Crystallography Open Database

Information card for entry 4069373

Preview

Coordinates	4069373.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H35 B F4 N4 O0.5 Rh
Calculated formula	C32 H35 B F4 N4 O0.5 Rh
Title of publication	Thermochromic and Aggregation Properties of Bis(phenylisocyano) Rhodium(I) Diimine Complexes
Authors of publication	Lo, Larry Tso-Lun; Ng, Chi-On; Feng, Hua; Ko, Chi-Chiu
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	13
Pages of publication	3597
a	19.0965 ± 0.0004 Å
b	20.8077 ± 0.0004 Å
c	15.4552 ± 0.0003 Å
α	90°
β	96.555 ± 0.002°
γ	90°
Cell volume	6101 ± 0.2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0695
Residual factor for significantly intense reflections	0.0468
Weighted residual factors for significantly intense reflections	0.1051
Weighted residual factors for all reflections included in the refinement	0.114
Goodness-of-fit parameter for all reflections included in the refinement	0.996
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4069373.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4069373.cif
40265	2012-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4069373 via cif-deposit CGI script.	4069373.cif