Crystallography Open Database

Information card for entry 4066223

Preview

Coordinates	4066223.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C60 H98 Al2 Ge Si8
Calculated formula	C60 H98 Al2 Ge Si8
Title of publication	Facile Synthesis of an Unsaturated Spiro Germane by Hydroalumination and Intramolecular 1,1-Carbalumination†
Authors of publication	Uhl, Werner; Rohling, Martina; Würthwein, Ernst-Ulrich; Ghavtadze, Nugzar; Bergander, Klaus
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	21
Pages of publication	5236
a	14.9993 ± 0.0005 Å
b	21.4156 ± 0.0007 Å
c	22.9117 ± 0.0008 Å
α	80.823 ± 0.001°
β	74.138 ± 0.001°
γ	80.236 ± 0.001°
Cell volume	6927 ± 0.4 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0914
Residual factor for significantly intense reflections	0.0485
Weighted residual factors for significantly intense reflections	0.1064
Weighted residual factors for all reflections included in the refinement	0.1223
Goodness-of-fit parameter for all reflections included in the refinement	0.976
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178554 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/62.	4066223.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4066223.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4066223.cif
33832	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4066223, 4066224 via cif-deposit CGI script.	4066223.cif