Crystallography Open Database

Information card for entry 4064519

Preview

Coordinates	4064519.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C47.5 H52 P2 Pd Si2
Calculated formula	C47.5 H53 P2 Pd Si2
Title of publication	Dinuclear Palladium and Platinum Complexes with Bridging Silylene Ligands. Preparation Using (Aminosilyl)boronic Ester as the Ligand Precursor and Their Reactions with Alkynes
Authors of publication	Tanabe, Makoto; Jiang, Jian; Yamazawa, Hideto; Osakada, Kohtaro; Ohmura, Toshimichi; Suginome, Michinori
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	15
Pages of publication	3981
a	10.113 ± 0.0014 Å
b	20.167 ± 0.003 Å
c	21.381 ± 0.003 Å
α	90°
β	96.812 ± 0.002°
γ	90°
Cell volume	4329.8 ± 1.1 Å³
Cell temperature	113 K
Ambient diffraction temperature	113 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0666
Residual factor for significantly intense reflections	0.047
Weighted residual factors for significantly intense reflections	0.108
Weighted residual factors for all reflections included in the refinement	0.1175
Goodness-of-fit parameter for all reflections included in the refinement	1.093
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4064519.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4064519.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4064519.cif
32935	2012-02-11	../uploads/cif-deposit/cod/cif Adding structures of 4064516, 4064517, 4064518, 4064519, 4064520, 4064521, 4064522 via cif-deposit CGI script.	4064519.cif