Crystallography Open Database

Information card for entry 4069527

Preview

Coordinates	4069527.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H42 Er2 N4
Calculated formula	C46 H42 Er2 N4
Title of publication	Investigations on Organolanthanide Derivatives with the Hydrazonido (−NHN═CPh2) Ligand: Synthesis, Crystal Structure, and Reactivity
Authors of publication	Han, Yanan; Zhang, Jie; Han, Fuyan; Zhang, Zhengxing; Weng, Linhong; Zhou, Xigeng
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	13
Pages of publication	3916
a	8.243 ± 0.006 Å
b	11.398 ± 0.008 Å
c	21.169 ± 0.015 Å
α	99.501 ± 0.008°
β	100.715 ± 0.008°
γ	98.183 ± 0.008°
Cell volume	1896 ± 2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1981
Residual factor for significantly intense reflections	0.1148
Weighted residual factors for significantly intense reflections	0.2829
Weighted residual factors for all reflections included in the refinement	0.327
Goodness-of-fit parameter for all reflections included in the refinement	1.092
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178584 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/95.	4069527.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4069527.cif
40317	2012-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4069520, 4069521, 4069522, 4069523, 4069524, 4069525, 4069526, 4069527 via cif-deposit CGI script.	4069527.cif