Crystallography Open Database

Information card for entry 4067625

Preview

Coordinates	4067625.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	{2,6-bis[1-(2,6-dimethylphenylimino)ethyl]pyridine} (trimethylsilylmethyl) cobalt(I)
Formula	C29 H38 Co N3 Si
Calculated formula	C29 H38 Co N3 Si
Title of publication	(Py)2Co(CH2SiMe3)2As an Easily Accessible Source of “CoR2”
Authors of publication	Zhu, Di; Janssen, Femke F. B. J.; Budzelaar, Peter H. M.
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	8
Pages of publication	1897
a	7.6802 ± 0.0003 Å
b	21.277 ± 0.001 Å
c	8.5207 ± 0.0004 Å
α	90°
β	99.1876 ± 0.0011°
γ	90°
Cell volume	1374.52 ± 0.11 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0398
Residual factor for significantly intense reflections	0.0379
Weighted residual factors for significantly intense reflections	0.0995
Weighted residual factors for all reflections included in the refinement	0.1008
Goodness-of-fit parameter for all reflections included in the refinement	1.075
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178567 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/76.	4067625.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4067625.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4067625.cif
34250	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4067621, 4067622, 4067623, 4067624, 4067625 via cif-deposit CGI script.	4067625.cif