Crystallography Open Database

Information card for entry 4064256

Preview

Coordinates	4064256.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H30.5 Ir4 O10 P Sn
Calculated formula	C46 H30.5 Ir4 O10 P Sn
Title of publication	A New Method for Introducing Tin Ligands into Tetrairidium Dodecacarbonyl
Authors of publication	Adams, Richard D.; Chen, Mingwei; Trufan, Eszter; Zhang, Qiang
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	4
Pages of publication	661
a	14.9667 ± 0.0005 Å
b	15.1697 ± 0.0005 Å
c	22.6389 ± 0.0008 Å
α	87.51 ± 0.001°
β	80.445 ± 0.001°
γ	68.589 ± 0.001°
Cell volume	4718 ± 0.3 Å³
Cell temperature	294 ± 2 K
Ambient diffraction temperature	294 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.059
Residual factor for significantly intense reflections	0.0364
Weighted residual factors for significantly intense reflections	0.0803
Weighted residual factors for all reflections included in the refinement	0.0895
Goodness-of-fit parameter for all reflections included in the refinement	1.006
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4064256.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4064256.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4064256.cif
32829	2012-02-10	../uploads/cif-deposit/cod/cif Adding structures of 4064254, 4064255, 4064256 via cif-deposit CGI script.	4064256.cif