Crystallography Open Database

Information card for entry 4067295

Preview

Coordinates	4067295.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	(N,N,N'N'-tetraethylethylenediamine)-bis(s-butyl)-zinc
Formula	C18 H40 N2 Zn
Calculated formula	C18 H40 N2 Zn
Title of publication	Toward Total Spontaneous Resolution ofsec-Butylzinc Complexes
Authors of publication	Lennartson, Anders; Hedström, Anna; Håkansson, Mikael
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	1
Pages of publication	177
a	18.546 ± 0.005 Å
b	9.3694 ± 0.0019 Å
c	13.01 ± 0.004 Å
α	90°
β	114.528 ± 0.007°
γ	90°
Cell volume	2056.7 ± 0.9 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0334
Residual factor for significantly intense reflections	0.0295
Weighted residual factors for significantly intense reflections	0.0711
Weighted residual factors for all reflections included in the refinement	0.0723
Goodness-of-fit parameter for all reflections included in the refinement	1.093
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178563 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/72.	4067295.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4067295.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4067295.cif
34151	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4067291, 4067292, 4067293, 4067294, 4067295, 4067296, 4067297, 4067298 via cif-deposit CGI script.	4067295.cif