Crystallography Open Database

Information card for entry 4065366

Preview

Coordinates	4065366.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C69 H74 Cl6 Cr2 N4 O
Calculated formula	C69 H74 Cl6 Cr2 N4 O
Title of publication	Chromium Complexes with Acenaphthene Imine Derivative Ligands Synthesis and Catalysis on Diene Polymerization
Authors of publication	Gao, Bo; Gao, Wei; Wu, Qiaolin; Luo, Xuyang; Zhang, Jingshun; Su, Qing; Mu, Ying
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	20
Pages of publication	5480
a	14.448 ± 0.0009 Å
b	15.1031 ± 0.0009 Å
c	16.4755 ± 0.001 Å
α	76.028 ± 0.001°
β	83.591 ± 0.001°
γ	69.277 ± 0.001°
Cell volume	3261.7 ± 0.3 Å³
Cell temperature	185 ± 2 K
Ambient diffraction temperature	185 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0982
Residual factor for significantly intense reflections	0.083
Weighted residual factors for significantly intense reflections	0.255
Weighted residual factors for all reflections included in the refinement	0.2752
Goodness-of-fit parameter for all reflections included in the refinement	1.051
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178546 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/53.	4065366.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4065366.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4065366.cif
33259	2012-02-11	../uploads/cif-deposit/cod/cif Adding structures of 4065365, 4065366, 4065367, 4065368 via cif-deposit CGI script.	4065366.cif