Crystallography Open Database

Information card for entry 4064483

Preview

Coordinates	4064483.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H49 N P2 Ru Zr
Calculated formula	C30 H49 N P2 Ru Zr
Title of publication	Synthesis of Group IV (Zr, Hf)−Group VIII (Fe, Ru) Heterobimetallic Complexes Bearing Metallocenyl Diphosphine Moieties and Their Application to Catalytic Dehydrogenation of Amine−Boranes
Authors of publication	Miyazaki, Takamasa; Tanabe, Yoshiaki; Yuki, Masahiro; Miyake, Yoshihiro; Nishibayashi, Yoshiaki
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	8
Pages of publication	2394
a	18.4803 ± 0.0009 Å
b	14.9182 ± 0.0006 Å
c	10.8453 ± 0.0005 Å
α	90°
β	90°
γ	90°
Cell volume	2990 ± 0.2 Å³
Cell temperature	173.1 K
Ambient diffraction temperature	173.1 K
Number of distinct elements	6
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for significantly intense reflections	0.0279
Weighted residual factors for all reflections included in the refinement	0.0713
Goodness-of-fit parameter for all reflections included in the refinement	1
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4064483.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4064483.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4064483.cif
32920	2012-02-11	../uploads/cif-deposit/cod/cif Adding structures of 4064473, 4064474, 4064475, 4064476, 4064477, 4064478, 4064479, 4064480, 4064481, 4064482, 4064483, 4064484 via cif-deposit CGI script.	4064483.cif