Crystallography Open Database

Information card for entry 4067290

Preview

Coordinates	4067290.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	4,6-diphenyl-2,2,2-tris(trifluoromethyl)-2H,4H-1,3,2-dioxagermin-2-ium-4-ide
Formula	C18 H11 F9 Ge O2
Calculated formula	C18 H11 F9 Ge O2
Title of publication	Neutral Pentacoordinate Group 14 Compounds with β-Diketonato ligands
Authors of publication	Bombicz, Petra; Kovács, Ilona; Nyulászi, László; Szieberth, Dénes; Terleczky, Péter
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	5
Pages of publication	1100
a	19.612 ± 0.004 Å
b	14.042 ± 0.003 Å
c	13.579 ± 0.003 Å
α	90°
β	105.02 ± 0.03°
γ	90°
Cell volume	3611.8 ± 1.4 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0656
Residual factor for significantly intense reflections	0.0609
Weighted residual factors for significantly intense reflections	0.1695
Weighted residual factors for all reflections included in the refinement	0.1755
Goodness-of-fit parameter for all reflections included in the refinement	1.088
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178563 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/72.	4067290.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4067290.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4067290.cif
34150	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4067290 via cif-deposit CGI script.	4067290.cif