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Information card for entry 4065061
Preview
| Coordinates | 4065061.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H54 Cl2 Sn3 |
|---|---|
| Calculated formula | C24 H54 Cl2 Sn3 |
| SMILES | C(C)(C)(C)[Sn]([Sn](C(C)(C)C)(C(C)(C)C)[Sn](C(C)(C)C)(C(C)(C)C)Cl)(C(C)(C)C)Cl |
| Title of publication | Reaction betweentBuMgCl and SnCl4, Illustrating the Solvent-Dependent Predominant Formation of Cl(tBu2Sn)nCl (THF,n= 1; Toluene,n= 2; Hexane,n= 3) and the Subsequent Wavelength-Selective Photochemical Transformation ofn= 3 →2 →1 |
| Authors of publication | Sharma, Hemant K.; Miramontes, Alma; Metta-Magaña, Alejandro J.; Pannell, Keith H. |
| Journal of publication | Organometallics |
| Year of publication | 2011 |
| Journal volume | 30 |
| Journal issue | 17 |
| Pages of publication | 4501 |
| a | 22.234 ± 0.006 Å |
| b | 9.352 ± 0.002 Å |
| c | 17.041 ± 0.004 Å |
| α | 90° |
| β | 112.376 ± 0.003° |
| γ | 90° |
| Cell volume | 3276.6 ± 1.4 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.03 |
| Residual factor for significantly intense reflections | 0.0212 |
| Weighted residual factors for significantly intense reflections | 0.0425 |
| Weighted residual factors for all reflections included in the refinement | 0.0479 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.126 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178503 (current) | 2016-03-21 | cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/50. |
4065061.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4065061.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4065061.cif |
| 33148 | 2012-02-11 | ../uploads/cif-deposit/cod/cif Adding structures of 4065061 via cif-deposit CGI script. |
4065061.cif |
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Users of the data should acknowledge the original authors of the
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