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Information card for entry 4069035
Preview
| Coordinates | 4069035.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | em4 |
|---|---|
| Formula | C32 H46 La N3 Si |
| Calculated formula | C32 H46 La N3 Si |
| Title of publication | Synthetic Diversity in the Formation of Triazoles from Nitriles and Diazo Compounds Using Metallocenes of Electropositive Metals |
| Authors of publication | Evans, William J.; Montalvo, Elizabeth; Champagne, Timothy M.; Ziller, Joseph W.; DiPasquale, Antonio G.; Rheingold, Arnold L. |
| Journal of publication | Organometallics |
| Year of publication | 2009 |
| Journal volume | 28 |
| Journal issue | 9 |
| Pages of publication | 2897 |
| a | 10.3739 ± 0.0017 Å |
| b | 22.451 ± 0.004 Å |
| c | 13.132 ± 0.002 Å |
| α | 90° |
| β | 97.526 ± 0.003° |
| γ | 90° |
| Cell volume | 3032.2 ± 0.9 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0745 |
| Residual factor for significantly intense reflections | 0.0426 |
| Weighted residual factors for significantly intense reflections | 0.0819 |
| Weighted residual factors for all reflections included in the refinement | 0.0905 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.007 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 204147 (current) | 2017-12-11 | cif/ Correcting the '_space_group.centring_type' data item enumeration values with the help of the cif_fix_values script from the cod-tools package revision 5887. |
4069035.cif |
| 178507 | 2016-03-21 | cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/90. |
4069035.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4069035.cif |
| 40100 | 2012-03-07 | ../uploads/cif-deposit/cod/cif Adding structures of 4069033, 4069034, 4069035, 4069036, 4069037, 4069038 via cif-deposit CGI script. |
4069035.cif |
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Users of the data should acknowledge the original authors of the
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