#------------------------------------------------------------------------------ #$Date: 2023-12-05 15:40:41 +0200 (Tue, 05 Dec 2023) $ #$Revision: 288034 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/03/90/4039022.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4039022 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.0533 _cell_length_b 9.6682 _cell_length_c 7.3499 _exptl_crystal_F_000 292.00 _reflns_d_resolution_high 0.7701 _cod_data_source_file BTA_4HCl.fcf _cod_data_source_block jw23121 _shelx_title ' jw23121_a.res in Pnnm' _shelx_refln_list_code 4 _shelx_f_calc_maximum 62.17 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x, y, -z' 'x-1/2, -y-1/2, z-1/2' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 712.59 759.65 18.77 o 6 0 0 0.78 1.55 0.12 o 8 0 0 223.96 221.78 3.34 o 10 0 0 177.90 190.20 4.14 o 1 1 0 11.94 11.50 0.21 o 4 1 0 40.89 43.74 0.67 o 5 1 0 211.97 216.94 2.69 o 6 1 0 492.51 509.91 6.69 o 7 1 0 612.36 638.33 8.47 o 8 1 0 44.58 45.59 0.57 o 9 1 0 4.49 4.96 0.19 o 10 1 0 59.49 65.23 1.15 o 1 2 0 13.96 8.22 0.15 o 2 2 0 103.84 100.80 1.50 o 4 2 0 539.73 523.57 22.29 o 5 2 0 724.98 730.90 57.33 o 6 2 0 893.88 911.13 17.20 o 7 2 0 215.42 214.72 2.52 o 8 2 0 18.89 20.21 0.32 o 9 2 0 447.08 461.08 5.95 o 10 2 0 139.31 139.42 2.32 o 2 3 0 382.53 440.23 23.02 o 3 3 0 1083.24 1097.17 23.78 o 4 3 0 854.62 885.31 38.03 o 5 3 0 74.81 85.05 1.00 o 6 3 0 24.58 25.58 0.42 o 7 3 0 13.24 15.05 0.27 o 8 3 0 829.03 838.77 9.99 o 9 3 0 256.39 251.43 3.12 o 10 3 0 82.28 87.79 1.39 o 3 4 0 1474.54 1476.31 50.90 o 4 4 0 48.77 53.97 0.63 o 5 4 0 7.77 8.84 0.17 o 6 4 0 52.96 52.23 0.61 o 7 4 0 1063.37 1093.63 17.85 o 8 4 0 163.40 165.35 1.79 o 9 4 0 2.87 3.02 0.16 o 1 5 0 0.95 1.12 0.08 o 2 5 0 36.32 52.46 1.08 o 3 5 0 251.87 235.16 2.52 o 4 5 0 13.59 12.63 0.20 o 6 5 0 91.43 88.54 1.04 o 7 5 0 6.99 7.28 0.19 o 8 5 0 2.19 1.92 0.12 o 9 5 0 121.61 122.55 1.80 o 0 6 0 114.75 133.59 3.01 o 1 6 0 18.25 19.06 0.42 o 3 6 0 103.12 90.58 1.14 o 4 6 0 3.11 3.21 0.11 o 5 6 0 917.01 923.06 12.56 o 6 6 0 56.12 53.49 0.72 o 7 6 0 1075.09 1082.28 15.53 o 8 6 0 44.57 46.44 0.80 o 9 6 0 43.58 38.25 0.70 o 1 7 0 180.51 182.16 2.80 o 2 7 0 106.51 114.21 1.36 o 3 7 0 222.67 220.81 2.46 o 4 7 0 543.83 519.15 7.15 o 5 7 0 84.13 87.72 1.18 o 6 7 0 205.99 202.52 2.45 o 7 7 0 44.34 42.47 0.83 o 8 7 0 444.08 431.25 9.13 o 0 8 0 5.11 4.08 0.24 o 1 8 0 228.19 215.58 3.01 o 2 8 0 358.60 343.54 4.50 o 3 8 0 320.43 316.92 3.73 o 4 8 0 1065.38 1021.58 19.86 o 5 8 0 282.00 274.41 3.40 o 6 8 0 469.72 468.63 5.84 o 7 8 0 18.28 19.08 0.36 o 8 8 0 135.58 139.25 3.49 o 1 9 0 249.01 249.68 3.25 o 2 9 0 372.16 376.89 4.81 o 3 9 0 1486.89 1495.95 49.31 o 4 9 0 151.76 157.62 2.59 o 5 9 0 53.29 58.18 1.03 o 6 9 0 113.44 117.31 2.07 o 7 9 0 4.90 5.38 0.18 o 0 10 0 1527.33 1472.07 67.73 o 1 10 0 47.74 48.74 0.79 o 2 10 0 35.38 37.88 0.55 o 3 10 0 0.30 0.52 0.10 o 4 10 0 8.37 7.22 0.27 o 5 10 0 137.98 137.84 2.52 o 6 10 0 40.82 40.12 0.73 o 1 11 0 84.32 84.88 1.24 o 2 11 0 418.25 420.48 6.06 o 3 11 0 246.90 240.60 4.00 o 4 11 0 4.83 7.39 0.28 o 5 11 0 121.00 116.05 2.07 o 0 12 0 472.72 473.43 8.95 o 1 12 0 283.62 282.36 4.01 o 2 12 0 77.17 78.36 1.43 o 3 12 0 340.19 334.99 6.36 o 1 0 1 9.17 7.58 0.19 o 7 0 1 484.02 503.27 6.33 o 9 0 1 626.22 655.87 10.14 o 1 1 1 367.61 410.38 12.16 o 2 1 1 550.96 585.93 24.64 o 4 1 1 135.88 159.02 1.57 o 5 1 1 195.50 202.25 1.72 o 6 1 1 419.17 427.05 3.45 o 7 1 1 1023.72 1113.03 21.59 o 8 1 1 491.83 497.85 3.89 o 9 1 1 76.78 77.38 0.74 o 10 1 1 4.54 4.22 0.11 o 2 2 1 3.15 7.91 0.12 o 3 2 1 710.72 811.55 11.67 o 4 2 1 2177.16 2322.91 58.28 o 5 2 1 579.00 622.15 8.99 o 6 2 1 756.65 785.20 11.31 o 7 2 1 16.27 15.92 0.19 o 8 2 1 241.60 246.52 1.87 o 9 2 1 153.85 152.57 1.38 o 10 2 1 112.70 118.79 1.32 o 0 3 1 39.78 39.41 0.66 o 2 3 1 302.10 308.29 4.26 o 3 3 1 294.65 331.23 3.75 o 4 3 1 186.71 169.47 1.41 o 5 3 1 473.66 489.39 4.83 o 6 3 1 1107.21 1127.77 21.31 o 7 3 1 1.33 1.65 0.06 o 8 3 1 65.23 64.72 0.55 o 9 3 1 14.04 15.15 0.22 o 10 3 1 158.82 159.11 1.62 o 1 4 1 283.86 278.27 4.57 o 2 4 1 870.98 722.90 31.26 o 3 4 1 990.53 992.97 43.23 o 4 4 1 118.53 124.29 0.92 o 5 4 1 56.60 55.89 0.45 o 6 4 1 7.26 8.71 0.12 o 7 4 1 1.43 1.73 0.07 o 8 4 1 392.41 397.24 3.02 o 9 4 1 96.40 99.82 1.04 o 1 5 1 0.35 1.05 0.06 o 2 5 1 0.61 2.42 0.08 o 3 5 1 199.10 210.06 1.56 o 4 5 1 961.87 976.65 17.71 o 5 5 1 17.34 18.66 0.21 o 6 5 1 6.11 5.85 0.13 o 7 5 1 118.27 121.02 1.09 o 8 5 1 22.70 23.69 0.27 o 9 5 1 48.05 47.53 0.53 o 1 6 1 394.67 405.33 5.09 o 2 6 1 3864.88 4113.44 171.98 o 3 6 1 581.04 567.41 5.93 o 4 6 1 136.08 130.30 1.06 o 5 6 1 69.16 68.11 0.58 o 6 6 1 139.07 138.50 1.14 o 7 6 1 4.05 3.66 0.11 o 8 6 1 52.36 47.71 0.60 o 9 6 1 0.08 0.41 0.07 o 0 7 1 1005.91 1126.42 49.66 o 1 7 1 1383.75 1342.53 50.34 o 2 7 1 0.07 0.48 0.04 o 3 7 1 23.83 22.15 0.22 o 4 7 1 578.46 555.60 5.12 o 5 7 1 41.67 41.45 0.57 o 6 7 1 54.48 49.69 0.51 o 7 7 1 2.33 2.04 0.13 o 8 7 1 17.87 17.36 0.29 o 1 8 1 521.04 498.74 5.65 o 2 8 1 47.40 49.35 0.51 o 3 8 1 220.92 210.13 1.86 o 4 8 1 398.88 383.48 3.62 o 5 8 1 13.88 14.34 0.22 o 6 8 1 43.08 44.04 0.49 o 7 8 1 31.14 27.73 0.38 o 0 9 1 649.39 640.23 8.83 o 1 9 1 197.70 191.98 1.94 o 2 9 1 197.00 194.03 1.70 o 3 9 1 415.94 407.68 3.64 o 4 9 1 259.68 254.06 2.63 o 5 9 1 4.55 5.94 0.17 o 6 9 1 317.70 318.77 3.27 o 7 9 1 184.88 174.65 2.93 o 1 10 1 150.93 148.10 1.45 o 2 10 1 332.23 332.02 2.88 o 3 10 1 0.74 0.94 0.06 o 4 10 1 107.24 108.97 1.26 o 5 10 1 715.82 729.81 11.49 o 6 10 1 1.01 1.25 0.08 o 0 11 1 11.46 13.89 0.36 o 1 11 1 52.79 54.60 0.63 o 2 11 1 27.05 26.93 0.39 o 3 11 1 397.16 396.30 4.40 o 4 11 1 0.52 0.41 0.06 o 1 12 1 4.32 4.83 0.11 o 2 12 1 29.27 25.94 0.39 o 2 0 2 119.32 108.49 1.46 o 6 0 2 44.49 46.50 0.71 o 8 0 2 103.52 105.39 1.38 o 10 0 2 192.37 188.70 2.89 o 3 1 2 73.27 60.13 0.60 o 4 1 2 64.45 58.75 0.55 o 5 1 2 22.17 23.79 0.25 o 6 1 2 49.03 55.85 0.53 o 7 1 2 43.58 42.04 0.44 o 8 1 2 294.87 297.17 2.50 o 9 1 2 31.47 32.29 0.42 o 10 1 2 0.26 0.45 0.05 o 2 2 2 433.13 446.00 10.97 o 3 2 2 109.25 116.82 1.02 o 4 2 2 34.92 27.92 0.26 o 5 2 2 6.51 4.93 0.11 o 6 2 2 312.90 321.68 2.55 o 7 2 2 6.74 7.57 0.14 o 8 2 2 79.31 78.69 0.70 o 9 2 2 102.63 108.72 1.13 o 10 2 2 221.06 226.56 2.47 o 1 3 2 1048.07 1181.26 26.67 o 2 3 2 480.27 455.88 12.30 o 3 3 2 1390.98 1475.63 25.95 o 5 3 2 595.71 613.21 5.95 o 6 3 2 355.74 347.41 2.66 o 7 3 2 8.29 7.88 0.13 o 8 3 2 124.64 124.78 0.99 o 9 3 2 5.07 3.96 0.10 o 0 4 2 217.73 211.05 3.98 o 1 4 2 69.63 72.11 0.93 o 2 4 2 16.74 23.27 0.25 o 4 4 2 68.80 70.99 0.56 o 5 4 2 13.00 17.02 0.17 o 6 4 2 1160.66 1211.67 18.17 o 7 4 2 632.47 632.96 5.37 o 8 4 2 176.26 174.40 1.45 o 9 4 2 21.99 19.48 0.28 o 1 5 2 562.79 567.10 18.88 o 2 5 2 58.33 47.26 0.41 o 3 5 2 277.44 269.49 2.05 o 4 5 2 46.10 42.56 0.38 o 5 5 2 869.91 861.67 8.47 o 6 5 2 21.24 22.29 0.24 o 7 5 2 97.75 97.67 0.94 o 8 5 2 3.32 4.04 0.11 o 9 5 2 854.34 847.43 19.91 o 0 6 2 3.86 4.97 0.19 o 1 6 2 572.03 579.84 13.13 o 2 6 2 1.19 2.56 0.07 o 3 6 2 1199.59 1158.81 18.99 o 4 6 2 12.06 11.01 0.17 o 5 6 2 80.53 82.44 0.71 o 6 6 2 516.81 504.62 4.15 o 7 6 2 564.88 566.11 5.81 o 8 6 2 37.65 36.05 0.50 o 1 7 2 26.64 25.46 0.27 o 2 7 2 6.96 6.57 0.10 o 3 7 2 3.69 4.08 0.12 o 4 7 2 1174.43 1149.00 17.60 o 5 7 2 409.28 400.01 3.32 o 6 7 2 513.74 502.22 4.53 o 7 7 2 92.45 96.08 1.38 o 8 7 2 88.41 84.41 1.15 o 0 8 2 304.49 314.63 3.77 o 1 8 2 828.84 847.39 12.38 o 2 8 2 224.49 219.66 1.87 o 3 8 2 0.54 0.59 0.04 o 4 8 2 33.93 35.15 0.37 o 5 8 2 9.14 9.09 0.15 o 6 8 2 543.46 551.58 6.14 o 7 8 2 4.44 3.44 0.12 o 1 9 2 300.75 299.14 2.71 o 2 9 2 361.50 369.37 3.12 o 3 9 2 274.78 268.99 2.35 o 4 9 2 114.98 113.56 1.08 o 5 9 2 52.41 54.37 0.64 o 6 9 2 73.82 79.54 0.93 o 0 10 2 382.86 381.67 4.83 o 1 10 2 205.68 201.39 1.79 o 2 10 2 0.57 0.84 0.09 o 3 10 2 75.50 77.54 0.84 o 4 10 2 483.08 482.30 4.97 o 5 10 2 18.55 19.93 0.30 o 1 11 2 157.44 154.34 1.64 o 2 11 2 696.81 690.31 8.20 o 3 11 2 11.85 11.76 0.20 o 4 11 2 86.16 91.40 1.36 o 0 12 2 396.08 387.46 6.19 o 1 12 2 724.86 693.56 11.88 o 2 12 2 4.53 3.65 0.12 o 1 0 3 638.82 718.18 38.21 o 5 0 3 2570.84 2501.91 104.58 o 7 0 3 20.74 15.45 0.37 o 9 0 3 479.78 511.26 11.84 o 1 1 3 265.10 270.43 3.87 o 2 1 3 835.22 805.06 33.68 o 3 1 3 811.57 756.09 16.61 o 4 1 3 232.72 244.34 1.85 o 5 1 3 228.99 236.29 1.80 o 6 1 3 463.80 454.60 4.25 o 7 1 3 1259.80 1243.47 26.80 o 8 1 3 7.63 9.63 0.17 o 9 1 3 8.59 9.48 0.17 o 1 2 3 306.86 285.11 3.20 o 2 2 3 6.18 5.33 0.12 o 3 2 3 387.17 380.92 3.79 o 4 2 3 1019.10 999.19 17.26 o 5 2 3 504.26 514.56 4.66 o 6 2 3 85.15 93.48 0.82 o 7 2 3 134.62 126.40 1.23 o 8 2 3 624.81 614.66 7.05 o 9 2 3 47.69 46.79 0.59 o 0 3 3 148.62 168.89 2.48 o 1 3 3 451.90 412.07 5.05 o 2 3 3 1310.05 1370.48 46.12 o 3 3 3 516.57 545.76 7.07 o 4 3 3 287.52 283.13 1.90 o 5 3 3 402.59 416.73 3.25 o 6 3 3 326.18 345.67 2.73 o 7 3 3 77.47 70.94 0.65 o 8 3 3 201.28 205.10 1.84 o 9 3 3 175.13 172.40 2.01 o 1 4 3 1060.19 962.54 42.86 o 3 4 3 925.59 849.53 18.64 o 4 4 3 76.94 77.92 0.61 o 5 4 3 425.55 406.84 3.49 o 6 4 3 258.06 234.65 2.04 o 7 4 3 1.04 1.31 0.07 o 8 4 3 128.10 135.34 1.51 o 9 4 3 5.90 5.78 0.15 o 1 5 3 24.65 24.12 0.23 o 2 5 3 778.29 803.63 11.83 o 3 5 3 0.10 0.25 0.03 o 4 5 3 576.01 571.12 4.33 o 5 5 3 69.03 60.95 0.54 o 6 5 3 128.31 122.06 1.08 o 7 5 3 67.43 69.98 0.73 o 8 5 3 11.97 14.79 0.25 o 9 5 3 0.23 0.61 0.09 o 1 6 3 474.61 499.88 5.15 o 3 6 3 142.68 136.60 1.05 o 4 6 3 3.27 4.11 0.08 o 5 6 3 28.15 22.79 0.26 o 6 6 3 72.42 75.99 0.73 o 7 6 3 2.34 2.35 0.14 o 8 6 3 17.99 15.95 0.29 o 0 7 3 820.47 835.87 18.19 o 1 7 3 558.89 553.33 5.43 o 2 7 3 45.71 51.19 0.46 o 3 7 3 495.71 513.16 4.04 o 4 7 3 63.76 68.28 0.71 o 5 7 3 433.99 424.64 3.80 o 6 7 3 17.68 16.85 0.33 o 7 7 3 22.75 21.71 0.39 o 8 7 3 13.93 15.30 0.28 o 1 8 3 535.97 537.67 4.43 o 2 8 3 0.10 0.33 0.04 o 3 8 3 991.70 1003.38 11.51 o 4 8 3 181.64 181.11 1.69 o 5 8 3 79.71 75.51 0.73 o 6 8 3 17.93 19.13 0.28 o 7 8 3 46.96 45.65 0.72 o 0 9 3 947.06 961.54 15.77 o 1 9 3 190.03 194.27 1.64 o 2 9 3 285.99 282.70 2.49 o 3 9 3 278.76 270.77 2.32 o 4 9 3 63.54 59.94 0.88 o 5 9 3 0.11 0.41 0.07 o 6 9 3 153.11 155.44 2.17 o 1 10 3 93.54 91.86 0.95 o 2 10 3 165.71 166.20 1.70 o 3 10 3 207.54 205.72 2.54 o 4 10 3 47.27 47.72 0.61 o 5 10 3 445.01 444.78 6.63 o 0 11 3 5.69 6.07 0.34 o 1 11 3 5.35 6.57 0.18 o 2 11 3 5.08 5.45 0.13 o 3 11 3 74.53 74.92 1.08 o 2 0 4 442.96 424.35 6.53 o 4 0 4 165.90 166.64 1.76 o 6 0 4 60.74 62.03 1.21 o 8 0 4 58.58 55.05 1.00 o 1 1 4 979.11 1017.94 42.75 o 4 1 4 3.20 4.15 0.08 o 5 1 4 11.86 11.26 0.15 o 6 1 4 91.36 95.58 0.90 o 7 1 4 5.14 3.49 0.11 o 8 1 4 110.43 108.80 1.25 o 9 1 4 2.52 2.10 0.09 o 0 2 4 885.65 947.00 39.65 o 2 2 4 138.73 152.23 1.04 o 3 2 4 737.57 733.73 11.00 o 4 2 4 654.94 619.16 6.97 o 5 2 4 727.26 687.82 8.05 o 6 2 4 228.49 232.94 2.03 o 7 2 4 19.25 22.14 0.39 o 8 2 4 111.01 105.36 1.22 o 9 2 4 69.79 74.47 0.89 o 1 3 4 674.46 595.59 9.29 o 2 3 4 35.02 37.93 0.29 o 3 3 4 319.22 318.59 2.22 o 4 3 4 585.93 556.06 5.41 o 5 3 4 97.48 92.29 0.87 o 6 3 4 225.32 200.73 1.77 o 7 3 4 61.59 58.08 0.60 o 8 3 4 236.09 236.13 2.85 o 9 3 4 49.88 49.58 0.69 o 0 4 4 1007.92 833.90 36.97 o 1 4 4 18.35 14.20 0.15 o 2 4 4 675.31 609.44 6.40 o 3 4 4 406.04 395.18 2.96 o 4 4 4 3.66 3.52 0.07 o 5 4 4 135.42 122.42 1.04 o 6 4 4 270.14 254.88 2.31 o 7 4 4 447.06 440.14 4.30 o 8 4 4 55.76 56.05 0.75 o 1 5 4 82.70 93.44 0.78 o 2 5 4 471.03 480.18 4.07 o 3 5 4 312.72 318.77 2.34 o 4 5 4 73.27 72.01 0.59 o 5 5 4 1471.67 1500.39 21.65 o 6 5 4 48.26 43.20 0.49 o 7 5 4 16.15 15.43 0.28 o 8 5 4 14.68 16.80 0.31 o 0 6 4 0.10 0.54 0.10 o 1 6 4 6.90 7.73 0.12 o 2 6 4 171.44 159.88 1.37 o 3 6 4 584.18 590.99 5.08 o 4 6 4 126.98 122.50 1.09 o 5 6 4 77.00 81.70 0.78 o 6 6 4 111.42 103.70 1.09 o 7 6 4 894.13 863.61 18.20 o 8 6 4 72.28 74.78 1.19 o 1 7 4 243.07 254.32 2.29 o 2 7 4 45.41 48.38 0.50 o 3 7 4 26.93 30.94 0.33 o 4 7 4 644.41 630.44 6.43 o 5 7 4 319.13 304.33 2.76 o 6 7 4 43.19 46.64 0.69 o 7 7 4 0.10 0.28 0.06 o 0 8 4 59.21 59.09 0.89 o 1 8 4 139.82 147.85 1.39 o 2 8 4 346.15 355.56 3.30 o 3 8 4 47.60 44.90 0.45 o 4 8 4 41.62 44.72 0.50 o 5 8 4 37.27 38.30 0.48 o 6 8 4 452.24 457.95 7.30 o 1 9 4 41.50 42.51 0.47 o 2 9 4 284.71 288.10 2.67 o 3 9 4 197.20 193.65 2.06 o 4 9 4 107.39 111.86 1.32 o 5 9 4 184.63 183.91 2.29 o 0 10 4 1560.23 1470.30 106.71 o 1 10 4 31.56 29.87 0.41 o 2 10 4 43.65 44.77 0.58 o 3 10 4 20.74 21.26 0.37 o 4 10 4 297.51 296.04 3.98 o 1 11 4 18.50 20.05 0.31 o 2 11 4 684.71 695.86 16.38 o 1 0 5 289.13 292.39 2.73 o 3 0 5 22.92 24.14 0.30 o 5 0 5 1770.50 1500.92 77.50 o 7 0 5 102.35 103.88 1.84 o 0 1 5 61.33 60.59 0.65 o 1 1 5 56.49 55.55 0.41 o 2 1 5 134.46 119.41 0.81 o 3 1 5 1593.44 1503.07 56.90 o 4 1 5 560.89 551.89 4.75 o 5 1 5 1.25 1.50 0.07 o 6 1 5 548.61 507.20 4.97 o 7 1 5 584.46 548.01 6.01 o 8 1 5 103.79 108.22 1.23 o 1 2 5 398.49 386.57 3.09 o 2 2 5 303.66 299.82 2.06 o 3 2 5 10.38 10.26 0.13 o 4 2 5 1544.80 1499.24 70.30 o 5 2 5 70.81 65.40 0.58 o 6 2 5 252.45 246.09 2.19 o 7 2 5 24.81 24.45 0.33 o 8 2 5 126.04 130.27 1.52 o 0 3 5 359.34 376.16 4.60 o 1 3 5 1371.32 1388.42 41.06 o 2 3 5 4.06 4.01 0.08 o 3 3 5 75.97 73.19 0.59 o 4 3 5 370.89 368.92 2.82 o 5 3 5 23.59 24.03 0.33 o 6 3 5 761.97 719.01 8.02 o 7 3 5 0.03 0.36 0.07 o 8 3 5 140.77 136.63 1.78 o 1 4 5 116.43 119.39 0.93 o 3 4 5 682.57 666.20 7.07 o 4 4 5 2.99 4.03 0.09 o 5 4 5 10.63 13.47 0.19 o 6 4 5 241.38 237.04 2.14 o 7 4 5 18.57 18.10 0.34 o 8 4 5 137.69 132.29 1.71 o 1 5 5 367.38 382.42 2.90 o 2 5 5 133.97 139.91 1.16 o 3 5 5 0.97 1.26 0.06 o 4 5 5 920.72 912.32 15.17 o 5 5 5 101.96 99.61 1.00 o 6 5 5 97.15 95.22 1.11 o 7 5 5 6.51 8.54 0.20 o 1 6 5 17.82 18.42 0.22 o 2 6 5 844.37 863.34 10.46 o 3 6 5 129.71 132.21 1.20 o 4 6 5 64.11 62.62 0.59 o 5 6 5 60.69 62.55 0.67 o 6 6 5 46.71 44.16 0.60 o 7 6 5 14.27 16.37 0.32 o 0 7 5 51.54 50.80 0.79 o 1 7 5 2082.85 2333.01 97.72 o 2 7 5 0.67 0.86 0.06 o 3 7 5 13.21 14.36 0.21 o 4 7 5 100.92 104.09 1.14 o 5 7 5 77.11 79.50 0.99 o 6 7 5 126.84 122.10 1.69 o 1 8 5 927.12 947.10 11.57 o 2 8 5 0.16 0.55 0.06 o 3 8 5 402.73 406.66 3.98 o 4 8 5 285.01 290.88 3.44 o 5 8 5 87.80 81.03 1.07 o 0 9 5 28.12 28.33 0.52 o 1 9 5 83.22 86.59 0.98 o 2 9 5 27.17 28.49 0.38 o 3 9 5 268.00 267.20 3.05 o 4 9 5 39.55 40.46 0.61 o 1 10 5 0.96 1.53 0.08 o 2 10 5 119.98 122.82 1.69 o 3 10 5 37.75 36.18 0.62 o 2 0 6 5.50 5.55 0.12 o 4 0 6 133.48 129.86 1.49 o 6 0 6 0.57 0.76 0.09 o 8 0 6 41.76 47.21 0.83 o 1 1 6 362.19 340.34 2.38 o 2 1 6 1041.73 1058.21 20.29 o 3 1 6 1108.51 1085.10 17.14 o 4 1 6 0.86 1.46 0.06 o 5 1 6 13.43 14.88 0.21 o 6 1 6 32.95 30.59 0.41 o 7 1 6 7.35 8.69 0.23 o 8 1 6 104.73 103.38 1.43 o 0 2 6 403.74 379.70 4.11 o 2 2 6 12.45 12.23 0.15 o 3 2 6 217.72 222.97 1.64 o 4 2 6 629.36 614.18 8.14 o 5 2 6 332.36 311.02 2.49 o 6 2 6 216.79 205.72 2.26 o 7 2 6 1.61 1.39 0.09 o 1 3 6 594.79 620.45 14.54 o 2 3 6 27.41 26.87 0.28 o 3 3 6 110.58 108.65 0.95 o 4 3 6 433.81 423.12 3.65 o 5 3 6 23.02 22.12 0.26 o 6 3 6 256.55 255.42 3.56 o 7 3 6 15.43 16.40 0.30 o 0 4 6 306.53 315.72 3.66 o 1 4 6 0.26 0.70 0.06 o 2 4 6 410.63 438.82 3.61 o 3 4 6 254.99 253.59 2.19 o 4 4 6 37.56 38.77 0.46 o 5 4 6 116.76 115.13 1.16 o 6 4 6 173.56 183.29 2.65 o 7 4 6 281.85 280.73 3.36 o 1 5 6 13.07 13.11 0.20 o 2 5 6 314.00 313.22 2.84 o 3 5 6 97.38 94.27 0.92 o 4 5 6 47.39 46.93 0.53 o 5 5 6 1048.99 944.00 25.57 o 6 5 6 49.53 50.76 0.72 o 0 6 6 38.41 39.24 0.72 o 1 6 6 4.19 5.49 0.13 o 2 6 6 150.77 158.73 1.61 o 3 6 6 515.77 515.11 6.07 o 4 6 6 37.62 37.42 0.61 o 5 6 6 14.10 12.86 0.26 o 6 6 6 42.66 41.40 0.77 o 1 7 6 267.02 282.74 2.95 o 2 7 6 50.06 50.34 0.62 o 3 7 6 3.26 2.98 0.14 o 4 7 6 496.57 505.28 7.55 o 5 7 6 161.88 169.02 2.32 o 0 8 6 104.32 110.16 1.95 o 1 8 6 123.52 132.02 1.72 o 2 8 6 135.23 140.00 1.70 o 3 8 6 15.03 16.00 0.28 o 4 8 6 27.02 26.83 0.44 o 1 9 6 1.83 2.75 0.11 o 2 9 6 205.56 214.45 2.77 o 3 9 6 142.58 147.17 2.11 o 1 0 7 180.81 161.60 1.91 o 3 0 7 190.67 195.14 2.45 o 5 0 7 1320.45 1259.22 64.98 o 7 0 7 29.57 33.03 0.97 o 0 1 7 649.66 585.53 11.59 o 1 1 7 60.07 60.06 0.57 o 2 1 7 352.69 356.86 2.91 o 3 1 7 276.93 274.69 2.45 o 4 1 7 31.55 32.12 0.37 o 5 1 7 97.76 95.70 1.22 o 6 1 7 164.28 164.23 2.29 o 7 1 7 607.92 566.46 23.91 o 1 2 7 129.76 147.73 1.37 o 2 2 7 24.99 23.04 0.27 o 3 2 7 58.87 60.39 0.60 o 4 2 7 429.85 417.79 3.73 o 5 2 7 137.49 135.09 1.68 o 6 2 7 11.86 9.78 0.23 o 0 3 7 60.91 58.28 0.89 o 1 3 7 120.76 137.95 1.39 o 2 3 7 316.22 319.96 2.92 o 3 3 7 173.31 178.89 1.66 o 4 3 7 235.27 231.98 2.20 o 5 3 7 142.47 135.13 1.51 o 6 3 7 153.96 143.62 1.86 o 1 4 7 261.00 265.13 2.32 o 2 4 7 802.67 805.85 14.27 o 3 4 7 424.49 433.38 4.08 o 4 4 7 28.00 29.06 0.40 o 5 4 7 150.37 155.13 1.84 o 6 4 7 179.41 183.14 2.32 o 0 5 7 2224.64 2293.42 96.24 o 1 5 7 40.07 37.84 0.45 o 2 5 7 247.62 250.25 2.39 o 3 5 7 3.23 3.41 0.10 o 4 5 7 179.22 182.22 1.98 o 5 5 7 74.98 77.28 0.98 o 1 6 7 131.10 139.02 1.64 o 2 6 7 502.37 528.64 6.82 o 3 6 7 81.16 85.36 1.00 o 4 6 7 0.14 0.34 0.06 o 5 6 7 8.27 9.74 0.20 o 0 7 7 201.01 217.43 3.56 o 1 7 7 261.82 283.95 3.46 o 2 7 7 10.91 10.43 0.21 o 3 7 7 289.32 284.64 3.65 o 4 7 7 22.64 21.28 0.38 o 1 8 7 345.31 354.87 4.54 o 2 8 7 2.77 2.58 0.11 o 0 0 8 852.25 950.59 47.97 o 2 0 8 18.00 16.25 0.31 o 4 0 8 829.87 808.33 18.27 o 1 1 8 265.80 258.44 2.54 o 2 1 8 805.21 795.28 13.00 o 3 1 8 76.27 71.32 0.86 o 4 1 8 4.42 5.00 0.15 o 5 1 8 17.47 15.51 0.36 o 0 2 8 345.96 346.36 4.88 o 1 2 8 918.05 902.11 25.22 o 2 2 8 94.36 95.53 1.08 o 3 2 8 5.55 5.76 0.14 o 4 2 8 23.38 22.03 0.33 o 5 2 8 30.71 29.01 0.64 o 1 3 8 153.37 169.94 1.81 o 2 3 8 20.18 25.37 0.35 o 3 3 8 290.24 294.23 2.95 o 4 3 8 398.27 394.10 5.24 o 5 3 8 189.13 177.44 3.09 o 0 4 8 155.13 157.82 2.60 o 1 4 8 8.14 10.78 0.21 o 2 4 8 2.42 3.19 0.11 o 3 4 8 366.47 371.19 4.77 o 4 4 8 2.01 2.19 0.09 o 1 5 8 136.81 138.83 1.57 o 2 5 8 47.72 43.00 0.58 o 3 5 8 122.47 117.99 1.41 o 0 6 8 2.14 3.16 0.16 o 1 6 8 75.06 79.98 1.01 o 2 6 8 0.85 0.70 0.07 o 1 0 9 28.84 25.71 0.55 o 3 0 9 161.85 174.29 4.00 o 0 1 9 0.57 0.40 0.09 o 1 1 9 17.09 19.26 0.31 o 2 1 9 12.00 11.43 0.25 o 3 1 9 314.24 313.35 4.91 o 1 2 9 155.65 170.29 2.24 o 2 2 9 0.86 0.63 0.07 o 3 2 9 100.50 109.47 1.60 o 0 3 9 47.91 46.15 0.82 o 1 3 9 587.04 604.23 23.98 o 2 3 9 67.45 69.94 0.97 o 1 4 9 90.20 91.40 1.27 o