Crystallography Open Database

Information card for entry 4067726

Preview

Coordinates	4067726.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C105.4 H103.44 Cl7.32 P4 Zn4
Calculated formula	C105.372 H103.43 Cl7.314 P4 Zn4
Title of publication	Isolation and Structures of Two New Organozinc Anions from Solutions Rich in Halide Ions
Authors of publication	MacIntosh, Ian S.; Sherren, Cody N.; Robertson, Katherine N.; Masuda, Jason D.; Pye, Cory C.; Clyburne, Jason A. C.
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	9
Pages of publication	2063
a	11.4075 ± 0.0011 Å
b	13.3666 ± 0.0013 Å
c	17.1784 ± 0.0016 Å
α	86.488 ± 0.001°
β	71.105 ± 0.001°
γ	87.171 ± 0.001°
Cell volume	2472.3 ± 0.4 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0806
Residual factor for significantly intense reflections	0.0432
Weighted residual factors for significantly intense reflections	0.1034
Weighted residual factors for all reflections included in the refinement	0.1198
Goodness-of-fit parameter for all reflections included in the refinement	1.015
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4067726.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4067726.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4067726.cif
34278	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4067723, 4067724, 4067725, 4067726 via cif-deposit CGI script.	4067726.cif