Crystallography Open Database

Information card for entry 4069540

Preview

Coordinates	4069540.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H91 B F4 Os2 P4
Calculated formula	C36 H91 B F4 Os2 P4
Title of publication	Trapping of a 12-Valence-Electron Osmium Intermediate
Authors of publication	Buil, María L.; Esteruelas, Miguel A.; Garcés, Karin; García-Raboso, Jorge; Oliván, Montserrat
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	15
Pages of publication	4606
a	17.14 ± 0.004 Å
b	15.568 ± 0.004 Å
c	17.737 ± 0.004 Å
α	90°
β	99.757 ± 0.004°
γ	90°
Cell volume	4664.4 ± 1.9 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0497
Residual factor for significantly intense reflections	0.031
Weighted residual factors for significantly intense reflections	0.0469
Weighted residual factors for all reflections included in the refinement	0.0497
Goodness-of-fit parameter for all reflections included in the refinement	0.827
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178584 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/95.	4069540.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4069540.cif
40324	2012-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4069539, 4069540 via cif-deposit CGI script.	4069540.cif