#------------------------------------------------------------------------------ #$Date: 2022-12-24 17:23:11 +0200 (Sat, 24 Dec 2022) $ #$Revision: 280034 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/03/90/4039013.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4039013 _cell_angle_alpha 90.000 _cell_angle_beta 110.054 _cell_angle_gamma 90.000 _cell_length_a 19.7264 _cell_length_b 6.2955 _cell_length_c 8.8067 _exptl_crystal_F_000 500.00 _reflns_d_resolution_high 0.8199 _cod_data_source_file 4-jw2390.fcf _cod_data_source_block jw2390 _shelx_title ' jw2390_a.res in C2/m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 179.08 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1253.98 1232.03 10.58 o 4 0 0 1908.27 1963.36 16.24 o 6 0 0 3107.49 3105.34 27.60 o 8 0 0 758.98 915.79 9.20 o 10 0 0 1130.50 1377.24 14.99 o 12 0 0 1.30 1.74 0.66 o 14 0 0 25.06 28.00 1.96 o 16 0 0 60.62 64.30 2.24 o 18 0 0 301.99 362.59 5.40 o 20 0 0 486.96 482.17 11.23 o 22 0 0 143.57 131.28 2.82 o 1 1 0 3218.00 3182.82 17.93 o 3 1 0 3782.25 3791.06 52.45 o 5 1 0 5101.56 5076.01 30.92 o 7 1 0 451.98 477.01 3.89 o 9 1 0 381.79 443.49 3.86 o 11 1 0 485.58 537.65 5.11 o 13 1 0 1768.80 1615.38 17.08 o 15 1 0 7.00 7.70 0.76 o 17 1 0 623.04 616.05 5.62 o 19 1 0 435.39 606.27 26.21 o 21 1 0 15.84 13.46 0.71 o 2 2 0 1121.97 1211.14 7.92 o 4 2 0 1476.91 1580.50 11.40 o 6 2 0 1898.38 1916.66 13.29 o 8 2 0 508.16 631.81 5.65 o 10 2 0 774.43 862.27 7.92 o 12 2 0 0.22 2.12 0.57 o 14 2 0 14.07 13.38 0.81 o 16 2 0 45.00 46.76 1.41 o 18 2 0 284.70 322.01 3.63 o 20 2 0 421.75 429.15 8.60 o 1 3 0 1731.50 1701.18 10.89 o 3 3 0 860.28 944.57 7.27 o 5 3 0 1945.04 2031.97 14.54 o 7 3 0 339.64 355.38 3.99 o 9 3 0 192.92 193.42 3.06 o 11 3 0 234.08 244.06 2.40 o 13 3 0 1216.53 1169.84 8.42 o 15 3 0 10.77 9.88 0.65 o 17 3 0 440.81 440.64 4.26 o 19 3 0 317.76 290.04 13.59 o 0 4 0 32068.24 27682.22 305.62 o 2 4 0 571.59 592.91 5.98 o 4 4 0 669.84 670.16 6.82 o 6 4 0 773.19 755.86 7.64 o 8 4 0 281.19 327.98 3.07 o 10 4 0 333.45 375.71 3.48 o 12 4 0 0.35 1.14 0.41 o 14 4 0 7.25 6.95 0.51 o 16 4 0 28.03 26.07 1.14 o 18 4 0 185.93 185.41 2.12 o 3 5 0 311.77 338.84 5.63 o 5 5 0 831.37 853.11 7.01 o 7 5 0 1185.39 1167.68 11.95 o 9 5 0 74.71 73.26 1.56 o 11 5 0 93.11 97.07 1.62 o 13 5 0 738.01 681.93 5.54 o 15 5 0 8.46 6.99 0.47 o 17 5 0 233.92 215.36 2.54 o 4 6 0 249.50 250.77 4.62 o 6 6 0 513.90 574.44 8.68 o 8 6 0 169.74 174.71 2.30 o 10 6 0 143.68 145.57 1.97 o 12 6 0 0.15 0.05 0.35 o 14 6 0 4.70 3.79 0.35 o 7 7 0 71.29 75.59 5.43 o 9 7 0 29.58 27.90 5.08 o -22 0 1 77.65 77.73 1.99 o -20 0 1 770.43 762.39 12.71 o -18 0 1 4722.06 4549.19 50.33 o -16 0 1 454.03 429.90 6.05 o -14 0 1 712.86 664.70 10.52 o -12 0 1 3325.79 3433.93 39.39 o -10 0 1 1762.32 2133.07 21.75 o -8 0 1 2274.02 2459.55 23.15 o -6 0 1 1071.55 1053.26 9.76 o -4 0 1 261.77 281.48 2.66 o -2 0 1 1191.59 1139.73 9.37 o 0 0 1 15030.68 12791.22 443.61 o 2 0 1 49.45 62.25 0.91 o 4 0 1 1138.81 1141.67 10.30 o 6 0 1 4884.82 5108.57 47.22 o 8 0 1 346.68 330.87 4.17 o 10 0 1 3745.47 4019.19 47.56 o 12 0 1 1245.24 1220.86 17.54 o 14 0 1 2.97 3.16 0.74 o 16 0 1 871.84 841.93 9.95 o 18 0 1 0.14 1.00 0.71 o 20 0 1 288.86 290.66 9.29 o -23 1 1 50.90 53.13 1.63 o -21 1 1 0.13 0.33 0.38 o -19 1 1 849.18 888.58 7.38 o -17 1 1 922.66 877.26 7.69 o -15 1 1 21.12 14.91 0.88 o -13 1 1 2248.28 1948.37 18.11 o -11 1 1 129.57 108.25 1.64 o -9 1 1 420.44 500.68 4.29 o -7 1 1 423.91 447.54 3.54 o -5 1 1 1330.67 1321.17 8.49 o -3 1 1 3186.33 2898.17 31.10 o -1 1 1 2009.65 1987.31 13.63 o 1 1 1 481.92 487.15 3.73 o 3 1 1 1573.98 1507.91 15.34 o 5 1 1 8640.25 8826.71 56.38 o 7 1 1 680.59 755.13 5.90 o 9 1 1 20.86 21.35 0.80 o 11 1 1 2809.67 2749.71 24.17 o 13 1 1 338.07 325.27 5.30 o 15 1 1 105.72 104.25 1.93 o 17 1 1 31.65 34.66 1.16 o 19 1 1 19.07 20.92 0.78 o -22 2 1 67.36 63.88 1.11 o -20 2 1 681.66 686.04 9.00 o -18 2 1 4072.71 3887.75 28.62 o -16 2 1 363.19 367.82 4.15 o -14 2 1 510.10 512.95 4.62 o -12 2 1 2848.42 2802.02 22.21 o -10 2 1 1170.47 1299.78 11.08 o -8 2 1 1364.01 1498.78 10.64 o -6 2 1 706.28 722.65 5.62 o -4 2 1 178.87 203.09 2.01 o -2 2 1 480.85 542.81 4.05 o 0 2 1 7612.34 7836.54 46.51 o 2 2 1 164.43 173.29 1.75 o 4 2 1 1130.24 1141.75 8.76 o 6 2 1 2906.40 3041.61 22.28 o 8 2 1 314.43 292.44 3.52 o 10 2 1 2963.25 3031.10 23.75 o 12 2 1 1045.67 1020.57 7.70 o 14 2 1 2.63 2.95 0.55 o 16 2 1 718.75 714.34 6.70 o 18 2 1 0.11 1.55 0.45 o 20 2 1 8.20 6.92 0.69 o -21 3 1 0.84 0.30 0.35 o -19 3 1 601.89 600.21 4.94 o -17 3 1 678.43 683.32 5.66 o -15 3 1 15.37 12.14 0.62 o -13 3 1 1478.79 1425.11 9.15 o -11 3 1 78.98 67.25 2.08 o -9 3 1 276.07 287.38 3.48 o -7 3 1 382.51 423.60 4.41 o -5 3 1 444.62 457.30 4.22 o -3 3 1 764.46 801.83 6.08 o -1 3 1 764.48 791.63 5.19 o 1 3 1 181.77 183.10 2.00 o 3 3 1 390.17 338.82 3.44 o 5 3 1 3728.30 3674.93 28.37 o 7 3 1 616.87 650.75 7.04 o 9 3 1 53.27 54.94 1.87 o 11 3 1 1558.42 1531.11 9.41 o 13 3 1 188.08 193.41 2.21 o 15 3 1 86.33 86.49 1.63 o 17 3 1 20.71 21.88 0.86 o 19 3 1 12.64 12.33 0.55 o -18 4 1 2644.78 2446.14 16.15 o -16 4 1 232.79 242.99 2.58 o -14 4 1 293.90 299.91 2.87 o -12 4 1 1639.42 1637.41 10.51 o -10 4 1 480.20 562.21 4.68 o -8 4 1 624.99 671.97 6.59 o -6 4 1 299.02 280.60 4.14 o -4 4 1 74.23 86.85 2.11 o -2 4 1 114.33 140.26 2.53 o 0 4 1 1971.85 2008.96 17.65 o 2 4 1 93.36 93.56 2.13 o 4 4 1 590.90 574.78 6.48 o 6 4 1 1299.20 1239.47 12.43 o 8 4 1 142.10 138.42 1.81 o 10 4 1 1602.14 1709.53 10.84 o 12 4 1 650.50 660.93 4.90 o 14 4 1 3.56 3.06 0.40 o 16 4 1 459.83 458.30 6.68 o 18 4 1 0.16 1.43 0.35 o -17 5 1 363.06 338.91 2.77 o -15 5 1 10.52 9.46 0.53 o -13 5 1 703.51 674.77 5.16 o -11 5 1 64.23 57.11 1.34 o -9 5 1 92.00 91.44 1.73 o -7 5 1 303.45 325.19 4.09 o -5 5 1 165.87 163.24 2.35 o -3 5 1 268.19 294.31 5.65 o 1 5 1 109.02 100.63 3.45 o 3 5 1 152.80 174.52 2.71 o 5 5 1 1424.96 1437.30 10.31 o 7 5 1 443.30 468.95 6.27 o 9 5 1 23.88 26.74 0.91 o 11 5 1 721.81 706.27 5.22 o 13 5 1 86.86 82.63 1.32 o 15 5 1 51.06 44.87 0.86 o -14 6 1 157.70 145.12 1.62 o -12 6 1 693.32 676.32 5.21 o -10 6 1 194.13 172.45 2.26 o -8 6 1 336.20 344.85 3.52 o -6 6 1 175.95 190.76 4.27 o -4 6 1 34.67 34.64 2.98 o 2 6 1 12.36 10.65 3.56 o 4 6 1 206.64 220.08 2.99 o 6 6 1 666.28 700.73 11.11 o 8 6 1 33.86 35.52 1.09 o 10 6 1 683.94 732.74 5.96 o 12 6 1 319.28 311.20 2.70 o -9 7 1 34.82 24.08 1.22 o 7 7 1 119.70 106.19 6.63 o -22 0 2 116.47 116.78 2.50 o -20 0 2 530.96 505.46 7.78 o -18 0 2 1479.43 1316.66 14.59 o -16 0 2 179.24 185.48 3.55 o -14 0 2 288.41 284.63 5.64 o -12 0 2 1143.35 1145.91 14.77 o -10 0 2 2281.83 2702.94 25.18 o -8 0 2 6699.96 6904.95 53.94 o -6 0 2 1147.62 1176.84 9.98 o -4 0 2 382.37 356.66 3.53 o -2 0 2 1969.39 1877.25 16.36 o 0 0 2 2210.00 2059.97 16.85 o 2 0 2 104.93 109.25 1.45 o 4 0 2 32.88 38.24 1.01 o 6 0 2 5.37 5.79 0.54 o 8 0 2 35.65 53.32 1.79 o 10 0 2 2693.53 2753.17 36.03 o 12 0 2 153.96 144.32 2.86 o 14 0 2 189.34 194.14 3.64 o 16 0 2 914.91 932.23 10.79 o 18 0 2 747.20 792.92 9.02 o 20 0 2 116.83 123.18 2.91 o -23 1 2 367.00 416.58 4.92 o -21 1 2 145.22 137.13 2.10 o -19 1 2 20.43 29.45 1.14 o -17 1 2 13.38 15.76 0.86 o -15 1 2 0.41 0.40 0.53 o -13 1 2 2564.56 2392.76 20.34 o -11 1 2 707.79 696.88 5.81 o -9 1 2 495.59 537.54 4.13 o -7 1 2 7631.61 8239.32 251.44 o -5 1 2 339.75 330.38 2.70 o -3 1 2 2229.53 2323.03 18.27 o -1 1 2 1718.37 1777.54 11.91 o 1 1 2 248.37 264.72 2.21 o 3 1 2 4974.00 4863.44 35.30 o 5 1 2 15.63 19.60 0.62 o 7 1 2 3494.69 3071.35 126.25 o 9 1 2 107.55 106.63 1.84 o 11 1 2 2855.72 2730.38 25.73 o 13 1 2 5767.05 6023.13 41.75 o 15 1 2 1009.99 1049.63 8.23 o 17 1 2 1076.38 1085.02 9.23 o 19 1 2 168.06 161.32 2.15 o -22 2 2 105.04 102.21 1.72 o -20 2 2 459.82 448.59 6.10 o -18 2 2 1274.24 1153.25 9.33 o -16 2 2 135.14 137.91 2.37 o -14 2 2 231.77 231.08 2.64 o -12 2 2 965.00 929.01 8.41 o -10 2 2 1455.26 1661.43 13.24 o -8 2 2 4135.60 4158.79 26.52 o -6 2 2 1074.46 1110.38 8.53 o -4 2 2 168.38 163.03 1.77 o -2 2 2 1356.46 1281.17 9.25 o 0 2 2 1058.75 1027.02 7.50 o 2 2 2 121.65 111.97 1.55 o 4 2 2 30.85 31.07 0.92 o 6 2 2 3.65 5.36 0.50 o 8 2 2 38.75 41.91 1.40 o 10 2 2 2239.42 2101.15 18.26 o 12 2 2 117.84 120.05 2.05 o 14 2 2 151.77 153.40 2.47 o 16 2 2 754.12 752.49 7.02 o 18 2 2 664.94 691.89 5.90 o -21 3 2 126.70 115.06 1.67 o -19 3 2 252.64 245.17 9.63 o -17 3 2 11.43 11.32 0.75 o -15 3 2 1.13 0.80 0.40 o -13 3 2 1675.05 1702.40 10.24 o -11 3 2 416.28 395.58 4.77 o -9 3 2 252.14 267.59 3.58 o -7 3 2 4193.21 4182.32 29.37 o -5 3 2 68.23 62.85 1.43 o -3 3 2 544.02 572.39 5.34 o -1 3 2 1256.51 1238.22 9.32 o 1 3 2 76.08 82.82 1.50 o 3 3 2 2051.44 1978.70 16.15 o 5 3 2 8.63 9.23 0.73 o 7 3 2 47.77 57.18 1.88 o 9 3 2 86.41 86.13 1.46 o 11 3 2 1934.21 1927.16 11.17 o 13 3 2 4206.85 4489.09 27.58 o 15 3 2 772.11 750.34 6.08 o 17 3 2 768.74 729.80 6.20 o -20 4 2 311.79 284.46 8.14 o -18 4 2 831.05 743.84 5.52 o -16 4 2 60.28 60.21 1.26 o -14 4 2 129.67 130.07 1.81 o -12 4 2 569.33 581.76 4.58 o -10 4 2 610.09 696.13 5.51 o -8 4 2 1697.49 1586.09 9.51 o -6 4 2 680.33 661.79 7.26 o -4 4 2 46.27 48.54 1.72 o -2 4 2 560.38 543.58 6.69 o 0 4 2 428.57 380.91 4.65 o 2 4 2 44.59 39.51 1.67 o 4 4 2 16.29 17.21 1.23 o 6 4 2 8.08 10.33 0.60 o 8 4 2 17.07 12.99 0.67 o 10 4 2 1311.78 1349.42 8.76 o 12 4 2 65.95 63.16 1.34 o 14 4 2 83.97 76.32 1.25 o 16 4 2 440.19 412.34 9.20 o -17 5 2 5.25 4.05 0.36 o -15 5 2 2.35 3.39 0.38 o -13 5 2 858.14 840.78 6.10 o -11 5 2 189.72 198.51 2.32 o -9 5 2 141.63 147.09 2.00 o -7 5 2 1734.95 1777.62 18.08 o -5 5 2 74.06 72.46 1.64 o -3 5 2 240.58 237.26 3.00 o -1 5 2 531.04 517.31 4.98 o 1 5 2 62.44 63.89 1.53 o 3 5 2 726.30 751.97 6.14 o 5 5 2 10.52 8.51 0.64 o 7 5 2 972.23 991.07 10.86 o 9 5 2 40.17 37.55 1.04 o 11 5 2 1164.09 1186.46 7.95 o 13 5 2 2349.74 2367.52 15.42 o 15 5 2 406.54 357.76 3.62 o -14 6 2 55.46 53.05 1.03 o -12 6 2 254.99 258.81 2.61 o -10 6 2 264.79 254.97 2.76 o -8 6 2 667.28 662.66 5.61 o -6 6 2 514.26 554.35 8.90 o -4 6 2 19.33 19.76 1.12 o -2 6 2 194.05 204.45 4.41 o 0 6 2 216.15 221.00 3.57 o 2 6 2 6.62 7.41 0.64 o 4 6 2 6.78 8.27 0.58 o 6 6 2 17.26 16.74 2.21 o 8 6 2 2.92 1.36 0.40 o 10 6 2 604.76 626.52 5.33 o -9 7 2 70.86 68.95 2.21 o 5 7 2 12.20 7.47 0.77 o -24 0 3 246.11 203.25 9.28 o -22 0 3 2.93 3.12 0.71 o -20 0 3 1051.39 1217.64 18.62 o -18 0 3 334.46 344.90 5.26 o -16 0 3 153.56 153.93 3.58 o -14 0 3 464.96 436.22 7.67 o -12 0 3 397.27 420.60 6.47 o -10 0 3 722.69 727.85 8.50 o -8 0 3 14.24 17.12 0.80 o -6 0 3 786.51 746.39 7.39 o -4 0 3 417.57 442.14 4.51 o -2 0 3 4878.62 4833.65 41.46 o 0 0 3 2338.85 2082.70 19.22 o 2 0 3 1606.34 1607.19 15.29 o 4 0 3 1390.18 1391.30 13.42 o 6 0 3 1373.73 1479.02 17.09 o 8 0 3 62.49 60.50 2.39 o 10 0 3 1320.73 1294.29 18.34 o 12 0 3 218.66 241.65 4.08 o 14 0 3 213.86 211.06 3.69 o 16 0 3 151.62 156.98 3.99 o 18 0 3 311.99 327.14 4.73 o -23 1 3 118.48 116.31 2.03 o -21 1 3 179.40 191.95 2.31 o -19 1 3 1025.29 992.46 8.11 o -17 1 3 444.23 462.89 4.48 o -15 1 3 144.00 134.74 2.01 o -13 1 3 1814.32 1692.45 14.84 o -11 1 3 24.04 26.09 0.89 o -9 1 3 109.96 128.46 1.56 o -7 1 3 733.76 776.87 5.90 o -5 1 3 7086.54 7345.24 46.01 o -3 1 3 5387.11 5218.82 32.79 o -1 1 3 3088.09 3111.37 19.95 o 1 1 3 1419.94 1354.84 9.50 o 3 1 3 13613.99 15090.92 99.81 o 5 1 3 2803.17 2861.24 19.97 o 7 1 3 1.19 2.84 0.47 o 9 1 3 67.71 70.09 2.10 o 11 1 3 1837.82 1827.95 13.92 o 13 1 3 1296.38 1348.38 11.06 o 15 1 3 7.26 7.82 0.63 o 17 1 3 89.15 87.47 1.51 o 19 1 3 59.47 59.54 1.21 o -22 2 3 2.81 3.57 0.48 o -20 2 3 900.29 1045.40 12.62 o -18 2 3 295.73 296.10 3.36 o -16 2 3 111.26 105.67 2.10 o -14 2 3 335.51 336.39 3.49 o -12 2 3 384.65 385.83 4.28 o -10 2 3 488.01 465.02 4.75 o -8 2 3 24.93 28.02 0.94 o -6 2 3 574.24 547.45 4.69 o -4 2 3 185.57 188.36 2.13 o -2 2 3 3174.43 3111.15 21.52 o 0 2 3 1639.24 1438.87 10.37 o 2 2 3 895.74 868.29 7.28 o 4 2 3 1299.36 1242.75 9.75 o 6 2 3 902.21 945.18 8.21 o 8 2 3 33.82 34.07 1.35 o 10 2 3 1092.92 1125.65 8.90 o 12 2 3 181.10 194.77 2.49 o 14 2 3 173.40 172.06 2.30 o 16 2 3 138.11 140.15 2.88 o 18 2 3 262.73 261.71 2.74 o -21 3 3 138.48 134.50 1.84 o -19 3 3 1158.35 1170.44 44.91 o -17 3 3 381.42 398.37 3.85 o -15 3 3 63.43 61.27 1.31 o -13 3 3 1139.50 1098.34 7.82 o -11 3 3 6.89 8.77 0.85 o -9 3 3 54.51 54.48 1.79 o -7 3 3 390.30 389.07 4.31 o -5 3 3 3079.62 3245.05 24.27 o -3 3 3 2185.97 2090.20 16.31 o -1 3 3 2130.08 2125.33 16.87 o 1 3 3 436.74 407.80 4.59 o 3 3 3 6255.61 6633.28 53.60 o 5 3 3 1953.94 1927.23 16.61 o 7 3 3 260.82 232.84 8.47 o 9 3 3 50.66 50.08 1.14 o 11 3 3 1318.46 1295.99 8.52 o 13 3 3 962.72 983.71 7.63 o 15 3 3 7.90 7.62 0.57 o 17 3 3 60.26 56.32 1.07 o -20 4 3 547.44 314.40 7.65 o -18 4 3 197.48 192.49 2.02 o -16 4 3 49.40 52.55 1.12 o -14 4 3 188.97 198.82 2.25 o -12 4 3 232.99 249.73 2.59 o -10 4 3 209.71 224.64 2.35 o -8 4 3 35.52 37.04 1.02 o -6 4 3 257.61 235.74 3.75 o -4 4 3 39.90 34.69 1.61 o -2 4 3 1385.67 1313.84 13.75 o 0 4 3 799.24 677.51 7.88 o 2 4 3 330.97 299.08 2.95 o 4 4 3 753.72 720.14 5.31 o 6 4 3 507.60 517.19 4.16 o 8 4 3 23.13 24.09 0.85 o 10 4 3 636.46 660.03 5.08 o 12 4 3 113.26 109.06 1.44 o 14 4 3 105.31 100.00 1.42 o -17 5 3 218.87 218.17 1.97 o -15 5 3 38.58 34.07 0.93 o -13 5 3 528.83 528.56 4.30 o -11 5 3 1.90 2.10 0.43 o -9 5 3 19.21 21.32 0.87 o -7 5 3 407.31 398.44 6.37 o -5 5 3 1155.27 1153.81 8.39 o -3 5 3 795.86 791.05 6.21 o -1 5 3 957.05 967.08 7.32 o 1 5 3 178.57 177.87 2.15 o 3 5 3 2713.51 2832.92 18.06 o 5 5 3 1047.66 1081.75 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4.00 o -17 1 9 479.27 481.86 4.52 o -15 1 9 1694.73 1623.75 13.12 o -13 1 9 140.31 165.85 2.25 o -11 1 9 204.65 197.23 2.32 o -9 1 9 218.17 213.47 2.67 o -7 1 9 55.13 59.61 1.40 o -5 1 9 32.57 34.12 1.15 o -3 1 9 204.74 304.88 5.51 o -1 1 9 73.85 79.27 1.58 o 1 1 9 1138.02 1219.97 9.70 o 3 1 9 657.83 679.59 5.87 o 5 1 9 31.62 39.92 1.29 o -16 2 9 545.91 553.43 4.93 o -14 2 9 741.35 737.14 6.51 o -12 2 9 29.61 31.33 0.99 o -10 2 9 357.38 370.72 3.79 o -8 2 9 3.34 3.10 0.44 o -6 2 9 13.28 12.53 0.70 o -4 2 9 470.09 482.71 4.33 o -2 2 9 30.99 30.99 1.02 o 0 2 9 195.08 192.62 2.31 o 2 2 9 746.31 710.19 6.01 o -15 3 9 1231.44 1175.37 10.83 o -13 3 9 101.46 117.22 1.59 o -11 3 9 152.79 157.14 2.01 o -9 3 9 159.41 162.53 2.03 o -7 3 9 40.56 44.63 1.14 o -5 3 9 26.24 27.37 0.90 o -3 3 9 141.50 180.23 4.14 o -1 3 9 56.95 58.20 1.08 o 1 3 9 862.71 886.37 8.20 o -10 4 9 101.82 138.01 2.27 o -8 4 9 1.52 1.74 0.34 o -6 4 9 9.84 8.04 0.50 o -4 4 9 307.28 298.56 3.19 o -14 0 10 3.88 8.69 0.83 o -12 0 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