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Information card for entry 4066900
Preview
Coordinates | 4066900.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H27 Br0.5 Cl0.5 N P Si |
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Calculated formula | C22 H27 Br0.5 Cl0.5 N P Si |
Title of publication | Facile Synthesis of Bifunctional Ligands using LiCH2PPh2═NPh Obtained from [PhNH−PPh3+][Br−] |
Authors of publication | Cao, Thi-Phuong-Anh; Payet, Elina; Auffrant, Audrey; Le Goff, Xavier F.; Le Floch, Pascal |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 17 |
Pages of publication | 3991 |
a | 18.378 ± 0.001 Å |
b | 11.475 ± 0.001 Å |
c | 22.068 ± 0.001 Å |
α | 90° |
β | 108.329 ± 0.001° |
γ | 90° |
Cell volume | 4417.8 ± 0.5 Å3 |
Cell temperature | 150 ± 0.1 K |
Ambient diffraction temperature | 150 ± 0.1 K |
Number of distinct elements | 7 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0571 |
Residual factor for significantly intense reflections | 0.0338 |
Weighted residual factors for significantly intense reflections | 0.0807 |
Weighted residual factors for all reflections included in the refinement | 0.0872 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.054 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
176467 (current) | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4066900.cif |
91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4066900.cif |
34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4066900.cif |
34017 | 2012-02-13 | ../uploads/cif-deposit/cod/cif Adding structures of 4066899, 4066900, 4066901 via cif-deposit CGI script. |
4066900.cif |
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Users of the data should acknowledge the original authors of the
structural data.