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Information card for entry 4067242
Preview
| Coordinates | 4067242.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C37 H60 N8 Zn4 |
|---|---|
| Calculated formula | C37 H60 N8 Zn4 |
| SMILES | [Zn]12([N]3(C(C)C)[Zn]4([N]1(C1=[N]([Zn]5([N]6(C(C)C)[Zn]7([N](=C3C1(C(=[N]4C(C)C)[N]57C(C)C)C6=[N]2C(C)C)C(C)C)C#C)C#C)C(C)C)C(C)C)C#C)C#C |
| Title of publication | Synthesis, Structure, and Reactivity of a Tetranuclear Amidinato Zinc Hydride Complex |
| Authors of publication | Gutschank, Benjamin; Schulz, Stephan; Bläser, Dieter; Boese, Roland; Wölper, Christoph |
| Journal of publication | Organometallics |
| Year of publication | 2010 |
| Journal volume | 29 |
| Journal issue | 22 |
| Pages of publication | 6133 |
| a | 10.6259 ± 0.0008 Å |
| b | 11.0517 ± 0.0008 Å |
| c | 18.1353 ± 0.0013 Å |
| α | 85.136 ± 0.004° |
| β | 89.363 ± 0.004° |
| γ | 72.877 ± 0.004° |
| Cell volume | 2027.8 ± 0.3 Å3 |
| Cell temperature | 103 ± 1 K |
| Ambient diffraction temperature | 103 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0477 |
| Residual factor for significantly intense reflections | 0.0291 |
| Weighted residual factors for significantly intense reflections | 0.0614 |
| Weighted residual factors for all reflections included in the refinement | 0.0671 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.007 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178563 (current) | 2016-03-21 | cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/72. |
4067242.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4067242.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4067242.cif |
| 34129 | 2012-02-13 | ../uploads/cif-deposit/cod/cif Adding structures of 4067240, 4067241, 4067242 via cif-deposit CGI script. |
4067242.cif |
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Users of the data should acknowledge the original authors of the
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