Crystallography Open Database

Information card for entry 4063532

Preview

Coordinates	4063532.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H38 F3 N O4 P Rh S2
Calculated formula	C32 H38 F3 N O4 P Rh S2
Title of publication	Cationic Rhodium (I) Complexes ofN-Phosphino-tert-butylsulfinamide Ligands: Synthesis, Structure, and Coordination Modes
Authors of publication	Achard, Thierry; Benet-Buchholz, Jordi; Riera, Antoni; Verdaguer, Xavier
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	2
Pages of publication	480 - 487
a	10.7401 ± 0.0003 Å
b	11.1503 ± 0.0003 Å
c	27.2682 ± 0.0007 Å
α	90°
β	90°
γ	90°
Cell volume	3265.51 ± 0.15 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	8
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0222
Residual factor for significantly intense reflections	0.0214
Weighted residual factors for significantly intense reflections	0.0562
Weighted residual factors for all reflections included in the refinement	0.0566
Goodness-of-fit parameter for all reflections included in the refinement	1.066
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178530 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/35.	4063532.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4063532.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4063532.cif
22903	2011-08-04	../uploads/cif-deposit/cod/cif Adding structures of 4063532 via cif-deposit CGI script.	4063532.cif