Crystallography Open Database

Information card for entry 4065698

Preview

Coordinates	4065698.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H19 O5 P Si W
Calculated formula	C22 H19 O5 P Si W
Title of publication	Reactivity of 2-Silyl- and 2-Stannyl-Substituted Phosphirenes
Authors of publication	Panichakul, Duanghathai; Lim, Yi Wee; Mathey, François
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	8
Pages of publication	1985
a	9.5783 ± 0.0003 Å
b	9.7533 ± 0.0003 Å
c	12.4712 ± 0.0004 Å
α	90°
β	90.589 ± 0.002°
γ	90°
Cell volume	1165 ± 0.06 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.026
Residual factor for significantly intense reflections	0.0196
Weighted residual factors for significantly intense reflections	0.0386
Weighted residual factors for all reflections included in the refinement	0.041
Goodness-of-fit parameter for all reflections included in the refinement	1.065
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178549 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/56.	4065698.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4065698.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4065698.cif
33659	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4065698 via cif-deposit CGI script.	4065698.cif