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Information card for entry 4064015
Preview
| Coordinates | 4064015.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C38.84 H46.34 Cl1.31 N3.34 O P Pd2 |
|---|---|
| Calculated formula | C38.8465 H46.3465 Cl1.307 N3.3465 O P Pd2 |
| Title of publication | Asymmetric Synthesis of P-Stereogenic Homo- and Heterobimetallic Complexes via Selective Monoinsertion of Dialkynylphosphine into the Pd−C Bond of a Palladacycle |
| Authors of publication | Chen, Shuli; Pullarkat, Sumod A.; Li, Yongxin; Leung, Pak-Hing |
| Journal of publication | Organometallics |
| Year of publication | 2011 |
| Journal volume | 30 |
| Journal issue | 6 |
| Pages of publication | 1530 |
| a | 9.9213 ± 0.0003 Å |
| b | 11.839 ± 0.0004 Å |
| c | 18.3636 ± 0.0006 Å |
| α | 76.468 ± 0.002° |
| β | 81.334 ± 0.002° |
| γ | 65.288 ± 0.001° |
| Cell volume | 1901.61 ± 0.11 Å3 |
| Cell temperature | 103 ± 2 K |
| Ambient diffraction temperature | 103 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 1 |
| Hermann-Mauguin space group symbol | P 1 |
| Hall space group symbol | P 1 |
| Residual factor for all reflections | 0.0364 |
| Residual factor for significantly intense reflections | 0.0328 |
| Weighted residual factors for significantly intense reflections | 0.0729 |
| Weighted residual factors for all reflections included in the refinement | 0.0868 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.077 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178502 (current) | 2016-03-21 | cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/40. |
4064015.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4064015.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4064015.cif |
| 32752 | 2012-02-10 | ../uploads/cif-deposit/cod/cif Adding structures of 4064011, 4064012, 4064013, 4064014, 4064015, 4064016, 4064017 via cif-deposit CGI script. |
4064015.cif |
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