Crystallography Open Database

Information card for entry 4064838

Preview

Coordinates	4064838.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C45 H76 Al2 N2
Calculated formula	C45 H76 Al2 N2
Title of publication	Reactivity of Permethylated Magnesium Complexes toward β-Diimines
Authors of publication	Michel, Olaf; Yamamoto, Koji; Tsurugi, Hayato; Maichle-Mössmer, Cäcilia; Törnroos, Karl W.; Mashima, Kazushi; Anwander, Reiner
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	14
Pages of publication	3818
a	37.826 ± 0.004 Å
b	11.3329 ± 0.0011 Å
c	24.359 ± 0.002 Å
α	90°
β	112.235 ± 0.009°
γ	90°
Cell volume	9665.7 ± 1.7 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.195
Residual factor for significantly intense reflections	0.1489
Weighted residual factors for significantly intense reflections	0.2953
Weighted residual factors for all reflections included in the refinement	0.3116
Goodness-of-fit parameter for all reflections included in the refinement	1.598
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178542 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/48.	4064838.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4064838.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4064838.cif
33061	2012-02-11	../uploads/cif-deposit/cod/cif Adding structures of 4064835, 4064836, 4064837, 4064838, 4064839 via cif-deposit CGI script.	4064838.cif