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Information card for entry 4036248
Preview
| Coordinates | 4036248.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C16 H22.25 O7.13 |
|---|---|
| Calculated formula | C16 H22.26 O7.13 |
| Title of publication | General Stereodivergent Enantioselective Total Synthetic Approach toward Macrosphelides A-G and M. |
| Authors of publication | Häcker, Christine; Plietker, Bernd |
| Journal of publication | The Journal of organic chemistry |
| Year of publication | 2015 |
| Journal volume | 80 |
| Journal issue | 16 |
| Pages of publication | 8055 - 8064 |
| a | 5.8884 ± 0.0007 Å |
| b | 14.8186 ± 0.0016 Å |
| c | 19.816 ± 0.002 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 1729.1 ± 0.3 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 3 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0414 |
| Residual factor for significantly intense reflections | 0.0307 |
| Weighted residual factors for significantly intense reflections | 0.0644 |
| Weighted residual factors for all reflections included in the refinement | 0.0675 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.019 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 234448 (current) | 2019-11-23 | cif/ Adding structures of 4036248 via cif-deposit CGI script. |
4036248.cif |
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Users of the data should acknowledge the original authors of the
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