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Information card for entry 4069182
Preview
| Coordinates | 4069182.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | Zirconium amido choloride |
|---|---|
| Chemical name | Zirconium Trimethyl silyl amido dimethyl amido chloride |
| Formula | C20 H60 Cl2 N6 Si4 Zr2 |
| Calculated formula | C20 H60 Cl2 N6 Si4 Zr2 |
| SMILES | CN(C)[Zr]1([Cl][Zr](N(C)C)(N(C)C)(N([Si](C)(C)C)[Si](C)(C)C)[Cl]1)(N(C)C)N([Si](C)(C)C)[Si](C)(C)C |
| Title of publication | Synthesis and Characterization of Group 4 Amide Chloride and Amide Imide Complexes |
| Authors of publication | Yu, Xianghua; Chen, Shu-Jian; Wang, Xiaoping; Chen, Xue-Tai; Xue, Zi-Ling |
| Journal of publication | Organometallics |
| Year of publication | 2009 |
| Journal volume | 28 |
| Journal issue | 15 |
| Pages of publication | 4269 |
| a | 24.927 ± 0.007 Å |
| b | 10.387 ± 0.003 Å |
| c | 15.126 ± 0.004 Å |
| α | 90° |
| β | 104.245 ± 0.005° |
| γ | 90° |
| Cell volume | 3796 ± 1.8 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0225 |
| Residual factor for significantly intense reflections | 0.0191 |
| Weighted residual factors for significantly intense reflections | 0.0549 |
| Weighted residual factors for all reflections included in the refinement | 0.0625 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.559 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 273129 (current) | 2022-02-23 | cif/4 Fixing Z values and formulae |
4069182.cif |
| 178580 | 2016-03-21 | cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/91. |
4069182.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4069182.cif |
| 40167 | 2012-03-07 | ../uploads/cif-deposit/cod/cif Adding structures of 4069182 via cif-deposit CGI script. |
4069182.cif |
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