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Information card for entry 4038841
Preview
| Coordinates | 4038841.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C21 H18 N2 O2 |
|---|---|
| Calculated formula | C21 H18 N2 O2 |
| Title of publication | Palladium-catalyzed Monoarylation of Arylhydrazines with Aryl Tosylates. |
| Authors of publication | Huang, Yange; Choy, Pui Ying; Wang, Junya; Tse, Man Kin; Sun, Raymond Wai-Yin; Chan, Albert Sun Chi; Kwong, Fuk Yee |
| Journal of publication | The Journal of organic chemistry |
| Year of publication | 2020 |
| a | 7.327 ± 0.004 Å |
| b | 15.647 ± 0.009 Å |
| c | 7.711 ± 0.004 Å |
| α | 90° |
| β | 96.781 ± 0.014° |
| γ | 90° |
| Cell volume | 877.8 ± 0.8 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 7 |
| Hermann-Mauguin space group symbol | P 1 c 1 |
| Hall space group symbol | P -2yc |
| Residual factor for all reflections | 0.1026 |
| Residual factor for significantly intense reflections | 0.0662 |
| Weighted residual factors for significantly intense reflections | 0.1419 |
| Weighted residual factors for all reflections included in the refinement | 0.1596 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.056 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 256779 (current) | 2020-09-26 | cif/ Adding structures of 4038841 via cif-deposit CGI script. |
4038841.cif |
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Users of the data should acknowledge the original authors of the
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