Crystallography Open Database

Information card for entry 4064901

Preview

Coordinates	4064901.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C88 H106 O1.63 Sn2
Calculated formula	C88 H106 O1.64 Sn2.02
Title of publication	Tethered Heavy Dicarbene Analogues: Synthesis and Structure of Ditetryldiyl Ethers (Ar′E)2(μ-O) (E = Ge, Sn; Ar′ = C6H3-2,6-(C6H3-2,6-iPr2)2)
Authors of publication	Summerscales, Owen T.; Olmstead, Marilyn M.; Power, Philip P.
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	13
Pages of publication	3468
a	11.9117 ± 0.0008 Å
b	13.3946 ± 0.0004 Å
c	13.7183 ± 0.0005 Å
α	111.263 ± 0.002°
β	103.04 ± 0.002°
γ	102.296 ± 0.002°
Cell volume	1879.52 ± 0.16 Å³
Cell temperature	90 ± 2 K
Ambient diffraction temperature	90 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0274
Residual factor for significantly intense reflections	0.0239
Weighted residual factors for significantly intense reflections	0.0614
Weighted residual factors for all reflections included in the refinement	0.0633
Goodness-of-fit parameter for all reflections included in the refinement	1.031
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178543 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/49.	4064901.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4064901.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4064901.cif
33084	2012-02-11	../uploads/cif-deposit/cod/cif Adding structures of 4064901 via cif-deposit CGI script.	4064901.cif