Crystallography Open Database

Information card for entry 4066399

Preview

Coordinates	4066399.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C35 H87 N8 O4 Zn4
Calculated formula	C35 H87 N8 O4 Zn4
Title of publication	Structural Study of the Reaction of Methylzinc Amino Alcoholates with Oxygen
Authors of publication	Hollingsworth, Nathan; Johnson, Andrew L.; Kingsley, Andrew; Kociok-Köhn, Gabriele; Molloy, Kieran C.
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	15
Pages of publication	3318
a	18.012 ± 0.0004 Å
b	15.054 ± 0.0004 Å
c	36.528 ± 0.001 Å
α	90°
β	97.679 ± 0.001°
γ	90°
Cell volume	9815.8 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1739
Residual factor for significantly intense reflections	0.1064
Weighted residual factors for significantly intense reflections	0.2546
Weighted residual factors for all reflections included in the refinement	0.2878
Goodness-of-fit parameter for all reflections included in the refinement	1.075
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178555 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/63.	4066399.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4066399.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4066399.cif
33885	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4066399, 4066400, 4066401, 4066402, 4066403, 4066404, 4066405 via cif-deposit CGI script.	4066399.cif