Crystallography Open Database

Information card for entry 4068913

Preview

Coordinates	4068913.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H42 Cl I N2 Si
Calculated formula	C30 H42 Cl I N2 Si
Title of publication	Reactivity of a Zwitterionic Stable Silylene toward Halosilanes and Haloalkanes
Authors of publication	Xiong, Yun; Yao, Shenglai; Driess, Matthias
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	6
Pages of publication	1927
a	10.8539 ± 0.0004 Å
b	12.5672 ± 0.0004 Å
c	13.3929 ± 0.0005 Å
α	66.973 ± 0.003°
β	74.202 ± 0.003°
γ	65.382 ± 0.004°
Cell volume	1515.36 ± 0.11 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.04
Residual factor for significantly intense reflections	0.0305
Weighted residual factors for significantly intense reflections	0.0793
Weighted residual factors for all reflections included in the refinement	0.0817
Goodness-of-fit parameter for all reflections included in the refinement	0.885
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178579 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/89.	4068913.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4068913.cif
40039	2012-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4068911, 4068912, 4068913, 4068914, 4068915, 4068916 via cif-deposit CGI script.	4068913.cif