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Information card for entry 4064517
Preview
| Coordinates | 4064517.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C36 H56 P4 Pd2 Si2 |
|---|---|
| Calculated formula | C36 H56 P4 Pd2 Si2 |
| SMILES | c1c(cccc1)[Si]1([Pd]([P](C)(C)C)([P](C)(C)C)[Si](c2ccccc2)(c2ccccc2)[Pd]1([P](C)(C)C)[P](C)(C)C)c1ccccc1 |
| Title of publication | Dinuclear Palladium and Platinum Complexes with Bridging Silylene Ligands. Preparation Using (Aminosilyl)boronic Ester as the Ligand Precursor and Their Reactions with Alkynes |
| Authors of publication | Tanabe, Makoto; Jiang, Jian; Yamazawa, Hideto; Osakada, Kohtaro; Ohmura, Toshimichi; Suginome, Michinori |
| Journal of publication | Organometallics |
| Year of publication | 2011 |
| Journal volume | 30 |
| Journal issue | 15 |
| Pages of publication | 3981 |
| a | 9.609 ± 0.004 Å |
| b | 10.751 ± 0.005 Å |
| c | 11.421 ± 0.005 Å |
| α | 98.7843 ± 0.0013° |
| β | 111.692 ± 0.004° |
| γ | 106.126 ± 0.007° |
| Cell volume | 1009.2 ± 0.8 Å3 |
| Cell temperature | 113.1 K |
| Ambient diffraction temperature | 113 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0404 |
| Residual factor for significantly intense reflections | 0.0316 |
| Weighted residual factors for significantly intense reflections | 0.0828 |
| Weighted residual factors for all reflections included in the refinement | 0.0861 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.989 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176467 (current) | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4064517.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4064517.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4064517.cif |
| 32935 | 2012-02-11 | ../uploads/cif-deposit/cod/cif Adding structures of 4064516, 4064517, 4064518, 4064519, 4064520, 4064521, 4064522 via cif-deposit CGI script. |
4064517.cif |
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Users of the data should acknowledge the original authors of the
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