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Information card for entry 4060714
Preview
| Coordinates | 4060714.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C15 H26 Ge N4 |
|---|---|
| Calculated formula | C15 H26 Ge N4 |
| SMILES | [Ge]123([N](CCN1C)(CCN2C)CCN3C)c1ccccc1 |
| Title of publication | Azametallatranes of Group 14 Elements. Syntheses and X-ray Studies |
| Authors of publication | Shutov, Pavel L.; Sorokin, Denis A.; Karlov, Sergey S.; Harms, Klaus; Oprunenko, Yuri F.; Churakov, Andrei V.; Antipin, Mikhail Yu.; Zaitseva, Galina S.; Lorberth, Jörg |
| Journal of publication | Organometallics |
| Year of publication | 2003 |
| Journal volume | 22 |
| Journal issue | 3 |
| Pages of publication | 516 - 522 |
| a | 8.3466 ± 0.0006 Å |
| b | 11.2962 ± 0.0008 Å |
| c | 16.3629 ± 0.0011 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 1542.8 ± 0.2 Å3 |
| Cell temperature | 110 ± 2 K |
| Ambient diffraction temperature | 110 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.04 |
| Residual factor for significantly intense reflections | 0.0383 |
| Weighted residual factors for all reflections | 0.0956 |
| Weighted residual factors for significantly intense reflections | 0.0945 |
| Goodness-of-fit parameter for all reflections | 1.033 |
| Goodness-of-fit parameter for significantly intense reflections | 1.049 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181334 (current) | 2016-04-04 | cif/4/06/ (antanas@kurmis) Adding full bibliography and additional information from the original publication to entries 4060711, 4060712, 4060713, 4060714. |
4060714.cif |
| 130149 | 2015-01-27 | cod/ (saulius@kolibris) Deriving Hall space group symbols for 12003 CIFs using the 'cif_filter --estimate-spacegroup' command. |
4060714.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4060714.cif |
| 966 | 2010-01-30 | cif/ Adding _cod_database_code tags to all COD entries. Adding tag description to the cif_cod.dic dictionary so that COD entries can be validated. |
4060714.cif |
| 19 | 2008-01-26 | Changing all end-of-line codes from DOS style to UNIX style in all COD CIF files, for more convenient processing: In the cod/cif/ directory: ff \*.cif | xargs perl -i -pe 's/\r\n/\n/' |
4060714.cif |
| 14 | 2008-01-14 | Appending a header with SVN keywords, COD URL and copying policy to all COD CIF files. |
4060714.cif |
| 13 | 2008-01-13 | Setting the svn:keywords property to "Author Date Revision URL Id" for all CIF files in the cod/cif directory. |
4060714.cif |
| 1 | 2007-11-30 | Adding all .cif files from the COD, downloaded in a Cod.zip file on 2007.02.07 (and the same Cod.zip is downloadable today, on 2007.11.29) |
4060714.cif |
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Users of the data should acknowledge the original authors of the
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