Crystallography Open Database

Information card for entry 4065681

Preview

Coordinates	4065681.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C50 H72 I4 N8 Zn4
Calculated formula	C50 H72 I4 N8 Zn4
Title of publication	Synthesis and X-ray Crystal Structures of Tetranuclear Zincamidinate Complexes
Authors of publication	Gutschank, Benjamin; Schulz, Stephan; Westphal, Ulrich; Bläser, Dieter; Boese, Roland
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	9
Pages of publication	2093
a	12.208 ± 0.0009 Å
b	12.208 ± 0.0009 Å
c	34.722 ± 0.003 Å
α	90°
β	90°
γ	120°
Cell volume	4481.5 ± 0.6 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	154
Hermann-Mauguin space group symbol	P 32 2 1
Hall space group symbol	P 32 2"
Residual factor for all reflections	0.0354
Residual factor for significantly intense reflections	0.0346
Weighted residual factors for significantly intense reflections	0.073
Weighted residual factors for all reflections included in the refinement	0.0732
Goodness-of-fit parameter for all reflections included in the refinement	1.291
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178549 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/56.	4065681.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4065681.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4065681.cif
33652	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4065679, 4065680, 4065681 via cif-deposit CGI script.	4065681.cif