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Information card for entry 4067280
Preview
| Coordinates | 4067280.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C27 H53 Lu O Si4 |
|---|---|
| Calculated formula | C27 H53 Lu O Si4 |
| SMILES | [Lu]1234([O]5CCCC5)([c]56[c]4([c]3([Si](C)(C)C)[cH]2[c]15[Si](C)(C)C)cccc6)(C[Si](C)(C)C)C[Si](C)(C)C |
| Title of publication | Half-Sandwich Indenyl Rare Earth Metal Dialkyl Complexes: Syntheses, Structures, and Catalytic Activities of (1,3-(SiMe3)2C9H5)Ln(CH2SiMe3)2(THF) |
| Authors of publication | Xu, Xin; Chen, Yaofeng; Feng, Jian; Zou, Gang; Sun, Jie |
| Journal of publication | Organometallics |
| Year of publication | 2010 |
| Journal volume | 29 |
| Journal issue | 3 |
| Pages of publication | 549 |
| a | 10.2276 ± 0.0007 Å |
| b | 15.9273 ± 0.0011 Å |
| c | 22.0779 ± 0.0016 Å |
| α | 90° |
| β | 97.619 ± 0.001° |
| γ | 90° |
| Cell volume | 3564.7 ± 0.4 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0636 |
| Residual factor for significantly intense reflections | 0.0333 |
| Weighted residual factors for significantly intense reflections | 0.0662 |
| Weighted residual factors for all reflections included in the refinement | 0.0729 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.831 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178563 (current) | 2016-03-21 | cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/72. |
4067280.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4067280.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4067280.cif |
| 34146 | 2012-02-13 | ../uploads/cif-deposit/cod/cif Adding structures of 4067279, 4067280, 4067281 via cif-deposit CGI script. |
4067280.cif |
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Users of the data should acknowledge the original authors of the
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