 53.0744 18.0580 12 9 4 -9 10.0619 13.3583 36 9 4 -9 37.1815 19.7780 34 9 4 -10 1997.78 66.7612 29 9 -4 -10 2027.82 69.9188 54 -9 -4 10 2019.81 64.5370 12 9 4 -10 1956.92 67.0018 44 9 4 -10 1960.44 64.9615 34 9 4 -10 1900.72 62.6033 30 9 4 -11 12.0511 12.8896 30 9 4 -11 17.0542 15.0335 29 9 -4 -11 11.4019 14.5012 54 9 4 -11 12.2728 13.4713 44 -9 -4 11-18.7383 13.8171 12 9 4 -11 21.6359 14.6385 34 9 -4 -12 624.117 34.9013 54 -9 -4 12 542.678 32.2423 12 9 4 -12 582.887 33.9301 23 9 4 -12 648.328 35.1601 44 9 5 2 51.0744 14.5873 26 -9 -5 -2 56.3695 14.4241 22 9 5 1 350.160 28.8525 26 -9 -5 -1 346.144 28.0574 22 9 5 0 386.658 31.0261 26 -9 -5 0 463.317 33.1957 22 9 5 -1 502.975 36.0405 26 9 5 -1 489.857 31.2676 33 9 5 -2 334.887 27.8593 23 -9 -5 2 354.280 31.2691 22 9 5 -2 290.201 26.3236 33 9 -5 -3 110.584 22.0960 54 9 5 -3 60.4952 16.8951 23 -9 -5 3 84.6280 20.5144 22 9 5 -3 59.3347 15.5738 33 9 5 -3 88.0664 20.9895 32 9 5 -3 39.4519 16.8658 30 9 5 -4 119.828 22.3133 30 9 -5 -4 131.705 23.2082 54 9 5 -4 134.377 21.5069 23 -9 -5 4 135.938 22.4918 22 9 5 -4 104.878 18.2312 33 9 5 -4 136.803 21.3848 32 9 5 -5 37.8526 16.7670 30 9 -5 -5 37.0193 18.6565 54 9 5 -5 16.2597 15.6829 23 -9 -5 5 14.8871 13.8031 22 9 5 -5 26.8295 12.9730 33 9 5 -5 21.8638 15.0797 32 9 5 -6 126.860 20.7673 30 9 -5 -6 165.707 25.4030 54 9 5 -6 130.940 22.5290 23 9 5 -6 185.735 25.6549 44 -9 -5 6 136.820 20.8806 22 9 5 -6 173.010 25.3413 36 9 5 -6 115.259 19.7668 32 9 5 -7 62.3689 17.1587 30 9 -5 -7 58.5876 18.6235 54 -9 -5 7 17.9957 11.6448 47 9 5 -7 83.0843 19.7010 23 9 5 -7 52.3306 19.2011 44 -9 -5 7 48.6840 15.0051 22 9 5 -7 51.8255 17.3957 36 9 5 -7 47.9693 19.2021 34 9 5 -7 28.6127 13.9718 32 9 5 -8 340.538 30.3351 23 -9 -5 8 376.291 26.9471 47 9 5 -8 383.625 31.5199 44 -9 -5 8 324.225 27.2264 22 9 5 -8 321.225 28.5701 36 9 5 -8 351.811 30.3885 34 9 5 -8 301.318 25.7317 32 9 5 -8 327.876 29.2959 30 9 5 -9 21.3593 13.1613 30 9 5 -9 36.7111 17.2609 29 9 -5 -9-2.19224 14.1621 54 -9 -5 9-17.9840 13.6922 12 -9 -5 9 1.03469 10.5269 47 9 5 -9 4.96345 13.2089 23 9 5 -9 14.5049 14.2145 44 -9 -5 9 9.87284 10.6035 22 9 5 -9-2.25489 12.8018 36 9 5 -9 16.1313 15.5098 34 9 5 -10 433.440 30.0243 29 9 -5 -10 460.049 31.4841 54 9 5 -10 367.960 28.4344 23 9 5 -10 387.301 29.2382 44 9 5 -10 391.061 28.5159 34 9 5 -10 396.254 28.2763 30 9 6 -1 105.744 17.9323 26 -9 -6 3 79.1617 14.8647 22 9 6 -3 96.5832 18.7562 32 9 6 -4 29.7989 14.8206 32 9 6 -4 37.1214 14.5458 30 9 6 -5 1.98561 12.8503 30 9 -6 -5 34.2583 14.6170 54 9 6 -5 1.95381 13.2777 32 9 6 -6 48.7466 14.2591 30 9 -6 -6 93.3324 16.8856 54 9 6 -6 75.8440 16.8952 32 9 6 -7 16.0375 12.2839 30 9 -6 -7 11.4047 11.7785 54 9 6 -8-6.96818 11.9151 44 10 0 0 41.7024 13.0722 23 10 0 -1-6.34582 12.3239 23 10 0 -2 6.14659 13.3243 23 10 0 -3-6.28545 13.1575 23 10 0 -4 4.51243 14.0342 23 -10 0 4 13.1516 11.1502 22 10 0 -5-10.5952 13.2074 23 -10 0 5-1.29599 11.4660 22 10 0 -6 27.2670 14.4911 23 -10 0 6 60.9808 14.9410 22 10 0 -7-24.0121 13.3647 23 -10 0 7-15.7362 12.9036 22 -10 0 8 85.5421 15.7849 22 10 -1 -1 166.441 20.0487 23 10 1 -1 119.415 17.6629 23 10 -1 -2 164.998 21.2786 23 10 1 -2 151.660 20.9929 23 -10 -1 2 140.451 18.2112 22 10 -1 -3 189.622 21.9761 23 10 1 -3 215.231 24.3686 23 -10 -1 3 249.889 23.7214 22 10 -1 -4-3.89073 11.8793 23 10 1 -4 23.9313 15.0748 23 -10 -1 4 21.2482 13.4429 22 10 -1 -5 42.6005 13.4408 23 10 1 -5 25.0611 13.9878 23 -10 -1 5 65.0322 17.2464 22 10 -1 -6 28.1697 12.1505 23 10 1 -6 39.3128 15.0430 23 -10 -1 6 39.6608 14.5051 22 10 1 -7 347.587 28.3314 23 -10 -1 7 330.666 27.5024 22 10 1 -8 1052.69 43.8353 23 -10 -1 8 1085.51 45.5213 22 10 2 -2 42.2285 15.3877 23 -10 -2 2 4.12247 11.0431 22 10 2 -3 63.7064 16.2728 23 -10 -2 3 93.1588 17.0602 22 10 2 -4 385.393 29.5782 23 -10 -2 4 439.013 30.4410 22 10 2 -5 31.6767 14.3482 23 -10 -2 5 20.8504 13.4814 22 10 2 -6 208.289 23.1654 23 -10 -2 6 234.478 23.7249 22 10 2 -7 65.8024 16.5443 23 -10 -2 7 75.5366 16.6051 22 10 2 -8 137.058 19.5367 23 -10 -2 8 123.590 18.2551 22 10 3 -4 146.002 19.3549 23 -10 -3 4 157.592 19.2602 22 10 3 -5 91.7905 16.6115 23 -10 -3 5 90.3271 16.2169 22 10 3 -6 205.557 21.6034 23 -10 -3 6 231.147 22.0109 22 0 0 0 0.00 0.00 0 TITL N-metil-I_3 in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 1.54184 8.334610 10.797952 17.615121 90.0000 103.2625 90.0000 ZERR 7.00 0.000160 0.000221 0.000343 0.0000 0.0019 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O UNIT 63.00 49.00 7.00 21.00 TREF HKLF 4 END ; _shelx_hkl_checksum 30510 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag C11 C 0.37945(16) 0.88804(12) 0.49981(8) 0.0448(3) Uani 1 1 d C12 C 0.38620(17) 0.91059(13) 0.58743(8) 0.0481(3) Uani 1 1 d C13 C 0.48712(18) 0.80977(14) 0.62839(9) 0.0517(3) Uani 1 1 d C14 C 0.5360(3) 0.7811(2) 0.70657(12) 0.0739(5) Uani 1 1 d C15 C 0.6304(3) 0.6748(3) 0.72625(16) 0.0938(8) Uani 1 1 d C16 C 0.6742(3) 0.6028(2) 0.66958(19) 0.0921(8) Uani 1 1 d C17 C 0.6271(2) 0.63103(16) 0.59060(15) 0.0716(5) Uani 1 1 d C18 C 0.53181(17) 0.73557(13) 0.57141(10) 0.0506(3) Uani 1 1 d C19 C 0.4879(2) 0.7294(2) 0.42384(12) 0.0681(5) Uani 1 1 d N1 N 0.46704(14) 0.78380(11) 0.49628(7) 0.0490(3) Uani 1 1 d O11 O 0.30774(14) 0.95186(11) 0.44549(6) 0.0595(3) Uani 1 1 d O12 O 0.31623(17) 0.99496(12) 0.61062(8) 0.0706(4) Uani 1 1 d H14 H 0.502(3) 0.833(3) 0.7474(16) 0.102(8) Uiso 1 1 d H15 H 0.658(4) 0.653(3) 0.7773(18) 0.107(9) Uiso 1 1 d H16 H 0.742(4) 0.526(3) 0.6794(18) 0.122(10) Uiso 1 1 d H17 H 0.661(3) 0.577(2) 0.5519(15) 0.097(8) Uiso 1 1 d H19A H 0.422(4) 0.651(3) 0.4188(17) 0.106(9) Uiso 1 1 d H19B H 0.462(5) 0.789(3) 0.376(2) 0.163(15) Uiso 1 1 d H19C H 0.596(4) 0.700(3) 0.4309(17) 0.110(9) Uiso 1 1 d C21 C 0.12081(18) 0.62647(14) 0.53216(9) 0.0516(3) Uani 1 1 d C22 C 0.18850(18) 0.56322(13) 0.61227(10) 0.0531(3) Uani 1 1 d C23 C 0.13817(16) 0.64347(13) 0.66917(9) 0.0466(3) Uani 1 1 d C24 C 0.1643(2) 0.63670(16) 0.74938(10) 0.0589(4) Uani 1 1 d C25 C 0.0988(2) 0.72869(19) 0.78786(10) 0.0674(5) Uani 1 1 d C26 C 0.0112(2) 0.82520(18) 0.74615(11) 0.0670(4) Uani 1 1 d C27 C -0.0151(2) 0.83457(14) 0.66549(10) 0.0561(4) Uani 1 1 d C28 C 0.04974(16) 0.74141(12) 0.62783(8) 0.0437(3) Uani 1 1 d C29 C -0.0515(2) 0.81230(18) 0.48786(11) 0.0623(4) Uani 1 1 d N2 N 0.04059(15) 0.72986(11) 0.54723(7) 0.0492(3) Uani 1 1 d O21 O 0.13703(18) 0.59092(13) 0.46890(8) 0.0717(4) Uani 1 1 d O22 O 0.26427(18) 0.46749(12) 0.62048(9) 0.0793(4) Uani 1 1 d H24 H 0.232(3) 0.572(2) 0.7793(13) 0.081(6) Uiso 1 1 d H25 H 0.118(3) 0.728(2) 0.8437(17) 0.100(8) Uiso 1 1 d H26 H -0.034(3) 0.893(2) 0.7760(14) 0.092(7) Uiso 1 1 d H27 H -0.080(3) 0.900(2) 0.6374(12) 0.073(6) Uiso 1 1 d H29A H -0.084(3) 0.767(2) 0.4390(16) 0.094(8) Uiso 1 1 d H29B H 0.013(3) 0.881(2) 0.4796(15) 0.094(8) Uiso 1 1 d H29C H -0.159(3) 0.837(2) 0.5029(14) 0.085(7) Uiso 1 1 d loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C11 0.0451(6) 0.0377(6) 0.0512(7) -0.0034(5) 0.0104(5) -0.0017(5) C12 0.0524(7) 0.0428(7) 0.0507(7) -0.0039(5) 0.0150(6) -0.0012(5) C13 0.0497(7) 0.0511(8) 0.0543(8) 0.0073(6) 0.0120(6) -0.0047(6) C14 0.0701(10) 0.0899(14) 0.0606(10) 0.0218(9) 0.0127(8) -0.0080(9) C15 0.0757(12) 0.1055(18) 0.0887(15) 0.0515(15) -0.0051(11) -0.0114(12) C16 0.0626(10) 0.0638(12) 0.139(2) 0.0420(14) -0.0004(12) 0.0034(9) C17 0.0526(8) 0.0448(8) 0.1128(16) 0.0100(9) 0.0099(9) 0.0040(6) C18 0.0416(6) 0.0386(7) 0.0706(9) 0.0031(6) 0.0111(6) -0.0037(5) C19 0.0669(10) 0.0684(11) 0.0715(11) -0.0267(9) 0.0213(8) 0.0008(8) N1 0.0506(6) 0.0409(6) 0.0557(7) -0.0083(5) 0.0127(5) 0.0004(5) O11 0.0656(6) 0.0553(6) 0.0537(6) 0.0044(5) 0.0059(5) 0.0060(5) O12 0.0856(8) 0.0620(7) 0.0670(7) -0.0127(6) 0.0234(6) 0.0157(6) C21 0.0531(7) 0.0473(8) 0.0592(8) -0.0060(6) 0.0233(6) -0.0010(6) C22 0.0512(7) 0.0411(7) 0.0701(9) -0.0006(6) 0.0199(6) 0.0042(6) C23 0.0445(6) 0.0399(7) 0.0564(8) 0.0006(5) 0.0134(6) -0.0011(5) C24 0.0570(8) 0.0616(9) 0.0562(8) 0.0072(7) 0.0088(7) -0.0031(7) C25 0.0718(10) 0.0791(12) 0.0519(9) -0.0075(8) 0.0154(7) -0.0047(8) C26 0.0731(10) 0.0667(10) 0.0652(10) -0.0191(8) 0.0242(8) 0.0016(8) C27 0.0595(8) 0.0446(8) 0.0667(9) -0.0048(6) 0.0194(7) 0.0062(6) C28 0.0440(6) 0.0383(6) 0.0500(7) -0.0019(5) 0.0135(5) -0.0014(5) C29 0.0609(9) 0.0650(10) 0.0601(9) 0.0136(8) 0.0119(7) 0.0069(8) N2 0.0541(6) 0.0451(6) 0.0500(6) 0.0025(5) 0.0150(5) 0.0050(5) O21 0.0838(8) 0.0743(8) 0.0660(7) -0.0130(6) 0.0358(6) 0.0011(6) O22 0.0859(9) 0.0542(7) 0.1005(10) 0.0020(6) 0.0271(7) 0.0279(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle O11 C11 N1 127.45(14) O11 C11 C12 126.29(13) N1 C11 C12 106.26(12) O12 C12 C13 131.75(15) O12 C12 C11 123.18(14) C13 C12 C11 105.05(12) C14 C13 C18 121.41(17) C14 C13 C12 131.71(17) C18 C13 C12 106.87(13) C13 C14 C15 117.1(2) C16 C15 C14 120.9(2) C15 C16 C17 122.63(19) C18 C17 C16 116.1(2) C17 C18 C13 121.77(17) C17 C18 N1 127.48(17) C13 C18 N1 110.74(13) C11 N1 C18 111.06(12) C11 N1 C19 123.58(14) C18 N1 C19 125.36(14) O21 C21 N2 127.03(16) O21 C21 C22 126.93(14) N2 C21 C22 106.04(12) O22 C22 C23 130.86(17) O22 C22 C21 123.96(15) C23 C22 C21 105.17(12) C24 C23 C28 120.97(14) C24 C23 C22 132.02(14) C28 C23 C22 107.02(13) C25 C24 C23 118.42(16) C26 C25 C24 120.02(16) C25 C26 C27 122.54(16) C28 C27 C26 116.75(15) C27 C28 C23 121.30(14) C27 C28 N2 127.68(13) C23 C28 N2 111.02(12) C21 N2 C28 110.75(12) C21 N2 C29 124.45(14) C28 N2 C29 124.67(13) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance C11 O11 1.2186(18) C11 N1 1.3507(18) C11 C12 1.5509(19) C12 O12 1.2025(18) C12 C13 1.461(2) C13 C14 1.379(2) C13 C18 1.400(2) C14 C15 1.389(4) C15 C16 1.379(4) C16 C17 1.390(4) C17 C18 1.377(2) C18 N1 1.409(2) C19 N1 1.451(2) C21 O21 1.2150(19) C21 N2 1.3584(19) C21 C22 1.553(2) C22 O22 1.2027(19) C22 C23 1.458(2) C23 C24 1.381(2) C23 C28 1.3949(19) C24 C25 1.383(3) C25 C26 1.383(3) C26 C27 1.391(3) C27 C28 1.382(2) C28 N2 1.4098(19) C29 N2 1.452(2) loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A C17 H17 O21 0.99(3) 2.55(3) 3.414(2) 145(2) 3_666 C19 H19C O22 0.94(3) 2.43(3) 3.183(2) 137(2) 3_666 C27 H27 O11 0.96(2) 2.65(2) 3.592(2) 168.6(18) 3_576