Crystallography Open Database

Information card for entry 4065893

Preview

Coordinates	4065893.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H21 Cl F6 N7 Os P
Calculated formula	C23 H21 Cl F6 N7 Os P
Title of publication	Osmium Complexes Containing N-Heterocyclic Carbene-Based C,N,C-Pincer Ligands
Authors of publication	Wong, Chun-Yuen; Lai, Lo-Ming; Pat, Pak-Kei; Chung, Lai-Hon
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	11
Pages of publication	2533
a	14.7557 ± 0.0002 Å
b	13.193 ± 0.0002 Å
c	14.9139 ± 0.0002 Å
α	90°
β	93.475 ± 0.001°
γ	90°
Cell volume	2897.98 ± 0.07 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0304
Residual factor for significantly intense reflections	0.0241
Weighted residual factors for significantly intense reflections	0.0587
Weighted residual factors for all reflections included in the refinement	0.0602
Goodness-of-fit parameter for all reflections included in the refinement	1.012
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178551 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/58.	4065893.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4065893.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4065893.cif
33720	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4065893 via cif-deposit CGI script.	4065893.cif