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Information card for entry 4037826
Preview
| Coordinates | 4037826.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H21 Cl O4 |
|---|---|
| Calculated formula | C24 H21 Cl O4 |
| Title of publication | Synthesis and Rhodium(II)-Mediated Cascade Cyclopropanation/Rearrangement/Isomerization of Diazo 2,3,5-Trisubstituted Furans: the Construction of Pentasubstituted Aromatic Compounds. |
| Authors of publication | Zhang, Jianfang; Yang, Qin; Zhu, Yang; Wang, Jianbo; Deng, Guisheng |
| Journal of publication | The Journal of organic chemistry |
| Year of publication | 2020 |
| a | 23.621 ± 0.006 Å |
| b | 10.647 ± 0.003 Å |
| c | 16.385 ± 0.004 Å |
| α | 90° |
| β | 93.303 ± 0.013° |
| γ | 90° |
| Cell volume | 4113.9 ± 1.9 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296.15 K |
| Number of distinct elements | 4 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0609 |
| Residual factor for significantly intense reflections | 0.0483 |
| Weighted residual factors for significantly intense reflections | 0.1282 |
| Weighted residual factors for all reflections included in the refinement | 0.14 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.035 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 246982 (current) | 2020-01-18 | cif/ Adding structures of 4037826 via cif-deposit CGI script. |
4037826.cif |
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