Crystallography Open Database

Information card for entry 4069409

Preview

Coordinates	4069409.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H39 Ge I Si4
Calculated formula	C14 H39 Ge I Si4
SMILES	[GeH](I)(C([Si](C)(C)C)[Si](C)(C)C)C([Si](C)(C)C)[Si](C)(C)C
Title of publication	Silylene- and Germylene-Mediated C−H Activation: Reaction with Alkanes, Ethers, and Amines
Authors of publication	Walker, Randon H.; Miller, Karla A.; Scott, Sara L.; Cygan, Zuzanna T.; Bartolin, Jeffrey M.; Kampf, Jeff W.; Banaszak Holl, Mark M.
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	9
Pages of publication	2744
a	9.2067 ± 0.001 Å
b	21.527 ± 0.002 Å
c	13.1974 ± 0.0014 Å
α	90°
β	110.055 ± 0.002°
γ	90°
Cell volume	2457 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0192
Residual factor for significantly intense reflections	0.0189
Weighted residual factors for significantly intense reflections	0.0502
Weighted residual factors for all reflections included in the refinement	0.0504
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178583 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/94.	4069409.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4069409.cif
40283	2012-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4069407, 4069408, 4069409 via cif-deposit CGI script.	4069409.cif