Crystallography Open Database

Information card for entry 4067892

Preview

Coordinates	4067892.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H24 Cl F6 N6 P Ru
Calculated formula	C23 H24 Cl F6 N6 P Ru
Title of publication	Carbene Transfer Reactivities of Nickel(II)‒N-Heterocyclic Carbene Complexes and Their Applications in the Synthesis of Metal‒NHC Complexes
Authors of publication	Liu, Bo; Liu, Xiaolong; Chen, Chao; Chen, Congyan; Chen, Wanzhi
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	1
Pages of publication	282
a	8.125 ± 0.0003 Å
b	14.2921 ± 0.0005 Å
c	23.9513 ± 0.0008 Å
α	90°
β	94.439 ± 0.003°
γ	90°
Cell volume	2772.96 ± 0.17 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0677
Residual factor for significantly intense reflections	0.0515
Weighted residual factors for significantly intense reflections	0.1311
Weighted residual factors for all reflections included in the refinement	0.1423
Goodness-of-fit parameter for all reflections included in the refinement	1.073
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178569 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/78.	4067892.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4067892.cif
38020	2012-03-04	../uploads/cif-deposit/cod/cif Adding structures of 4067886, 4067887, 4067888, 4067889, 4067890, 4067891, 4067892 via cif-deposit CGI script.	4067892.cif