Crystallography Open Database

Information card for entry 4067105

Preview

Coordinates	4067105.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40.5 H37 B Cl F4 N2 O3.5 P2 Rh2
Calculated formula	C40.5 H37 B Cl F4 N2 O3.5 P2 Rh2
Title of publication	Dirhodium Complexes Bridged by Bis(diphenylphosphino)phthalazine (PNNPPh): Central Ring Size and Charge Effects As Compared with the Pyrazolate Derivative (PNNPPy)
Authors of publication	Yamaguchi, Takafumi; Koike, Takashi; Akita, Munetaka
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	23
Pages of publication	6493
a	11.088 ± 0.001 Å
b	12.5827 ± 0.0008 Å
c	15.695 ± 0.001 Å
α	105.234 ± 0.004°
β	93.866 ± 0.004°
γ	95.413 ± 0.004°
Cell volume	2093.6 ± 0.3 Å³
Cell temperature	213.2 K
Ambient diffraction temperature	213 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.0388
Weighted residual factors for all reflections included in the refinement	0.1313
Goodness-of-fit parameter for all reflections included in the refinement	1.027
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4067105.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4067105.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4067105.cif
34085	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4067103, 4067104, 4067105, 4067106, 4067107, 4067108, 4067109, 4067110, 4067111, 4067112 via cif-deposit CGI script.	4067105.cif