Crystallography Open Database

Information card for entry 4065757

Preview

Coordinates	4065757.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C128 H112 Cl12 N2 O4 Os2 P6
Calculated formula	C128 H112 Cl12 N2 O4 Os2 P6
Title of publication	Synthesis, Characterization, and Electrochemical Properties of Bisosmabenzenes Bridged by Diisocyanides
Authors of publication	Huang, Jinbo; Lin, Ran; Wu, Liqiong; Zhao, Qianyi; Zhu, Congqing; Wen, Ting Bin; Xia, Haiping
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	13
Pages of publication	2916
a	13.2136 ± 0.0004 Å
b	13.7646 ± 0.0004 Å
c	18.1729 ± 0.0006 Å
α	103.599 ± 0.003°
β	99.835 ± 0.003°
γ	95.375 ± 0.002°
Cell volume	3134.35 ± 0.18 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0487
Residual factor for significantly intense reflections	0.0368
Weighted residual factors for significantly intense reflections	0.0927
Weighted residual factors for all reflections included in the refinement	0.0955
Goodness-of-fit parameter for all reflections included in the refinement	1
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178550 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/57.	4065757.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4065757.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4065757.cif
33679	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4065757 via cif-deposit CGI script.	4065757.cif