Crystallography Open Database

Information card for entry 4069729

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Structure parameters

Formula	C45 H40 Cl2 P2 Pt Si
Calculated formula	C45 H40 Cl2 P2 Pt Si
Title of publication	Synthesis and Characterization of Neutral and Cationic Platinum(II) Complexes Featuring Pincer-like Bis(phosphino)silyl Ligands: Si−H and Si−Cl Bond Activation Chemistry
Authors of publication	Mitton, Samuel J.; McDonald, Robert; Turculet, Laura
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	17
Pages of publication	5122
a	13.5856 ± 0.0014 Å
b	16.9084 ± 0.0017 Å
c	19.771 ± 0.002 Å
α	89.7276 ± 0.0014°
β	76.0291 ± 0.0014°
γ	67.8835 ± 0.0013°
Cell volume	4064.2 ± 0.7 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0874
Residual factor for significantly intense reflections	0.0498
Weighted residual factors for significantly intense reflections	0.1225
Weighted residual factors for all reflections included in the refinement	0.1423
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
301829 (current)	2025-08-20	Add cross-references to PubChem compounds in COD range 4/06/ Each referenced PubChem compound corresponds to the full crystal structure.	4069729.cif
178586	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/97.	4069729.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4069729.cif
40416	2012-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4069729, 4069730, 4069731, 4069732, 4069733 via cif-deposit CGI script.	4069729.cif