Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4069551
Preview
| Coordinates | 4069551.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C27 H32 N2 Pt Si |
|---|---|
| Calculated formula | C27 H32 N2 Pt Si |
| SMILES | [PtH2]1([Si](CC)(CC)CC)[n]2c(c3n1c(cc3c1ccccc1)c1ccccc1)cccc2 |
| Title of publication | Five-Coordinate Dihydridosilyl Platinum(IV) Complexes Supported by a Chelating Monoanionic Nitrogen-Based Ligand |
| Authors of publication | McBee, Jennifer L.; Tilley, T. Don |
| Journal of publication | Organometallics |
| Year of publication | 2009 |
| Journal volume | 28 |
| Journal issue | 13 |
| Pages of publication | 3947 - 3952 |
| a | 41.674 ± 0.008 Å |
| b | 9.7404 ± 0.0018 Å |
| c | 24.917 ± 0.005 Å |
| α | 90° |
| β | 104.912 ± 0.003° |
| γ | 90° |
| Cell volume | 9774 ± 3 Å3 |
| Cell temperature | 146 ± 2 K |
| Ambient diffraction temperature | 146 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 9 |
| Hermann-Mauguin space group symbol | C 1 c 1 |
| Hall space group symbol | C -2yc |
| Residual factor for all reflections | 0.0834 |
| Residual factor for significantly intense reflections | 0.0516 |
| Weighted residual factors for significantly intense reflections | 0.0874 |
| Weighted residual factors for all reflections included in the refinement | 0.1013 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.018 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 209982 (current) | 2018-08-20 | cif/4/ Updating bibliography in entries 4069551, 4083428. Marking entry 4083428 as a duplicate of entry 4069551. |
4069551.cif |
| 178584 | 2016-03-21 | cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/95. |
4069551.cif |
| 103932 | 2014-03-08 | cif/4 Fixing Z values and formulae for several entries |
4069551.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4069551.cif |
| 40329 | 2012-03-07 | ../uploads/cif-deposit/cod/cif Adding structures of 4069551 via cif-deposit CGI script. |
4069551.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.