Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4066483
Preview
| Coordinates | 4066483.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C82 H104 Si2 Sn2 |
|---|---|
| Calculated formula | C82 H104 Si2 Sn2 |
| SMILES | c1(c(cccc1c1c(cccc1C(C)C)C(C)C)c1c(cccc1C(C)C)C(C)C)[Sn](C#C[Si](C)(C)C)[Sn](c1c(cccc1c1c(cccc1C(C)C)C(C)C)c1c(cccc1C(C)C)C(C)C)C#C[Si](C)(C)C.c1ccccc1.c1ccccc1 |
| Title of publication | Synthesis and Structures of Low-Valent Alkynyl Tin and Germanium Complexes Supported by Terphenyl Ligands: Heavier Group 14 Element Enediyne Analogues† |
| Authors of publication | Lei, Hao; Fettinger, James C.; Power, Philip P. |
| Journal of publication | Organometallics |
| Year of publication | 2010 |
| Journal volume | 29 |
| Journal issue | 21 |
| Pages of publication | 5585 |
| a | 12.7099 ± 0.0004 Å |
| b | 13.3036 ± 0.0004 Å |
| c | 13.6135 ± 0.0004 Å |
| α | 63.3794 ± 0.0003° |
| β | 74.5853 ± 0.0003° |
| γ | 62.9725 ± 0.0003° |
| Cell volume | 1827.52 ± 0.1 Å3 |
| Cell temperature | 90 ± 2 K |
| Ambient diffraction temperature | 90 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0237 |
| Residual factor for significantly intense reflections | 0.0226 |
| Weighted residual factors for significantly intense reflections | 0.0611 |
| Weighted residual factors for all reflections included in the refinement | 0.0618 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.059 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178556 (current) | 2016-03-21 | cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/64. |
4066483.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4066483.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4066483.cif |
| 33908 | 2012-02-13 | ../uploads/cif-deposit/cod/cif Adding structures of 4066483, 4066484, 4066485, 4066486 via cif-deposit CGI script. |
4066483.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.