Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4063405
Preview
| Coordinates | 4063405.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C44 H73 Mo N3 O2 Pd Sn2 |
|---|---|
| Calculated formula | C44 H73 Mo N3 O2 Pd Sn2 |
| Title of publication | Insertion vs Ligand Exchange: Reactivity of DistannaAnsaHalf-Sandwich Complexes of Molybdenum and Tungsten toward Isocyanide and Phosphine Complexes of Nickel and Palladium |
| Authors of publication | Braunschweig, Holger; Dörfler, Rainer; Gruss, Katrin; Köhler, Julia; Radacki, Krzysztof |
| Journal of publication | Organometallics |
| Year of publication | 2011 |
| Journal volume | 30 |
| Journal issue | 2 |
| Pages of publication | 305 - 312 |
| a | 11.8836 ± 0.0011 Å |
| b | 23.225 ± 0.002 Å |
| c | 17.791 ± 0.0016 Å |
| α | 90° |
| β | 92.918 ± 0.002° |
| γ | 90° |
| Cell volume | 4903.9 ± 0.8 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0307 |
| Residual factor for significantly intense reflections | 0.0254 |
| Weighted residual factors for significantly intense reflections | 0.0606 |
| Weighted residual factors for all reflections included in the refinement | 0.0645 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.081 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178529 (current) | 2016-03-21 | cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/34. |
4063405.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4063405.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4063405.cif |
| 18993 | 2011-05-06 | ../uploads/cif-deposit/cod/cif Adding structures of 4063399, 4063400, 4063401, 4063402, 4063403, 4063404, 4063405, 4063406 via cif-deposit CGI script. |
4063405.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.