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Information card for entry 4038830
Preview
| Coordinates | 4038830.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H39 Li N3 P |
|---|---|
| Calculated formula | C24 H39 Li N3 P |
| Title of publication | P-chirogenic Diphosphazanes with Axially Chiral Substituents and their Use in Rh-catalyzed Asymmetric Hydrogenation. |
| Authors of publication | Moritz, Jan-Ole; Chakrabortty, Soumyadeep; Müller, Bernd H; Spannenberg, Anke; Kamer, Paul C. J. |
| Journal of publication | The Journal of organic chemistry |
| Year of publication | 2020 |
| a | 8.8123 ± 0.0002 Å |
| b | 30.9425 ± 0.0007 Å |
| c | 9.2575 ± 0.0002 Å |
| α | 90° |
| β | 98.8763 ± 0.0008° |
| γ | 90° |
| Cell volume | 2494.05 ± 0.1 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.034 |
| Residual factor for significantly intense reflections | 0.0337 |
| Weighted residual factors for significantly intense reflections | 0.0908 |
| Weighted residual factors for all reflections included in the refinement | 0.0911 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.016 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 256679 (current) | 2020-09-24 | cif/ Adding structures of 4038830 via cif-deposit CGI script. |
4038830.cif |
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Users of the data should acknowledge the original authors of the
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